二钠

The spectral test results indicate that besides polyphosphoric acid,silicon phosphates on silica supported H_3PO_4 are also formed.On silica supported NaH_2PO_4 only sodium polyphosphates are present.

光谱试验结果显示，在二氧化硅负载的磷酸上，除了聚磷酸外，还有硅磷酸盐的存在；在二氧化硅负载的磷酸二氢钠上，仅发现聚磷酸钠存在。

The resultant of dehydration of both sodium silicate and polysilicic acid is silicic gel. The sodium cations have double impact on the process.

硅酸钠脱水硬化和纯硅酸脱水硬化都生成硅凝胶，钠正离子的存在有正负二重影响。

By orthogonal experimental design method, the optimized degumming parameters have been confirmed: preacid processing, the concentration of sulfuric acid 2 g/L, treatment time 120 min, treatment temperature 60℃, bath ratio 1:15; alkali treatment, the alkaline concentration of one-pot 7.5 g/L, that of two-pot 9 g/L, treatment time of one-pot 3.5h, that of two-pot 2h, treatment temperature 100℃, bath ratio 1:20, each concentration of the Sodium Silicate, carbamide, and JFC 2%.

预酸处理，硫酸溶液质量浓度2 g/L，处理时间120 min，处理温度60℃，浴比1：15；碱处理，一煮碱溶液质量浓度7.5 g/L，二煮碱溶液质量浓度9 g/L，一煮处理时间3.5 h，二煮处理时间2 h，处理温度100℃，浴比1：20，其中一煮与二煮中添加2%的硅酸钠、尿素和JFC。

Methods This study contained a total of 16 culture groups, including one group as control and 5 groups treated by 5 drugs (calcium L-threonate, sodium L-threonate, alendronate, 17β-estradiol and calcium gluconate) each at the final concentrations of 10^(-9)mol/L, 10^(-7)mol/L, 10^(-5)mo1/L respectively. After 7 days, eight bone slices of every group were stained with toluidine blue and the areas of resorptive pits were analyzed under light microscope; the concentrations of C-telopeptide of type Ⅰ collagen CT(subscript x or Crosslaps in culture supernatants were measured by ELISA.

制备骨磨片，培养OC，并分别加入高中低浓度10^(-5、10^(-7)、10^(-9)mol/L的L-苏糖酸钙、L-苏糖酸钠、阿仑麟酸钠、17β-雌二醇、葡萄糖酸钙，实验设以上各浓度组及对照组（共16组，每组n=8），甲苯胺蓝染色一光镜观察分析骨片上骨吸收陷窝面积，ELISA测定上清液Ⅰ型胶原C-末端肽（CTx或Crosslaps）浓度。

The inclusion bodies were washed with Deoxycholic acid Sodium Salt for several times, and then dissolved in N-Lauroyl Sarcosine Sodium for denaturant.

以脱氧胆酸钠洗涤包涵体，然后用N—十二烷基肌氨酸钠溶解，将溶解包涵体进行透析复性。

Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.

采用&一勺烩&方法，以4-羟基苯甲腈为起始原料，首先与硫氢化钠和无水氯化镁在N，N-二甲基甲酰胺中反应，所得中间体不经分离，直接加入2-氯乙酰乙酸乙酯进行环合反应，得到2-(4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯（2）；然后通过六亚甲基四胺/三氟乙酸进行Duff反应，得到2-(3-甲酰基-4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯（3）；再经盐酸羟胺/甲酸/甲酸钠体系脱水得到目标化合物。

Also, the type of dispersion of four gasliquid-liquid systems: air-decane-aqueous solution of sodium sulfite and surfactant, airmixture of decane and dodecene-aqueous solution of rhodium complex, ligand, and surfactant, air-mixture of decane, dodecene and tridecyl aldehyde-aqueous solution of rhodium complex, ligand and surfactant, and air-mixture of decane and dodeceneaqueous solution of trisodium salt of tri (m-sulfophenyl) phosphine, and surfactant is determined by electric conductivity.

本文采用电导率测量的方法实验研究了空气—正癸烷—亚硫酸钠和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷、1-十二碳烯和十三醛混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—三间磺化苯基膦三钠盐和十六烷基三甲基溴化铵水溶液四个三相体系的液液分散特性。当有机相与水相体积比分别为7／3、1／1和3／7时，前三个体系均形成水包油型分散，并有稳定的乳状液生成。

Using trimeric surfactant C_(14-2-14-2-14) as templating agent, the low cost and facile inorganic species sodium aluminate and sodium silicate as inorganic precursors, highly ordered 2D hexagonal aluminosilicate MCM-41 with high Al content were successfully synthesized.

利用廉价易得的硅酸钠和偏铝酸钠作为无机前驱体，以低聚季铵盐表面活性剂C_(14-2-14-2-14)为模板剂合成了高铝含量，高有序性的二维六方结构介孔硅铝酸盐材料，并对材料的结构、表面性质、形貌以及酸性进行了研究。

The invention provides a foliar fertilizer specially used for Chinese gooseberries, which has the functions of cold resistance and consists of the following raw materials according to weight percentage: 0.1 to 8 percent of DMSO, 0.05 to 5 percent of trimethylene glycol, 0.05 to 5 percent of salicylic acid, 0.05 to 2 percent of compound ammonium nitrate, 1 to 15 percent of humic acid, 0.5 to 10 percent of chitosan, 1 to 10 percent of citric acid, 2 to 15 percent of urea, 1 to 10 percent of borax, 1 to 20 percent of zinc sulfate, 0.5 to 10 percent of ferrous sulfate, 0.05 to 5 percent of ammonium molybdate, 1 to 15 percent of manganese sulfate, 0.1 to 2 percent of SDBS and 35 to 80 percent of water.

本发明提供一种具有抗寒作用的猕猴桃专用叶面肥，它由下述各组分重量百分比的原料组成：二甲基亚砜0.1％～8％、丙二醇0.05％～5％、水杨酸0.05％～5％、复硝铵0.05％～2％、腐殖酸1％～15％、壳聚糖0.5％～10％、柠檬酸1％～10％、尿素2％～15％、硼砂1％～10％、硫酸锌1％～20％、硫酸亚铁0.5％～10％、钼酸铵0.05％～5％、硫酸锰1％～15％、十二烷基苯磺酸钠 0.1％～2％、水35％～80％。

The present invention adopts ammonium salt solution as leach, and adopts the liquid-phase oxidation activating agent formed from surfactant sodium ligno-sulfonate or sodium dodecyl sulfonate, liquir phase oxidation catalyst Cu(2+) and sulfur-extracting agent tetrachloroethylene to implement quick leaching process of sulkfide mineral in gas-liquid-solid three-phase reactor, all the sulfurs contained sulfide in mineral powder can be converted into elementary sulfur and sulfuric acid radical, the contained zinc, copper, nickel, cobalt, lead, cadmium and silver can be changed into soluble salt, and fed into leach or remained in the leaching out slag.

本发明涉及的有色金属硫化矿的铵盐液相氧化直接浸出方法，其特征在于：采用铵盐溶液作浸出剂，采用由表面活化剂木质磺酸钠或十二烷基磺酸钠，液相氧化催化剂Cu2+、萃硫剂四氯乙烯组成的液相氧化活化剂，在气液固三相反应器内，实现硫化矿的快速浸出过程，矿粉中各种硫化物所含的硫转变为单质硫和硫酸根，所含的锌、铜、镍、钴、铅、镉、银等变成可溶性盐类进入浸出液中或留在浸出渣中，消除传统流程中二氧化硫，硫化氢，氮氧化物及含砷含汞含铅等有毒烟气的排放。

Shop assistant: Please check at the door.

店员：请您到门口柜台交费。

In the end, transportation of PAHs in the environmental matrix was preliminarily investigated and discussed according to PAHs data of soils and sediments from a certain region in Shanghai. The result indicated that there are two or more pathways on PAHs transportation in the environmental matrix.

最后，对上海特定地区内PAHs在环境介质中的迁移径途进行了分析讨论，结果表明上海市土壤和沉积物等环境介质中PAHs的迁移存在多种途径。