二钠的

Pretreatment of arsenical refractory gold concentrate - Leaching by sodium dichromate ;2. The solution of sulfuric acid was added dropwise to the reaction vessel contained 1,3-dichloro-2-propanol, sodium dichromate and water.

将硫酸水溶液滴加到1，3-二氯-2-丙醇与重铬酸钠水溶液的混合物中，在温度23~27℃的条件下搅拌反应5 h，重铬酸钠∶1，3-二氯-2-丙醇=1∶2，此条件下收率为79。

The solution of sulfuric acid was added dropwise to the reaction vessel contained 1,3-dichloro-2-propanol, sodium dichromate and water.

将硫酸水溶液滴加到1，3-二氯-2-丙醇与重铬酸钠水溶液的混合物中，在温度23~27℃的条件下搅拌反应5 h，重铬酸钠∶1，3-二氯-2-丙醇=1∶2，此条件下收率为79.6%。

The softening water capability of sodium metasilicate is poor. New phosphate-free detergent builders are developed in order to increase softening water capability of alkali silicates.

新型无磷洗涤助剂的研究围绕着提高碱金属硅酸盐的抗硬水能力展开，一是制备结晶层状二硅酸钠，二是将硅酸钠与其它助剂复合制备复合洗涤助剂。

The dispersion mechanism of the dispersants was analyzed by testing the Zeta potential of the dispersion phase in the dispersion medium. It was shown that Ⅰ and Ⅱ raised obviously the absolute values of surface Zeta potential of titania particles, and NK-1 formed good solvate layers of the particles so that the nano-titania particles were stably dispersed in the water solns.

通过测定分散相在分散递质中的Zeta电位，分析了分散剂的分散机理，说明六偏磷酸钠和硅酸钠可显著提高整理液中二氧化钛颗粒表面Zeta电位的绝对值，NK-1在纳米二氧化钛颗粒表面形成良好的溶剂化层，使纳米二氧化钛颗粒在水溶液中获得优良的分散稳定性。

Each medicine used in the study totally has obivious effect on lens sodium-pump. Either on the molecular and cellular level or on the histological and organic level , they all have their distinctive demonstration. 1.Ouabain、Digoxine、DMSO decrease the expression of αsubunit of sodium pump on mRNA level , the cell morphology and ultramicroscopic structure demonstrated destructive effect,it indicates the cause of cataract of the medicines.2.D-thyroxine、Amphotericin B、Vitamin E increase the expression of αsubunit of sodium pump on mRNA level ,from the demonstration of the cell morphology and ultramicroscopic structure ,it indicates the medicines have protective or anti-distructive effect on lens.3.The medicines have isoform-specific action on lens sodium-pump,it indicates exploitting isoform-specific medicine has a promising clinical application.4. Lens sodium-pumps are inhibited probably lead to cataract, so in clinical medication, especially to the cardiovascular doctor, while he is using the sodium-pump inhibitors, he should pay more attention to adjust the dosage and duration of the drug therapy. 5. To creat the animal model of cataract through inhibiting lens sodium-pump, whether it can be a kind of classical method or not, it is worthy of further research.

本研究所选用的药物对晶状体钠泵均有明显的影响作用，在分子水平、细胞水平、组织器官水平均有特异的表现：1、哇巴因、地高辛、二甲基亚砜三种药物可降低晶状体钠泵α亚单位在 mRNA水平的表达，在细胞形态和超微结构上表现为损伤效应，提示了其潜在的导致白内障的可能。2、D甲状腺素、两性霉素B、维生素 E三种药物可升高晶状体钠泵α亚单位在 mRNA水平的表达，从细胞形态和超微结构上的表现，提示了其对晶状体有保护作用或抗损伤效应。3、药物作用于晶状体钠泵具有重整异构特异性，提示了开发出特异的具有重整异构作用的药物是极有临床应用前景的。4晶状体钠泵抑制后可能导致白内障的发生，故临床用药，尤其是心内科医生在使用这些钠泵抑制剂时应注意调整用药剂量及药物疗程。5 通过抑制晶状体钠泵来制作白内障动物模型能否成为一种经典的制作方法，还有待于进一步研究。

The possible pathway of ABAS degraded by Zoogloea HP3 was that ABAS was first cleaved to produce o-phthalic acid and products. The former was further degraded and the composites of the latter were 2-amino-3-hydroxyl-5bromobenzenic sulfonic sodium and 2, 3-dihydroxyl-5-bromobenzenic sulfonic sodium.

动胶菌HP3作用下溴胺酸可能的降解途径为蒽醌环开裂生成中间产物邻苯二甲酸，邻苯二甲酸被进一步降解；溴胺酸降解后的最终产物为2-氨基-3-羟基-5-溴苯磺酸钠和2，3-二羟基-5-溴苯磺酸钠。

Reaction of ketones with sodium diselenide and sodium hydrogen selenide under the catalysis of n-BuNH2 gave a moderate yield of diselenides in a "one-pot" fashion.

在正丁胺的催化下，酮与硒氢化钠、二硒化钠乙醇溶液通过&一锅&法反应得到了中等产率的二硒醚。

A new type builder for phosphatefree detergent:Layered crystal sodium disilicate;2. One way is the manufacturing of crystalline layered sodium disilicates, and the other is that of the manufacture of composite detergent builders.

新型无磷洗涤助剂的研究围绕着提高碱金属硅酸盐的抗硬水能力展开，一是制备结晶层状二硅酸钠，二是将硅酸钠与其它助剂复合制备复合洗涤助剂。

The oxidation of p-nitrotoluene-2-sulfonic acid to prepare 4, 4'-dinitrostilbene-2, 2'-disulfonic acid was monitored, and the mechanism for the formation of by-products 4-nitrobenzaldehyde-2-sulfonic acid and 4-nitro-2-sulfobenzonic acid was suggested.

跟踪了对硝基甲苯邻磺酸制备4，4'-二硝基二苯乙烯－2，2'-二磺酸的过程，推测了4-硝基苯甲醛2-磺酸钠与4-硝基苯甲酸2-磺酸钠杂质的生成机理。

The products were identified by IR,NMR,MS and elemental analysis. In our method,K.OH was used in place of NaOH to synthesize benzyl ester of 3,5-dimethyl-4-hydroxybenzoic acid,2',6'-dimethyl-4'-(n-succinimidyloxycarbonyl) phenyl-acridinium-9-carboxylate was purified on a silica gel column with chloroform/ethylacetate(4:l,v/v) as eluent and further purified by triturating with hexane/acetone(2:l,v/v).The luminescence produced by DMAE-NHS is a flash light with maximumemission at 0.4s and decay half-time of 0.9s. The luminescence intensity is 6.11x10 cps/mol,which is affected by the composition of trigger and surfactant.

DMAE·NHS的合成是本论文的关键和难点，我们对文献方法进行改进：文献方法用氢氧化钠与3，5-二甲基-4-羟基苯甲酸反应制得3，5-甲基-4-羟基苯甲酸钠，再用3，5-二甲基-4-羟基苯甲酸钠与苄氯作用制备3，5-二甲基-4-羟基苯甲酸苄酯，我们用氢氧化钾代替氢氧化钠，使合成取得成功；在合成2'，6'-二甲基-4'-苯基-吖啶-9-甲酸酯时，文献方法对粗产品进行两次硅胶柱层析纯化，第一次柱层析用氯仿/乙酸乙酯(4：1，Ⅴ：Ⅴ)作溶剂和淋洗剂，第二次柱层析用己烷/丙酮(2：1，Ⅴ：Ⅴ)作溶剂和淋洗剂，按照文献方法得到的不是所需要的化合物，我们只进行第一次柱层析纯化，然后用己烷/丙酮(2：1，Ⅴ：Ⅴ)进行研磨，过滤，洗涤，除去溶于己烷/丙酮(2：1，Ⅴ：Ⅴ)的部分，得到所需要的产品。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。