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In the present study, we have investigated the antidotal action of several sulphhydryl compounds against Sb-71 and their influence upon the inhibiting action of Sb-71 on Ehrlich ascites tumour in mice.

二巯基丁二酸钠1500毫克/公斤,BAL-glucoside 2000毫克/公斤,BAL 40毫克/公斤或半胱氨酸1000毫克/公斤可分别将Sb-71的急性LD_(50)剂量由40毫克/公斤提高至232,76,68和87毫克/公斤。

The model of adiabatic spherical to columnar hydrogen bubble growth in large leak sodium water reaction as well as the model of secondary loop pressure propagation with the one dimensional characteristic method are established under one double ended guillotine tube break in the steam generator of liquid metal cooled fast breeder reactor.

研究建立了钠冷快堆蒸汽发生器在单管束发生双端断裂情况下钠水反应中气泡从球形到柱状的变温绝热生长模型,及采用一维特征线方法建立的压力波在快堆二回路中的传播模型。模型中考虑了爆破膜、管壁弹性变形和气蚀的影响。

The antimony doped tin oxide nanoparticles were synthesized at 240℃for 17 h by the complexing hydrothermal oxidation method using stannate, antimony white and sulphuric acid as the starting materials, sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant. The resulting powders were characterized by means of differential thermal analysis, infrared spectrometry, X-ray diffraction and transmission electron microscope. The mechanism of the preparation of ATO powder was investigated as well.

摘 要:以锡酸钠、锑白和硫酸为原料,酒石酸氢钠为配合剂,双氧水为氧化剂,采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时,合成单分散性的蓝色锑掺杂二氧化锡粉末,用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征,并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

The antimony-doped tin oxide nanoparticles were synthesized at 240℃ for 17h by the complexing-hydrothermal oxidation method using stannate, antimony white and sulphuric acid as the starting materials, sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant. The resulting powders were characterized by means of differential thermal analysis, infrared spectrometry, X-ray diffraction and transmission electron microscope. The mechanism of the preparation of ATO powder was investigated as well.

以锡酸钠、锑白和硫酸为原料,酒石酸氢钠为配合剂,双氧水为氧化剂,采用配合-水热氧化法在水热氧化温度为240℃和水热保温时间为17h时,合成单分散性的蓝色锑掺杂二氧化锡粉末,用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征,并对ATO纳米粉体的配合-水热氧化合成机理进行探讨。

The antimonydoped tin oxide nanoparticles were synthesized at 240 ℃ for(17 h) by the complexinghydrothermal oxidation method using stannate,antimony white and sulphuric acid as the starting materials,sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant.

以锡酸钠、锑白和硫酸为原料,酒石酸氢钠为配合剂,双氧水为氧化剂,采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时,合成单分散性的蓝色锑掺杂二氧化锡粉末,用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征,并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

The antimonydoped tin oxide nanoparticles were synthesized at 240 ℃ for(17 h) by the complexing hydrothermal oxidation method using stannate,antimony white and sulphuric acid as the starting materials,sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant.

以锡酸钠、锑白和硫酸为原料,酒石酸氢钠为配合剂,双氧水为氧化剂,采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时,合成单分散性的蓝色锑掺杂二氧化锡粉末,用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征,并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

The spectral test results indicate that besides polyphosphoric acid,silicon phosphates on silica supported H_3PO_4 are also formed.On silica supported NaH_2PO_4 only sodium polyphosphates are present.

光谱试验结果显示,在二氧化硅负载的磷酸上,除了聚磷酸外,还有硅磷酸盐的存在;在二氧化硅负载的磷酸二氢钠上,仅发现聚磷酸钠存在。

Also, the type of dispersion of four gasliquid-liquid systems: air-decane-aqueous solution of sodium sulfite and surfactant, airmixture of decane and dodecene-aqueous solution of rhodium complex, ligand, and surfactant, air-mixture of decane, dodecene and tridecyl aldehyde-aqueous solution of rhodium complex, ligand and surfactant, and air-mixture of decane and dodeceneaqueous solution of trisodium salt of tri (m-sulfophenyl) phosphine, and surfactant is determined by electric conductivity.

本文采用电导率测量的方法实验研究了空气—正癸烷—亚硫酸钠和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷、1-十二碳烯和十三醛混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—三间磺化苯基膦三钠盐和十六烷基三甲基溴化铵水溶液四个三相体系的液液分散特性。当有机相与水相体积比分别为7/3、1/1和3/7时,前三个体系均形成水包油型分散,并有稳定的乳状液生成。

Using trimeric surfactant C_(14-2-14-2-14) as templating agent, the low cost and facile inorganic species sodium aluminate and sodium silicate as inorganic precursors, highly ordered 2D hexagonal aluminosilicate MCM-41 with high Al content were successfully synthesized.

利用廉价易得的硅酸钠和偏铝酸钠作为无机前驱体,以低聚季铵盐表面活性剂C_(14-2-14-2-14)为模板剂合成了高铝含量,高有序性的二维六方结构介孔硅铝酸盐材料,并对材料的结构、表面性质、形貌以及酸性进行了研究。

In mole antimony-doped tin oxide were deposited on soda-lime glass substrate s with and without SiO_2-coated by the solgel method.

用溶胶凝胶法在已镀SiO2膜的钠钙硅玻璃和没有镀SiO2的钠钙硅玻璃基片上镀制了锑掺杂摩尔分数为8.0%的二氧化锡薄膜。

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