二钠

In this paper , two fluorocarbon amphoteric phosphate surfactants were synthesized and their performances were determined.

首先，磷酸二氢钠与环氧氯丙烷开环加成合成2-羟基-3-氯丙基磷酸酯钠，分离提纯后，分析其红外。

This rock zone, with a NE striking, the whole length of 1 400 km and the width of 100～150 km, is characterized by not onlyalkaline rocks (analcite biotite olivine melilitites, leucititic alnoites, nephelite syenites, aegirite augite syenites, melanite syenites, riebeckite syenite and aegirite bearing quartz syenites) and alkaline granite (riebeckite granite, and aegitite augite riebeckite granite), but also a lot of syenites, monzonites and alkaline feldspar granites or miarolitic K feldspar granites.

该岩带全长约1400km，宽100～150km，不仅发育有狭义的碱性岩(方沸黑云橄榄黄长岩、白榴黄长煌斑岩、霞石正长岩、霓辉石正长岩、黑榴石正长岩和含霓石石英正长岩)和碱性花岗岩(钠闪石花岗岩、霓辉石钠闪石花岗岩)，还发育有大量的正长岩类二长岩类碱长花岗岩或晶洞钾长花岗岩。

Trioxide antinomy can be dissolved in the solution of sodium hydroxide and glycerin to produce sodium antimonite containing glycerin.

甘油、木糖醇等低C多元醇，在有碱参与的条件下能与三氧化二锑很好地发生反应，生成甘油亚锑酸钠、木糖醇亚锑酸钠，溶液在一定的碱浓度下可保持稳定。

Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.

采用"一勺烩"方法，以4-羟基苯甲腈为起始原料，首先与硫氢化钠和无水氯化镁在N，N-二甲基甲酰胺中反应，所得中间体不经分离，直接加入2-氯乙酰乙酸乙酯进行环合反应，得到2-(4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯（2）；然后通过六亚甲基四胺/三氟乙酸进行Duff反应，得到2-(3-甲酰基-4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯（3）；再经盐酸羟胺/甲酸/甲酸钠体系脱水得到目标化合物。

The model of adiabatic spherical to columnar hydrogen bubble growth in large leak sodium water reaction as well as the model of secondary loop pressure propagation with the one dimensional characteristic method are established under one double ended guillotine tube break in the steam generator of liquid metal cooled fast breeder reactor.

研究建立了钠冷快堆蒸汽发生器在单管束发生双端断裂情况下钠水反应中气泡从球形到柱状的变温绝热生长模型，及采用一维特征线方法建立的压力波在快堆二回路中的传播模型。模型中考虑了爆破膜、管壁弹性变形和气蚀的影响。

Cycloalkylation of diethyl malonate and ethyl cyanoacetate with alkyl halide was investigated in the presence of toluene.

以甲苯为溶剂及带水剂，用粉末K2CO3代替常规使用的乙醇钠，在季铵盐和聚乙二醇混合相转移催化剂的存在下，含有活泼氢的丙二酸二乙酯和氰乙酸乙酯与二卤代物进行缩合反应，得到相应的环化物。

RESULTS: All aromatic anesthetics inhibited I at a holding potential which produce half-maximal current V(1/2; inhibition was modest with 1,3,5-trifluorobenzene (8%+/- 2%), pentafluorobenzene (13%+/- 2%), and hexafluorobenzene (13%+/- 2%), but greater with benzene (37%+/- 2%), fluorobenzene (39%+/- 2%), 1,2-difluorobenzene (48%+/- 2%), 1,4-difluorobenzene (31 +/- 3%), and 1,2,4-trifluorobenzene (33%+/- 1%).

结果：在最高电流的一半的控制电压下所有芳香族麻醉药都阻断钠电流；均苯三酚（8%+/- 2%）、戊苯(13%+/- 2%)、戌苯(13%+/- 2%)的抑制是适度的比苯(37%+/- 2%)、氟苯(39%+/- 2%)，1.2-二氟二苯(48%+/- 2%)，1，4-二氟二苯(31 +/- 3%)，和1，2，4三氟苯(33%+/- 1%)明显。

Diethylene gly- col butylmethyl ether was synthesized through the Williamson reaction between butyl bro- mide (n-C_4 H_9 Br) and CH_3 OCH_2 CH_2OCH_2 CH_2 ONa.

通过正溴丁烷与二乙二醇单甲醚钠的Williamson反应合成了二乙二醇甲基丁基醚。

The synthetic technique of anionic surfactant sodium dodecyl diphenyl ether disulfonate was studied.The best reaction conditions were determined.Alkylation was carried out with n∶ n=5∶1 at 70 ℃ for 5 h to attain 82% yield.

研究了十二烷基二苯醚二磺酸钠阴离子表面活性剂的合成工艺，得出烷基化的最佳反应条件为：催化剂用量为n∶n =5∶1；反应时间 5h ；反应温度 70℃；二苯醚的转化率 82 %。

The premixing self-assembly solution of horseradish peroxide with poly(sodium 4-styrenesulfonate) is made by blending HRP and polyelectrolyte PSS,and the active.enzyme muhilayer biofilm is fabricated by altemate deposition of and PDDA on the surface of negative ionized PET.

以阳离子化的辣根过氧化物酶和阴离子聚苯乙烯磺酸钠的预混合溶液，与阳离子聚电解质聚二甲基二烯丙基氯化铵通过逐层组装，在阴离子化聚对苯二酸乙二酯表面构建了多层生物活性膜。

Shop assistant: Please check at the door.

店员：请您到门口柜台交费。

In the end, transportation of PAHs in the environmental matrix was preliminarily investigated and discussed according to PAHs data of soils and sediments from a certain region in Shanghai. The result indicated that there are two or more pathways on PAHs transportation in the environmental matrix.

最后，对上海特定地区内PAHs在环境介质中的迁移径途进行了分析讨论，结果表明上海市土壤和沉积物等环境介质中PAHs的迁移存在多种途径。