二钠的

The crosslinked rubber with dicyclopentadienecrosslinkage was prepared by the reaction between the chlorohydrin rubberand the cyclopentadienyl sodium.

以环戊二烯基钠与氯醇橡胶反应，制得了含CPD侧基和双环戊二烯交联的聚合物。

The total iron in iron ore was titrated by potassium permanganate standard solution with sodium diphenylamine sulfonate as indicator.

用HNO3-HF处理，硫-磷混酸溶解试样，在盐酸介质中，用二氯化锡－三氯化钛将Fe(上标 3+)还原为Fe(上标 2+)，以二苯胺磺酸钠为指示剂，以高锰酸钾标准溶液滴定铁矿石中的全铁量。

Mesoporous zincum sulfide is synthesized by room-temperature method and hydrothermal technique, employing the surfactant cetyltrimethyl ammonium bromide, duodecimal alkyl sulfonic natrium and lauryl amine as templates. All kinds of technic parameters' influence to the synthesis has been systematically discussed, and the extracting of templates have been investigated.

本论文以十六烷基三甲基溴化铵、十二烷基磺酸钠及十二胺为模板，采用水热法和室温法合成了介孔硫化锌，系统探讨了各种工艺参数对合成材料结构特征的影响。

In order to reduce the corrosion of acidic paint stripper to aeronautical metals and provide with better anti-corrosion additive for AIL4130, TC4, LY12, and 20(superscript #) steel, a series of inhibitors and their composite were investigated. Weight loss experiment, Tafel curves measurement and SEM observation were carried out for the above metals in the formic acid solution which was normally used in the paint stripper. The experimental results indicate that the optimizing composite inhibitor consists of sodium benzoate, 2-thiourea, hexamethylenetetramine, sodium laurylsulfonate and 1, 2, 3-benzotriazole.

为降低酸性脱漆剂对飞机金属材料的腐蚀，以脱漆剂中经常使用的甲酸水溶液为研究介质，以AIL4130、TC4、LY12、20钢等材料为研究对象，通过腐蚀失重法、塔菲尔曲线测量和SEM观察，筛选出对以上各金属材料缓蚀效果较好的复配缓蚀剂体系，即苯甲酸钠、硫脲、六次甲基四胺、十二烷基磺酸钠、苯并三氮唑等缓蚀剂的优化组合。

A selective and mild PS-DIB/ionic-liquid immobilized 2, 2, 6, 6-tetramethyl-piperidin-4-ol-N-oxyl catalytic oxidation procedure of alcohols to the corresponding aldehydes and ketones in ionic liquid BF4 at room temperature was developed. The oxidant PS-DIB was prepared via the iodation and acetylation of polystyrene resin. For the preparation of the ionic-liquid immobilized TeMPO catalyst, 4-(2, 2, 6, 6-Tetramethyl-1-oxyl-4-piperidoxyl)butyl bromide was first synthesized from TeMPO and 1, 4-dibromobutane.

将聚苯乙烯树脂先碘化再乙酰基化，制得了负载型二乙酰氧碘苯作为氧化剂。2， 2， 6， 6-四甲基－N-氧自由基哌啶醇与1， 4-二溴丁烷反应生成4-溴丁氧基－2， 2， 6， 6-四甲基－哌啶－1-氧化物，再与N-甲基咪唑发生季铵化反应，生成的溴化季铵盐与四氟硼酸钠进行离子交换制得氟硼酸型2， 2， 6， 6-四甲基－N-氧自由基哌啶负载离子液体。

A selective and mild PS-DIB/ionic-liquid immobilized TEMPO catalytic oxidation procedure of alcohols to the corresponding aldehydes and ketones in ionic liquid BF4 at room temperature was developed. The oxidant PS-DIB was prepared via Iodation and acetylation of polystyrene resin. For the preparation of the ionic-liquid immobilized TEMPO catalyst, 4-(2,2,6,6-Tetramethyl-1-oxyl-4-piperidoxyl)butyl bromide was first synthesized from 2,2,6,6-tetramethyl-piperidin-4-ol-N-oxyl and 1,4-dibromobutane.

将聚苯乙烯树脂先碘化再乙酰基化，制得了负载型二乙酰氧碘苯(diacetoxyiodo polystyrene，PS-DIB)作为氧化剂。2，2，6，6-四甲基-N-氧自由基哌啶醇(2，2，6，6-tetramethyl-piperidin-4-ol-N-oxyl，TEMPO)与1，4-二溴丁烷反应生成4-溴丁氧基-2，2，6，6-四甲基-哌啶-1-氧化物，再与N-甲基咪唑发生季铵化反应，生成的溴化季铵盐与四氟硼酸钠进行离子交换制得氟硼酸型2，2，6，6-四甲基-N-氧自由基哌啶负载离子液体TEMPO-IL。

The diameter of secondary pore is 2.64nm, which is twice of the diameter of supercage, therefore we suggested that secondary pore was formed by connecting two adjacent supercages resulted from breakdown of the sodalite between them.

我们以〓Xe NMR方法，首次得到超稳Y型沸石中二次孔的大小为264nm，该直径约为超笼直径的二倍，因此我们认为二次孔的形成是方钠石笼被破坏后，两个相邻超笼相连的结果。

In this paper the emulsion of polyacrylamide was synthesized in the polyglycol solutions, acryl amide and acrylic acid sodium was used as the monomer. In more detail, we investigated the effect of the concentration of the monomers, the ratio of monomer and PEG, the ratio of monomers, temperature, and emulsifier on the stability of the HPAM emulsion and the molecular weight of the HPAM.

为了提高聚丙烯酰胺相对分子质量，以丙烯酰胺与丙烯酸钠为原料，在聚乙二醇水溶液中合成了聚丙烯酰胺水包水乳液，考察了初始单体质量分数、共聚单体与聚乙二醇摩尔比、共聚单体摩尔比、聚合反应温度、乳化剂种类及其浓度对HPAM水包水乳液稳定性及相对分子质量的影响，所得共聚产物相对分子质量可达1.5×10^7。

Given the current complexity of industrial recovery of 3'-methyl-2'-butenyl 3, 3-dimethyl-pentenoate and the decomposition problems with 2-methyl-1-butene, research was conducted on a process for direct recycling of MBDP involving an ester exchange reaction of MBDP with either methanol, trimethyl orthoacetate, or solutions of methanol and trimethyl orthoacetate.

针对目前工业上回收3，3-二甲基－4-戊烯酸－3'-甲基－2'-丁烯酯工艺复杂、异戊烯大量分解问题，研究了MBDP直接返回循环使用工艺，MBDP与甲醇、原乙酸三甲酯或与甲醇原乙酸三甲酯混合溶液进行酯交换反应的回收新工艺，比较了四异丙基钛酸酯、甲醇钠、氢氧化钾用作酯交换催化剂的效果，筛选出回收MBDP&一锅煮&最佳工艺：按照n：n：n：n＝1.0：9.8：9.2：0.05物质的量比投料，74℃~78℃反应21h，MBDP转化为贲亭酸甲酯和异戊烯醇，单程转化率87.7%，用85%的磷酸中和甲醇钠，蒸出甲醇，直接用于合成贲亭酸甲酯。

Methods:The target compound was synthesized using 4-hydrazino-N-methyl-benzyl-sulphonamide hydrochloride and 4,4-dimethoxy-N,N-dimethyl butylamine as the starting materials,PPA and sodium dihydrogen phosphate instead as catalysts and isopropyl ether and acetone as solvents for recrylstallization,via 4-step reactions:condensation,rearrangement,cyclization and salt formtion.

以4-肼基-N-甲基-苄基磺酰胺盐酸盐与4，4-二甲氧基-N，N-二甲基-丁胺为起始原料，改用多聚磷酸和磷酸二氢钠作为催化剂，后处理采用异丙醚和丙酮作为重结晶溶剂，经缩合、重排、环合、成盐的4步反应合成琥珀酸舒马曲坦。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。