二钠

Main products: Ifosfamide,Ifosfamide acylate,2-Deoxy-D-Glucose,Vecuronium Bromide, Ceftiofur Hcl,Ceftiofur Sodium,Buflomedil Hcl,Oteracil Potassium,Gimeracil,Cinildipine

主要产品有：异环磷酰胺、异环磷酰胺酰化物、2-脱氧-D-葡萄糖、维库溴铵、头孢噻呋、头孢噻呋钠、氧嗪酸钾、吉莫斯特、西尼地平、马尼地平、培美曲塞、培美曲塞酸、培美曲塞二钠、尼索地平、消旋卡多曲、雷尼酸锶、盐酸丁咯地尔、1-(3-三氟甲基苯基)哌嗪、4-溴-2-甲基苯甲酸。

Main products: Ifosfamide,Ifosfamide acylate,2-Deoxy-D-Glucose,Vecuronium Bromide, Ceftiofur Hcl,Ceftiofur Sodium,Buflomedil Hcl,Oteracil Potassium,Gimeracil,Cinildipine, Manidipine dihydrochloride,Pemetrexed intermediate,Pemetrexed acid,Pemetrexed Disodium, Nisoldipine, Racecadotril, Strontium Ranelate, 1-(3-Trifluoromethylphenyl)piperazine hydrochloride, 4-Bromo-2-methylbenzoic acid.

主营业务：主要产品有：异环磷酰胺、异环磷酰胺酰化物、2-脱氧-D-葡萄糖、维库溴铵、盐酸头孢噻呋、头孢噻呋钠、氧嗪酸钾、吉莫斯特、西尼地平、盐酸马尼地平、培美曲塞、培美曲塞酸、培美曲塞二钠、尼索地平、消旋卡多曲、雷尼酸锶、盐酸丁咯地尔、1-(3-三氟甲基苯基)哌嗪盐酸盐、4-溴-2-甲基苯甲酸。

When proceeding the research of drug identification by ultraviolet spectrophotometry, this paper adopts the approaches below: to identify Metronidazole Buccal Tablets and Potassium Sodium Dehydroandroan Drographolide Succinate by ulviolet maximum absorbent wavelength; to identify Metronidazole Disodium Phosphate for Injection by ulviolet maximum absorbent wavelength and minimum absorbent wavelength; to identify Ceftriaxone Sodium for Injection and Clarithromycin Tablets by retention time of high performance liquid chromatography- ultraviolet spectrophotometry.

通过测定紫外最大吸收波长λ_(max鉴别甲硝唑口颊片和炎琥宁、测定紫外最大吸收波长λ_(max和最小吸收波长λ_(min鉴别注射用甲硝唑磷酸二钠，结合高效液相色谱(high performance liquid chromatography-ultraviolet detector，HPLC-UV)中保留时间的测定鉴别注射用头孢曲松钠和克拉霉素片，本文建立了药物鉴别的紫外分光光度法。

The research indicates that:(1) detecting λmax (277nm) can identify Metronidazole Buccal Tablets prepared by Chongqing Medical College;(2) detecting λmax (321nm) and λmin (265nm) can identify Metronidazole Disodium Phosphate for Injection prepared by Chongqing Medical College;(3) detecting tr (6.7min) in HPLC-UV spectrum can identify Ceftriaxone Sodium for Injection prepared by Chongqing Keru Pharmacy Co.;(4) detecting tR (10.2min) 6.7min in HPLC-UV spectrum can identify Clarithromycin Tablets prepared by Harebin Yida Pharmacy Co.;(5) detecting λmax (254nm) can identify Potassium Sodium Dehydroandroan Drographolide Succinate prepared by Hong Kong Yaohen Co..

结果表明：①测定紫外最大吸收波长λ_(max277nm可鉴别重庆医科大学医药研究所制备的甲硝唑口颊片；②测定紫外最大吸收波长λ_(max321nm和最小吸收波长λ_(min265nm可鉴别重庆医科大学医药研究所制备的注射用甲硝唑磷酸二钠；③测定HPLC-UV中的保留时间(t_R6.7min)可鉴别重庆科瑞制药股份有限公司制备的注射用头孢曲松钠；④测定高效液相色谱的保留时间(t_R10.2min)可鉴别哈尔滨伊达制药厂提供的克拉霉素片；⑤测定紫外最大吸收波长(又max254nm)可鉴别香港耀恒公司提供的炎琉宁。

It is a method most in use to analyze drugs.This paper chooses the antibiotics intending to be registered as research topics to study their identification, tests and assay by ultraviolet spectrophotometry. These antibiotics includes Metronidazole Buccal Tablets, Metronidazole Disodium Phosphate for Injection, Ceftriaxone Sodium for Injection, Clarithromycin Tablets, Potassium Sodium Dehydroandroan Drographolide Succinate.

本文选择拟注册的抗生素类药物甲硝唑口颊片、注射用甲硝唑磷酸二钠(Metronidazole Disodium Phosphate for Injection)、注射用头孢曲松钠(Ceftriaxone Sodium for Injection)、克拉霉素片和炎琥宁(Potassium Sodium Dehydroandroan Drographolide Succinate)为研究对象，应用紫外分光光度法进行鉴别、检查和含量测定研究。

Said method includes the following steps: firstly, adopting dipotassium hydrogen phosphate, magnesium sulfate, calcium chloride, citric acid, ammonium ferric citrate, disodium EDTA, sodium carbonate and minor element solution A5 to prepare culture liquor of nostoc according to a certain ratio; then controlling temp. light intensity and deration condition of the culture liquor to make culture of nostoc; third ste, harvesting nostoc; fourth ste, extracting nostoc polysaccharide; and fifth step, purifying, harvesing and drying nostoc polysaccharide.

首先是配制葛仙米培养液：采用磷酸氢二钾、硫酸镁、氯化钙、柠檬酸、柠檬酸铁铵、乙二胺四乙酸二钠盐、碳酸钠，微量元素溶液A5按比例配制；其次是葛仙米的培养：控制温度、光强、光质、培养液通气条件；第三是葛仙米的收获；第四是葛仙米多糖的提取；第五是葛仙米多糖的纯化、收获与干燥。

The factors which affect the average molecular weight of the polymer of AM and DMDAAC were investigated. The optimal reaction conditions are as follows: the concentration of monomer AM was 30%, while DMDAAC was 5%; the reaction temperature was 30℃, the amount of initiators at the low temperature stage was 0.05‰(compared to the weight of the monomers joining the polymerization), while V-50 was 0.025‰, the weight ratio of potassium persulphate to sodium bisulphite is 1:1, the amount of carbamide was 40‰, and complexing agent was 0.05‰, besides, aerate nitrogen gas for 8min, then the high molecular weight polymer (M=1.217×10^7) could be got after 16h reaction.

研究了影响AM与DMDAAC共聚物的平均分子量的因素，得到了优化条件为：单体浓度为30%，DMDAAC与AM摩尔比为5：95，聚合温度为30℃，低温段引发剂用量为0.05‰，K2S2O8与NaHSO3质量比为1：1，偶氮二异丁基脒盐酸盐(V-50)用量为0.025‰，尿素用量为40‰，乙二胺四乙酸二钠(EDTA-2Na)用量为0.05‰，在此优化条件下聚合反应16h后得到分子量为1.217×10^7的阳离子型聚丙烯酰胺。

He sample is dissolved in a mixture of nitric acid and potassium chlorate.The determinations of Te,Bi,Fe and Cu are performed on a flame atomic absorption spectrophotometer.The selenium is determined photormetrically with 3,3'-diaminobenzidine,and the sulfur is determined gravimetrically as barium sulfate,precipitated frorm an EDTA-citric acid medium.

辉碲铋矿物经HNO＿3－KCIO＿3溶解，用火焰原子吸收法或乙二胺四乙酸二钠络合滴定法测定Bi，火焰原子吸收法测定Te、Fe、Cu，3，3＇二氨基联苯胺光度法测定Se，硫酸钡重量法测定S。

An ODS column was selected as the separation column at 25 ℃, and pH 4.50, 0.02 mol/L of trisodium citrate-0.05 mol/L sodium phosphate dibasic to methanol (95:5, volume ratio) without ion-pair at a flow rate of 1.0 mL/min.

该实验采用ODS柱，流动相为V(0.02 mol/L柠檬酸三钠-0.05 mol/L磷酸氢二钠)：V=95：5的溶液，用电化学检测器检测。

The volumetric flask is then filled with a stock solution consisting of 0.010 M HNO3 and 0.001% disodium EDTA dihydrate provided by the TA.

然后用助教提供的，含有0.010M HNO3和0.001%二水合乙二胺四乙酸二钠的储备液，注满容量瓶。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。