二钠

In this method, EDTA was used as complexant which can form 1∶1 complex with Cr〓, this complex carried negative charge and can be detected directly by UV absorbance at 200nm, therefore, the CrO〓 and Cr〓 can be separated and determined in one run.

采用乙酸钠-乙二胺四乙酸钠-CTAB-乙酸缓冲液体系，加入EDTA使Cr〓与其生成的1∶1络合物，带负电荷且具有紫外吸收，在200nm处可用直接紫外法检测。

Analysis of K and Na in nepheline were curried out with higher precision and repeatability by means of adding fluohydric acid during sample melting to remove SiO2 ,adjusting the ratio of K and Na in the solution to reduce the mutual interference of the two elements, and adding cesium chloride to eliminate ionization interference.

摘要本方法用于测定霞石中的钾、钠，主要通过在溶样时加入氢氟酸除去二氧化矽，调整溶液中钾、钠的含量，消除互相之间的干扰，加入氯化铯消除电离因素的干扰，提高了分析结果的准确性和重现性，使测定结果更接近化学分析值。

Analysis f K and Na in nepheline were curried out with higher precision and repeatability by means of adding fluohydric acid during sample melting to remove SiO2, adjusting the ratio of K and Na in the solution to reduce the mutual interference of the two elements, and adding cesium chloride to eliminate ionization interference.

摘要本方法用于测定霞石中的钾、钠，主要通过在溶样时加入氢氟酸除去二氧化矽，调整溶液中钾、钠的含量，消除互相之间的干扰，加入氯化铯消除电离因素的干扰，提高了分析结果的准确性和重现性，使测定结果更接近化学分析值。

By the state-level key high-tech enterprises - Jinke Technology Group Holdings initiated the establishment of the Company, Ltd., founded in May 2001, is located in China's economy the most dynamic Yangtze River Delta, Hangzhou Bay the south bank of Hangzhou Bay Fine Chemical Park, adjacent to Shanghai Port and Ningbo Port, is the factory covers an area of 880 acres, with more than 600 employees, specializing in the production of sodium percarbonate, tetraacetylethylenediamine, sodium perborate, solid peracetic acid and sodium acetate.

浙江金科化工股份有限公司系由国家级重点高新技术企业－金科科技集团控股发起设立的股份有限公司，创建于2001年5月，地处中国经济最具活力的长江三角洲地区，杭州湾南岸的杭州湾精细化工园区毗邻上海港与宁波港，现厂区占地880亩，拥有员工600余名，专业生产过碳酸钠、四乙酰乙二胺、过硼酸钠（SPB、固体过氧乙酸及醋酸钠。

Chemical corporations within this region may provide matching chemical products and raw materials such as citric acid, starch sugar, L-lactic acid, nitrochlorobenzene, paranitrophenol sodium salt sodium para-nitro phenolate, pphenylenediamine , sodiumhydroxide, benzene anhydride, carbonic acid propylene grease, polyacrylamide ,2.4- dinitrochlorobenzene, 2.4- dinitrosixchlorin, and sodium cyanide.

区内化工企业可配套提供柠檬酸、淀粉糖、 L —乳酸、硝基氯苯、对硝基酚钠、对苯二胺、烧碱、苯酐、碳酸丙烯脂、聚丙烯酰胺、2.4—二硝基氯化苯、2.4—二硝基6氯、氰化钠等化工产品或原料。

As a precursive work of polymerization directly from vesicles, a polymerizable surfactant, allyl dodecyl dimethylammonium bromide was synthesized, and spontaneous stable vesicles were formed from aqueous solutions of ADDB and sodium dodecyl sulfonate in equimolar composition.

作为可聚合囊泡制备的前期基础工作，研究了一种可聚合的囊泡体系：1-丙烯基－2，2，二甲基－十二烷基溴化胺和ADDB与十二烷基磺酸钠的等摩尔比混合体系。

Pillared montmorillonite, as a representative of Sandwich like pillared interlayered clays ,caught many scientist"s attention not only because of its special structure of two-dimensional sheets but also its excellent activity of catalysis and adsorption. It is well documented that the method to prepare PILM, ion-exchanging, needed a long periods and was affected by many factors, and that the product had low thermal stability especially hydro-thermal stability which was the primary obstruction of its using in large-scale production. At the same time, PILM was well documented prepared with Na-montmorillonite, while there were a few documents about PILM prepared with Ca-montmorillonite. The large cost of remodel of Ca-montmorillonite to Na-montmorillonite was another obstacle of the application of PILM, while Ca-montmorillonite was widely distributed in nature, as a result, to prepare PILM with Ca-montmorillonite has practical significance. What"s more, PILM was mainly studied as a catalyst in oil refining process till now, but rarely documented in other catalysis reactions, especially in coal liquification filed which also needed high activity catalyst.

以柱撑蒙脱石为代表的具有"三明治"结构的柱撑粘土矿物因其特殊的二维孔道结构和优良的催化和吸附性能近年来成为国内外广泛关注和研究的热点，但是目前国内外大量报道的PILM制备大多采用离子交换法，生产周期很长，影响因素很多，并且产物热稳定性不够高，特别是水热稳定性较差，这是其不能在实际中大规模生产和应用的主要障碍，因此制备一种高稳定性的PILM意义非常；文献中大量报道的都是钠基蒙脱石合成的柱撑粘土矿物，传统的离子交换法必须将钙基蒙脱石钠化改型，其成本相当高，而自然界中大量存在的却是钙基蒙脱石，直接用钙基蒙脱石合成柱撑粘土矿物有很现实的意义，但目前这方面的报道却很少见；另外，迄今为止，PILM作为催化剂的研究领域主要在石油的炼制中应用，而在煤炭的液化中却鲜有报道，如果能在煤炭转化领域应用这一成果，其影响也将是相当大的。

Pillared montmorillonite, as a representative of Sandwich like pillared interlayered clays ,caught many scientist's attention not only because of its special structure of two-dimensional sheets but also its excellent activity of catalysis and adsorption. It is well documented that the method to prepare PILM, ion-exchanging, needed a long periods and was affected by many factors, and that the product had low thermal stability especially hydro-thermal stability which was the primary obstruction of its using in large-scale production. At the same time, PILM was well documented prepared with Na-montmorillonite, while there were a few documents about PILM prepared with Ca-montmorillonite. The large cost of remodel of Ca-montmorillonite to Na-montmorillonite was another obstacle of the application of PILM, while Ca-montmorillonite was widely distributed in nature, as a result, to prepare PILM with Ca-montmorillonite has practical significance. What's more, PILM was mainly studied as a catalyst in oil refinin g process till now, but rarely documented in other catalysis reactions, especially in coal liquification filed which also needed high activity catalyst.

以柱撑蒙脱石为代表的具有"三明治"结构的柱撑粘土矿物因其特殊的二维孔道结构和优良的催化和吸附性能近年来成为国内外广泛关注和研究的热点，但是目前国内外大量报道的PILM制备大多采用离子交换法，生产周期很长，影响因素很多，并且产物热稳定性不够高，特别是水热稳定性较差，这是其不能在实际中大规模生产和应用的主要障碍，因此制备一种高稳定性的PILM意义非常；文献中大量报道的都是钠基蒙脱石合成的柱撑粘土矿物，传统的离子交换法必须将钙基蒙脱石钠化改型，其成本相当高，而自然界中大量存在的却是钙基蒙脱石，直接用钙基蒙脱石合成柱撑粘土矿物有很现实的意义，但目前这方面的报道却很少见；另外，迄今为止，PILM作为催化剂的研究领域主要在石油的炼制中应用，而在煤炭的液化中却鲜有报道，如果能在煤炭转化领域应用这一成果，其影响也将是相当大的。

The diameter of secondary pore is 2.64nm, which is twice of the diameter of supercage, therefore we suggested that secondary pore was formed by connecting two adjacent supercages resulted from breakdown of the sodalite between them.

我们以〓Xe NMR方法，首次得到超稳Y型沸石中二次孔的大小为264nm，该直径约为超笼直径的二倍，因此我们认为二次孔的形成是方钠石笼被破坏后，两个相邻超笼相连的结果。

6 Buffer comprised 6 mmol/L sodium phosphate, 10 mmol/L sodium borate, 25 mmol/L sodium dodecyl sulphate is used as runing solution, and UV detection wavelength is at 227 nm to determining disperse blue 2BLN in dyeing wastewater.

6mmol/L磷酸钠、10mmol/L硼砂、25mmol/L十二烷基磺酸钠组成的pH9 6的缓冲溶液作电泳液，UV检测波长227nm，测定了印染废水中分散蓝2BLN 的含量。

Shop assistant: Please check at the door.

店员：请您到门口柜台交费。

In the end, transportation of PAHs in the environmental matrix was preliminarily investigated and discussed according to PAHs data of soils and sediments from a certain region in Shanghai. The result indicated that there are two or more pathways on PAHs transportation in the environmental matrix.

最后，对上海特定地区内PAHs在环境介质中的迁移径途进行了分析讨论，结果表明上海市土壤和沉积物等环境介质中PAHs的迁移存在多种途径。