二金属的

A novel layout of IC transformer is proposed to achieve both high turn ratio and coupling coefficient in this paper. In order to discuss the coupling coefficient, the layouts are designed with different turn ratio. The thesis is mainly includes of three experiment topics. The multi-stack structure is proposed to achieve prior goal in first topic. Two groups of proposed devices are designed to maintain identical self- inductances in transformer's primary and secondary coils. Total six devices are fabricated in foundry 90-nm CMOS technology. Using the 9 and 5 metal layers in primary and secondary coils in a specific layout, measurement results show that the transformer has the largest benefit using the bottommost return layer in layout design. In one word, the adoption of more metal layers to construct different turn ratio transformer shows not only improving the N value but also saving the chip area in this experiment.

中文摘要本文是针对不同圈数比变压器探讨其耦合量的变化，并且期望其变压器能同时达到高圈数比及高耦合系数的特性，本论文主要可分为三个实验主题，首先第一个主题提出以90nm CMOS制程技术实现的多层金属层的布局方式，并以相同的一、二次侧自感值分为两组，利用不同返回层来达到不同的圈数比，且从量测结果可以得知，在变压器布局设计上使用最底金属层来作返回层会得到较好的特性，最后从此实验得知一结论，利用合适的多层金属架构达到不同的圈数比，不仅可以改善圈数比，还可以缩小晶片面积。

Aim To study the preparation conditions of the metal chelate gel with chitosan as support.

目的 研究利用壳聚糖为载体、戊二醛为交联剂、亚氨基二乙酸为螯合配基制备金属登合亲和吸附剂的条件。

The meshless analysis of the plastic forming processes is realized with the hypothesis of the rigid-plastic material,the velocity field simulated by the moving least square method and the essential boundary condition employed by the transformation method.

将无网格方法引入金属塑性成形过程分析，基于刚塑性材料假设，采用移动最小二乘法对速度场进行逼近，利用变换法施加本质边界条件，实现了金属塑性成形过程的无网格方法模拟。

Based on the problem of various types of catalyst and according to the features of carbonylation catalysts reactions, our team has been designed a series of new metal complexes of benimidazoles, which can be used for carbonylation catalyst of industry. Seven new benzimidazole derivatives were prepared by the o-phenylenediamine、oxalic acid、glycolic acid、monomethyl monopotassium malonate、ethyl cyanoacetate、succinic anhydride. The structures of them were confirmed by IR、Elemental analsis. The crystal structures of d and e were determined by X-ray single crystal diffraction of Germanic Bruker Smart APEX II CCD. The catalysis of them was tested by carbonylation reactions.

本文设计以邻苯二胺和草酸、羟基乙酸、丙二酸单甲酯、氰基乙酸乙酯、丁二酸单甲酯为原料采用PPA催化和无机酸催化法，合成了4种苯并咪唑-2-羧酸衍生物并进行了表征；培养了2个化合物d、e的晶体并测定和讨论了晶体结构；制备了3种未见报道的苯并咪唑金属配合物，对配合物在羰基化法制醋酐-醋酸反应的催化作用进行了初步试验。

The effects of reaction temperature, space velocity and the molar ratio of H2O2 to phenol on the concentration of diphenol product, the ratio of catechol to hydroquinone and reactive period of catalyst were investigated.

在连续全混反应器中，用含铁复合金属氧化物催化剂，研究了反应温度、空速、过氧化氢/苯酚对反应产物中苯二酚浓度、邻苯二酚/对苯二酚比例和催化剂的活性周期的影响。

Due to this, our goal is to develop a new method to functionalize implant surface by plasma treatment. Argon plasma removes all chemical traces such as adsorbed contaminates and impurities. Oxidation in oxygen plasmas by ion bombardment results in a dense oxide layer.

因此，本研究利用低温电浆来发展一植体表面处理技术，先以氩气电浆清洁钛金属表面，再以氧电浆让钛金属表面产生一层致密的二氧化钛层。

To assess the sensitivity of local species to toxic chemicals relative to those from other jurisdictions reported in the literature, ecotoxicological testing was also performed on three local marine species, Dunaliella salina, Brachionus plicatilis, and Lutjanus malabaricus, using 12 representative PPTSL chemicals including metals, pesticides (endosulfan, diazinon, permethrin, atrazine, tributyltin), and industrial chemicals (di-n-octyl phthalate, nonylphenol, acenaphthene).

为了评估与其他相关成文规定的当地有毒化学品种类，生态毒性测试也在三个地方的海洋物种上进行，杜氏盐藻，轮虫和红鳍笛石斑鱼，使用了十二种pptsl代表的化学元素，包括金属，杀虫剂（硫丹，二嗪磷，氯菊酯，莠去津，三丁基锡），和工业化学品（苯二甲酸二正辛酯，壬基酚，苊）。

In the thesis, a series of novel single and multi-armed oxadiazole bridging ligands and pyridyl-4, 5-imidazole dicarboxylic acid ligands have been synthesized. The coordination chemistry of these novel ligands with transition metal ions was investigated. In addition, two 1, 3, 4-oxadiazole bridging ligands end-capped by chelating Schiff-base coordination sites have been designed and synthesized. The coordination chemistry based on one of the two ligands with metal ions was primarily investigated.

本文报道了一系列新颖的含1， 3， 4-Oxadiazole杂环的单臂及多臂有机配体，研究了它们与过渡金属离子的配位反应化学；合成了吡啶基-4，5-咪唑二羧酸有机配体，研究了它们在水热条件下与过渡金属离子的配位反应化学；另外，还合成了1， 3， 4-Oxadiazloe杂环桥联的双Schiff-base有机配体，初步探讨了其与过渡金属离子的配位反应化学。

In this research, two novel compounds in which alkylenedithiomethylene Malonic acid act as the main coordination agents and the compounds containing N atom (such as pyridine, Phenanthroline Ethanediamine and 4,4'-Bipyridinyl) act as the associating coordination agents have been synthesized by the means of solution and solid-liquid diffusing reactions. 9 coordination complexes and polymers have been designed and synthesized in which the transition metals Cu and Zn acted as the centre ions. These compounds have been characterized by X-ray single crystal diffraction analysis, and some properties of them have been tested and analyzed.

本论文设计合成了两种结构新颖的含有二硫缩烯酮结构的丙二酸类化合物，以此为主要配体，以含氮化合物(吡啶、邻菲罗啉、乙二胺和4，4'-联吡啶)为辅助配体，采用常规溶液合成和固-液相扩散等方法，设计合成了9个过渡金属Cu和Zn离子配合物和配位聚合物，采用单晶X-射线衍射等技术对晶体结构表征，并对其部分性质进行了测试和分析。

In this thesis, nano-scale particles of metals, metal sulfides, selenides, oxides and nano-composites of metals/polymer, semiconductor sulfides/polymer have been successfully prepared by γ-ray irradiation technique in sorts of systems including water system, alcohol system, ethylenediamine system, microemulsion and emulsion system at room temperature and under ambient pressure. The possible formation mechanisms of nano-scale materials were suggested, and some factors of affecting the formation of nano-materials were studied.

本论文使用〓Co-γ射线辐射技术，在常温常压下分别于水体系、乙醇体系、乙二胺体系、微乳液和乳液体系中，成功地制备了纳米金属、硫化物、硒化物、氧化物以及金属／聚合物、半导体硫化物／聚合物纳米复合材料，并初步探讨了纳米材料形成的可能机理和影响因素。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。