二钠

A process of electrolytic synthesis of sodium perchlorate from sodium chlorate solution by lead dioxide anode based titanium metal is introduced.

介绍了以钛基体二氧化铅作为阳极，电解氯酸钠合成高氯酸钠的过程。

Sodium chlorate solution was electrolyzed for the preparation of sodium perchlorate by two steps method.

采用二步法通过电解氯酸钠溶液制备高氯酸钠。

SBA-15 samples obtained from both silica sources were highly ordered p6mm symmetric pillar structure,as was evidenced by XRD patterns,with similar surface area and slightly larger pore volume for the samples prepared from TEOS than those from sodium metasilicate.

通过X射线粉末衍射对样品进行表征，发现两种硅源合成的SBA-15都具有高度有序的二维六方立柱形结构。它们的比表面积相近，用TEOS作为硅源的SBA-15的孔容比用硅酸钠作为硅源的SBA-15的略大；用硅酸钠作为硅源的SBA-15有更高的微孔率和更厚的孔壁。

II: ① take a thin wire, one end with sand paper wipe, and then lightson alcohol to non-yellow flame ignition,② wire with the end of the water dip, and then dip a number of sodium chloride or anhydrous sodium carbonate powder,③ ignited a new spirit lamp (lamp wick is clean, pure ethanol),④ the stained sodium salt powder on the wire on the ignitiontip, when there is a sharpsmall yellow flame, which is sodium flame.

方法二：①取一条细铁丝，一端用砂纸擦净，再在酒精灯外焰上灼烧至无黄色火焰，②用该端铁丝沾一下水，再沾一些氯化钠或无水碳酸钠粉末，③点燃一盏新的酒精灯，④把沾有钠盐粉末的铁丝放在外焰尖上灼烧，这时外焰尖上有一个小的黄色火焰，那就是钠焰。

The antimony doped tin oxide nanoparticles were synthesized at 240℃for 17 h by the complexing hydrothermal oxidation method using stannate, antimony white and sulphuric acid as the starting materials, sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant. The resulting powders were characterized by means of differential thermal analysis, infrared spectrometry, X-ray diffraction and transmission electron microscope. The mechanism of the preparation of ATO powder was investigated as well.

摘 要：以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

The antimony-doped tin oxide nanoparticles were synthesized at 240℃ for 17h by the complexing-hydrothermal oxidation method using stannate, antimony white and sulphuric acid as the starting materials, sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant. The resulting powders were characterized by means of differential thermal analysis, infrared spectrometry, X-ray diffraction and transmission electron microscope. The mechanism of the preparation of ATO powder was investigated as well.

以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合－水热氧化法在水热氧化温度为240℃和水热保温时间为17h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合－水热氧化合成机理进行探讨。

The antimonydoped tin oxide nanoparticles were synthesized at 240 ℃ for(17 h) by the complexinghydrothermal oxidation method using stannate,antimony white and sulphuric acid as the starting materials,sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant.

以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

The antimonydoped tin oxide nanoparticles were synthesized at 240 ℃ for(17 h) by the complexing hydrothermal oxidation method using stannate,antimony white and sulphuric acid as the starting materials,sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant.

以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

The effect of various concentration of surfactant and sodium dodecylbenzene sulfonate on the aqueous photodegradation of sodium pentachlorophenate were studied.

研究了不同浓度的阴离子表面活性剂十二烷基苯磺酸钠对五氯酚钠在水溶液中光解的影响。

Given the current complexity of industrial recovery of 3'-methyl-2'-butenyl 3, 3-dimethyl-pentenoate and the decomposition problems with 2-methyl-1-butene, research was conducted on a process for direct recycling of MBDP involving an ester exchange reaction of MBDP with either methanol, trimethyl orthoacetate, or solutions of methanol and trimethyl orthoacetate.

针对目前工业上回收3，3-二甲基－4-戊烯酸－3'-甲基－2'-丁烯酯工艺复杂、异戊烯大量分解问题，研究了MBDP直接返回循环使用工艺，MBDP与甲醇、原乙酸三甲酯或与甲醇原乙酸三甲酯混合溶液进行酯交换反应的回收新工艺，比较了四异丙基钛酸酯、甲醇钠、氢氧化钾用作酯交换催化剂的效果，筛选出回收MBDP&一锅煮&最佳工艺：按照n：n：n：n＝1.0：9.8：9.2：0.05物质的量比投料，74℃~78℃反应21h，MBDP转化为贲亭酸甲酯和异戊烯醇，单程转化率87.7%，用85%的磷酸中和甲醇钠，蒸出甲醇，直接用于合成贲亭酸甲酯。

Shop assistant: Please check at the door.

店员：请您到门口柜台交费。

In the end, transportation of PAHs in the environmental matrix was preliminarily investigated and discussed according to PAHs data of soils and sediments from a certain region in Shanghai. The result indicated that there are two or more pathways on PAHs transportation in the environmental matrix.

最后，对上海特定地区内PAHs在环境介质中的迁移径途进行了分析讨论，结果表明上海市土壤和沉积物等环境介质中PAHs的迁移存在多种途径。