二酸的

Similar to S-adenosylmethionine decarboxylase(B26),S-adenosylmethionine methyl-transferase(B70), allene oxide synthase(B38),ethylene receptor(B96),cytochrome P450(B58) and methionine synthase (B77) were found in ovaries of Pingyi Tiancha at 1d before the blossom day,which related to plant hormone and could participate in metabolic pathways of ethylene,polyamine,jasmonate acid and gibberellin,et al.,as well as had close relationship with maturity and senescence of plants.

在平邑甜茶开花前1d的子房中发现的S-腺苷甲硫氨酸脱羧酶(B26)、S-腺苷甲硫氨酸甲基转移酶(B70)、丙二烯氧化合酶(B38)、乙烯受体(B96)、细胞色素P450酶(B58)、甲硫氨酸合酶(B77)等相似基因片段与植物体内的生长素有关，将会参与乙烯、多胺、茉莉酸、赤霉素等的代谢途径，与植物的成熟和衰老具有密切的关系。

New ruthenium benzylidene complexes benzylidene[1,3-bis(2,6-dimethylphenyl)-4,5-dihydroimidazol-2-ylidene] [k~2-diphenylphosphinoacetato] monochlororuthenium (46), benzylidene[1,3-bis(2,6-dimethylphenyl)-4,5-dihydroimidazol-2-ylidene][k~2-3-propionato]monochlororuthenium (47), benzylidene[1,3-bis(2,6-dimethylphenyl)-4,5-dihydroimidazol-2-ylidene] [k~2-2-benzonato]monochlororuthenium (48) featured five-membered, flexible six-membered and rigidsix-membered chelating rings respectively are prepared by reactions of complex 41 withcorresponding sodium phosphino-carboxylates. It is confirmed by X-ray crystallographicanalysis that the coordination geometries of complexes 46 and 47 are distorted squarepyramids with phosphino-carboxylate ligands chelating to ruthenium, and the coordinationbetween ruthenium and benzylidene ligands are strengthened.

用二苯基瞵乙酸盐、二苯基膦丙酸盐、二苯基膦苯甲酸盐与钌卡宾配合物41反应合成了三个新的钌卡宾配合物：含五元膦-氧螯合环的1，3-二-(2，6-二甲苯基)-4，5-二氢咪唑基1-苯亚甲基--一氯合钌(46)、含六元柔性膦-氧螯合环的[1，3-二-(2，6-二甲苯基)-4，5-二氢咪唑基1-苯亚甲基--一氯合钌(47)及含六元刚性膦-氧螯合环的[1，3-二-(2，6-二甲苯基)-4，5-二氢咪唑基]-苯亚甲基--一氯合钌(48)。X射线单晶衍射分析证明，配合物46、47都为变形的四方锥构型，膦-氧与钌形成螯合配位，其中苯亚甲基与钌的配位得以加强。

Metabolites, including 1 phenolic diterpene, 2 phenolic acids (rosmarinic acid and caffeic acid), 2 flavonoids (6-methoxyluteolin-7-glucoside and homoplantaginin) and 1 coumaric acid ( cis-4-glucosyloxycinnamic acid), were successfully identified from two rosemary extracts with chloroform-methanol ( v / v , 3/1) and 50% aqueous methanol on the basis of HPLC, UV, NMR and MS data.

基于高效液相色谱、紫外吸收、核磁共振波谱及质谱数据，具有代表性的6个迷迭香代谢物的结构得到了确定，它们分别为1个酚类二萜、2个酚酸、2个黄酮（6-甲氧基木樨草素-7-葡萄糖苷和高车前甙）和1个香豆酸(顺-4-香豆酸葡萄糖苷)。

A method for the preparation of microcellular elastomeric polyurethane foams from a reaction mixture comprising a polyisocyanate component containing at least 85% by weight of 4,4'-diphenylmethane diisocyanate or a variant thereof, a polyol composition comprising at least one polyoxyalkylene polyol having an average nominal hydroxyl functionality of from 2 to 6, an average hydroxyl equivalent weight of at least 1300 and an average oxyethylene content of between 50 and 85% by weight, water, a chain extender having an average hydroxyl equivalent weight of from 15 to 250 and optionally a crosslinking agent, the hardblock-content being more than 45% by weight.

本发明是有关一种制备微孔弹性聚氨基甲酸酯泡沫体的方法，其反应混合物包括：一种含至少85重量％的4，4′－二苯甲烷二异氰酸酯或其变体的聚异氰酸酯组分，一种多元醇组合物，其包含至少一种平均标称羟基官能度从2至6、平均羟基当量至少1300且平均氧乙烯含量介于50至85重量％之间的聚氧亚烷基多元醇，水，一种平均羟基当量为15至250之增链剂，以及视需要使用的交联剂，该硬性嵌段－含量（hardblock-content）大于45重量％。

A modified analysis method based on the determination of ozone—indigo disulphonate spectrophotometer(GB/T 15437-1995) in gas phase has been developed to detect the concentration of ozone in liquid phase. An analytical condition of λmax=612～615 nm,ε=20 000 L/, pH 2 is obtained by the titration of indigo disulphonate. Compared with potassium iodide method,it shows a higher precision and accuracy,CV＜3.0%. The results also prove that blank experiment will bring about 5.0%systematic error.

在气相臭氧浓度的靛蓝二磺酸钠分光光度法(GB/T15437-1995)基础上提出了液相臭氧浓度的测定方法，采用靛蓝二磺酸钠标准曲线法代替采用易分解的臭氧标准曲线法，得出测定条件λmax=612～615 nm、ε=20 000 L/、pH为2，通过碘量法比较实验，说明新的测定方法具有较高的精度和准确度，相对标准偏差小于3.0%；比较结果表明忽略空白实验将引入5.0%的系统误差。

In this paper, the glyoxal structure both in reagent and in bulking solution were detected by infrared spectro and mass spectra, the result shows that there is no aldehyde group but only hydrate existing in both solutions. Besides, the mechanism of the ac-tion between glyoxal and waterlogged wood is discussed and some problems like how to prevent the bulk-ing solution from acidification are also mentioned.

此外，还运用红外光谱和质谱法测定了试剂乙二醛和加固液的结构，详细讨论了乙二酯在试剂和加固液中官能团的存在形式和聚合状态的细微变化，指出在二种溶液中并不存在醛基，乙二醛仅以水合物的形式存在并讨论了乙二醛与饱水古木的作用机理，提出用醇溶液能有效控制乙二醛使用中易返酸等问题。

Both three-dimensional chiral compounds have intriguing chiral channels, which are built up of homochiral intertwined double helices. The circular dichroism spectra of 1 and 2 in water have shown they are stable in solution, which document they will be significantly useful in asymmetric catalysis and chiral medicine.

以Keggin结构多金属氧酸盐为建筑单元，通过手性的铜-脯氨酸配合物作为模板剂构筑了2个基于Keggin结构多金属氧酸盐的3D纯手性化合物，化合物1和2是一对对映体，代表了世界上第一例3D手性多酸化合物，具有由同手性螺旋缠绕形成的手性孔道，水溶液中的圆二色谱表征这个3D手性化合物可稳定存在，显示这个物种可以在不对称催化及手性药物方面有潜在的巨大的应用价值。

Based on the results of 1H-NMR, 13C-NMR, ESI-MS and UV spectra, the structures of three compounds with antitumor activity were identified as Prodigiosin、7-Hexadecenoic acid、7,10-Octadecadienoic acid, respectively; another compounds (no activity to above tumor cells)was identified as Myristic acid.

运用核磁共振（1H-NMR、13C-NMR）、质谱、紫外光谱等现代波谱技术分析，将其中3种具有抗肿瘤活性的化合物分别鉴定为灵菌红素、7-十六碳烯酸（7-Hexadecenoic acid）、7，10-十八碳二烯酸（7，10-Octadecadienoic acid）；鉴定另一种对上述肿瘤细胞无活性的化合物为肉豆蔻酸。

In this paper, 4-4-(trifluoromethoxy benzoyl cyclohexyl-3, 5-diaminobenzoate with a large branch chain, pyromellitic dianhydride and 4-(4-aminobenzyl) benzenamine were used to synthesize polyimides. The effect of monomer charge order on pretilt angle was investigated for the first time when PIs were used as LC alignment layer, and the effect of diamine mole ratio on pretilt angle was studied. The thermal stability of the pretilt angle was discussed.

文章用均苯四酸二酐、4，4'-二胺基二苯甲烷和具有较大支链的4-（4-苯甲酰基）环己基－3，5-二胺基苯甲酸酯等单体制备聚酰亚胺，首次研究了单体加料顺序对液晶预倾角的影响，同时也研究了二胺配比对液晶预倾角的影响问题，并探讨了预倾角的热稳定性等问题。

It is concluded that the infrared photodissociation spectroscopy of protonated serine clusters H+n, n = 2 8, provides evidence for a size-dependent transition from neutral to zwitterionic network structures.

第四章的结论中提到由此一系列由二至八的丝胺酸团簇红外吸收光谱结果，我们观察到从二聚体的中性丝胺酸单位到八聚体的两性离子单位，中间经历了结构转换的过程。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新