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Originally techniques dropped formaldehyde into the mixture of phosphorous acid and monosodium of imino diacetic acid in high temperature. Owing to phosphorous acid is produced from phosphorus trichloride in industry by hydrolysis, inspissation and crystallization, if we use phosphoros trichloride directly on synthesize N- iminodiacetic acid, not only can simplify operation, but also can reduce the cost and save energy.

原工艺采用的是在酸性条件下高温时将甲醛滴加到亚磷酸与亚氨基二乙酸一钠盐混合溶液中进行反应,考虑到工业上亚磷酸的合成一般采用三氯化磷水解、提浓、结晶制得,直接将三氯化磷用于双甘膦的合成,不仅可以简化操作过程,而且对于降低生产成本和能耗有明显意义。

Chemical oxidations of sodium plumbite solution in alkali are readily achieved with chlorine, bromine, and hydrogen peroxide and simple lead salts may be oxidized with 37 M nitric acid.

用氯、溴和过氧化氢在碱性条件下可实现化学氧化铅酸钠。简单的二价铅的盐可用37M的硝酸溶液来氧化

Methods Tissue culture was used to study the cataractous lenses of rats induced by sodium selenite or galactose. At the early stage, the content of nonprotein sulfhydryl, protein sulfhydryl, non-soluble disulfide bond, malonaldehyde and the activities of glutathione peroxidase, glutathione reductase and glutathione-S-transferase were measured in the cataractous lenses, and they were compared with that of the normal lenses. Results The two kinds of material could all induce cataract in rats, sodium selenite being more potent.

采用器官培养方法,以不同浓度亚硒酸钠及半乳糖作用于晶状体,诱发大鼠晶状体形成白内障,在培养初期测定晶状体内非蛋白质巯基(nonprotein sulfhydryl, NP-SH、蛋白质巯基(protein sulfhydryl ,P-SH)和不溶性蛋白质二硫键的含量,脂类过氧化水平,以及与谷胱甘肽代谢有关的谷胱甘肽过氧化物酶(GSH peroxidase, GSH-PX)、谷胱甘肽还原酶(GSH reductase, GSSG-R)及谷胱甘肽硫转移酶(GSH S transferase, GSH-S)的活性。

In pH value 6.40 Clark-Lubs buffer solution, the fluorescence intensity of safranine T and sodium dodecyl benzene sulfonatewas determined. After adding organophosphorus pesticides, the fluorescence intensity was determined. Based on this, a new fast and simple method for determination of the organophosphorus pesticides total-residues was developed.

方法]在pH值6.40的Clark-Lubs缓冲溶液中,加入碱性藏花红与一定浓度的十二烷基苯磺酸钠,测定荧光强度,再加入有机磷农药,检测荧光强度变化,据此建立测定有机磷农药残留总量的新方法。

It is based on the facts that in the presence of sulfuric acid and sodium dodecyl benzene sulfonate, vanadium activated by vitamin C can catalyze potassium bromate to oxidize safranine O, the oxidation products of safranine O can emit intense and stable fluorescence on nitrocellulose membrane.

基于在硫酸介质和十二烷基苯磺酸钠存在下,抗坏血酸活化钒催化溴酸钾氧化番红花红O发射强而稳定的荧光的特性,建立了ⅤC活化溴酸钾氧化番红花红O催化荧光法测定痕量钒的新方法。

Study on the optimal conditions of cellulase from termites The optimal pH when Cx from Reticulitermes flaviceps reacted with substrate sodium carboxymethylcellulose was between 5.0-7.4 and 5.0-6.2 when BG enzyme was reacted with substrate salicin, the relation between activities of enzymes and relevant pH values accorded with Quadratic models.

一、白蚁纤维素酶最适反应条件研究黄胸散白蚁 Reticulitermes flaviceps C_N酶与羧甲基纤维素钠(Carboxymethylcellulose sodium,CMC-Na)反应的最适pH值范围在5.0-7.4之间,BG酶与Salicin反应的最适pH值为5.0-6.2,2种酶的活性均与pH值符合二次项曲线模型。

Methods Porcine bile duct and ureter were treated using detergent sodium dodecylsulphate and 1% Triton X-100 to prepare the acellular lumens matrix. The toxic effects of different concentrations of acellular lumens matrix extract were tested by MTT to assess the proliferation of human scarfskin fibroblasts. The cytotoxicity of the target biomaterial was graded according to the national standards. The growth manner of the human intrahepatic bile duct endothelial cells seeded on the acellular lumens matrix was studied after 20 d under scanning electron microscopy.

采用十二烷基磺酸钠、Triton X-100处理封闭群小香猪输尿管和胆管,获得去细胞管腔基质支架材料; MTT法检测基质支架材料的不同浓度浸提液对细胞增殖的影响,并按医用生物材料细胞毒性分级标准进行评级;在基质支架材料上种植人肝内胆管上皮细胞,于接种后20 d通过扫描电镜观察人肝内胆管上皮细胞在支架上的生长情况。

The effects of mixed ratio and concentration on the spontaneous formation of vesicles in a cationic cetyltrimethylammonium bromide and anionic sodium dodecylbenzenesulfonate system were investigated.

讨论了十六烷基三甲基溴化铵/十二烷基苯磺酸钠复配比例、体系浓度对其囊泡自发形成的影响和不同制备方法与放置时间对囊泡尺寸的影响,同时用TEM考察了囊泡的结构与形态。

Catalytic activities and regioselectivities of sodium dihydrogen phosphate for nitrations of toluene were investigated by gas chromatography.

研究了磷酸二氢钠催化甲苯硝化反应的催化活性,通过气相色谱考察了催化剂用量、反应时间、硝化反应温度及催化剂的重复使用等因素对甲苯转化率和产物区域选择性的影响。

The carbon foam were prepared by self-bubbling at high pressure from AR pitch added sodium dodecyl benzene sulfonate and Span-40, respectively. The bulk density, pore rate, compressive strength, thermal conductivity at room temperature and crystallitic parameters of carbon foam were measured. The rheological properties of AR pitch and pore structure of carbon foam were investigated.

以十二烷基苯磺酸钠和Span-40表面活性剂为添加剂,AR沥青为原料,制备炭素泡沫材料,测定了材料的体积密度、显气孔率、压缩强度、常温热导率以及微晶结构参数,研究了添加表面活性剂后AR沥青的流变性能和炭素泡沫材料孔胞结构的变化。

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