二酸的

Biological activity of the compounds were studied and the result indicated that the compound 1,1'-ethyl dicarboxylate gem-dimethyl-cyclopropanediacylhydrazine has good activity against bean aphidsin at 250mg/L.

生物活性测定结果表明，在250mg/L的浓度下，化合物1，1'-二羧酸乙酯偕二甲基环丙烷双酰肼对蚕豆蚜虫有较好杀虫活性。

This is the first example of two-dimensional lanthanide MOFs with one dimensional water chains.2、Coordination polymer[Nd_2_3(H_2O)_2]·bpy·4H_2O(2)(bpdc=2, 2′-bipyridine-3,3′-dicarboxylate,bpy=4,4′-bipyridine)had been synthesized under hydrothermal conditions and its structures were determined by X-ray diffraction,and confirmed by IR and TG analysis.

该结构是在二维骨架的镧系配位聚合物中首次观察到的一维的水链结构。2、以Nd_2O_3，2，2′-联吡啶-3，3′-二羧酸和4，4′-联吡啶为原料，采用水热法合成了一个具有二维骨架结构的配位聚合物[Nd_2_3(H_2O)_2]bpy·4H_2O，通过IR、x射线单晶衍射分析和热重等手段对其结构进行了表征。

A method for determination of Secoisolariciresonol diglucoside, secoisolariciresinol, enterolactone and enterodiol in serum by LC/MS/MS was established. In this method,β-Glucuronidase was used to hydrolyze the serum samples, the electrospray ionization sourse and negative ion MRM scan were employed.

本实验用β葡萄糖醛酸苷酶酶解血清样品，采用电喷雾离子源，负离子MRM扫描，建立了血清中司可异罗叶松甘油二酯、司可异罗叶松酯素、肠内二醇、肠内脂的IC/MS/MS分析方法。

A high proportion of 1,3- dihydroxy units were also formed in the acid-catalyzed hydrolysis of poly, however, hydrolysis of GIE generated only a 2,3-dihydroxy product.

有很大比例的1，3 -二羟基单位也形成酸催化水解聚，然而，旅游局水解生成只有2，3 -二羟基产品。

Trifluoromethyl-3-heptadfluoroisopropyl-2-perfluoropentene-4-(N',N'-dimethylamino propyl) imino was prepared by the reaction of hexafluoropropene timer with N,N-dimethyl propanediamine in the molar ratio 1:1.0 at room temperature for 8h, and the structures of VIII were identified by IR and NMR spectra.

以六氟丙烯三聚体与N，N-二甲基丙二胺为原料合成叔胺2-三氟甲基-3-七氟异丙基-2-全氟戊烯-4-(N'，N'-二甲胺丙基)亚胺，利用红外光谱和核磁共振确定其结构，并通过对合成条件的考察得其最佳合成条件：乙醚为溶剂，碳酸钠为缚酸剂，摩尔投料比为1：1.0，在室温下反应8小时。

In this Ph. D. dissertation, reverse microemulsion method was fully used infabricating and modifying polyacrylamide with functional and high-relative moleculeweight. The copolymerization of 2-acrylamide-2-methylpxopanesulfonic acid, fluorescent monomer 4-methoxy-N-(2-N\', N\'-dimethylamino ethyl)naphthalimide alkyl chloride quaternary ammonium salt, fluorescentmonomer 4-(N\'-methyl-1-piperazinylallyl)-N-butyl-naphthalimide chloride quaternaryammonium salt, Cationic monomer dimethylethylammonium bromide and hydrophobical monomer octadecylacrylate with acrylamide and properties of the copolymers werestudied. The interaction between five polymers and Al_2O_3(012) crystal surface have beensimulated by Materials Studio 3.0 program package, binding energies and non-bondinteraction energies and deformation energies have also been acquired.

本文以制备具有较高相对分子质量和功能型PAM为研究目的，将反相微乳液法运用到其制备及改性的有关环节，通过反相微乳液聚合工艺，将几种改性功能单体2-丙烯酰胺基-2-甲基-丙磺酸、荧光单体2-(4-甲氧基-1，8-萘二甲酰亚胺基)-乙基二甲基烯丙基氯化铵、荧光单体4-(N'-甲基-1-哌嗪基)-N-丁基-1，8-萘烯丙氯季铵盐、阳离子单体丙烯酰氧乙基-二甲基-乙基溴化铵和疏水单体丙烯酸十八酯与AM共聚，制备AMPS改性PAM、荧光示踪型PAM、阳离子单体DMB改性PAM和OA改性PAM等四类不同功能单体改性PAM，并研究其应用性能。

The castor oil based polyurethane potting materials were synthesized from castor oil,4,4 diphenylmethane diisocyanate,trimethylolpropane and 1,2 propanediol.

以蓖麻油，4，4' -二苯基甲烷二异氰酸酯、三羟甲基丙烷与 1，2 -丙二醇为原料合成了蓖麻油基聚氨酯灌封胶，研究了灌封胶的固化流变行为和凝胶化时间。

The recent advances in the main clean processes to synthesize diphenylmethane diisocyanates are reviewed, such as BTC method, condensation of aniline, reductive carbonylation of nitrobenzene, oxidative carbonylation of aniline, methoxycarbonylation of aniline, alcoholysis of N,N'-diphenyl urea and the coupling process.

回顾了清洁合成二苯甲烷二异氰酸酯的几种主要方法，如BTC法、苯胺缩和法、硝基苯还原羰基化法、苯胺氧化羰基化法、碳酸酯法、二苯基脲法和反应耦合法等合成路线。

As can be seen in Fig. 5, dipropyl ether will be recovered in the distillate using 1-pentanol, N,N-dimethylformamide and 2-ethoxyethanol as entrainers and butyl propionate is the only entrainer studied that inverts the volatility of the azeotropic mixture.

从图 5可以看出，使用1-戊醇、N，N-二甲基甲酰胺和2-乙氧基乙醇作为共溶剂时二丙醚将在馏分中回收，丙酸丁酯是唯一与共沸混合物挥发性相反的共溶剂。

The extracted components were qualitatively and quantitatively analyzed by gas chromatography mass spectrometry.The results showed that 30,26 compounds were identified from the volatile components extracted by DSE,SDE methods resp.36 kinds of components were extracted by 2 methods in total,among them the content of hexadecanoic aci...

结果表明，从DSE、SDE法提取的挥发性成分中分别鉴定出30(总含量58.24μg/g)、26种化合物总含量(86.66μg/g，2种方法共提取出36种化合物，其中十六酸含量最高，其次为亚油酸、油酸、邻苯二甲酸二异丁酯、间甲苯甲醛、龙脑。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。