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Main production sulfide Green, Chloropicrin, picric acid, dinitro-chlorobenzene, potassium chlorate, high sodium chlorate, ammonium perchlorate, such as more than 30 kinds of products, exports of Asia and Europe more than 30 countries and regions. In 2000 through ISO9002 quality system certification, production scale, cost-effective, enterprise management, technological advancement, product quality, environmental protection are rising, has very broad prospects for development.

主要生产硫化青、氯化苦、苦味酸、二硝基氯化苯、氯酸钾、高氯酸钠、高氯酸铵等30多种产品,出口亚欧30多个国家和地区。2000年通过ISO9002质量体系认证,生产规模、经济效益、企业管理、技术进步、产品质量、环境保护均不断提升,具有十分广阔的发展前景。

The process is carried out by taking organic acid and sulfoxide chloride as raw materials, acyl chloride synthesizing, reacting ethylenediamine with sodium chloroacetate to synthesize intermediate sodium EDDA, and reacting it with acyl chloride to synthesize the final product.

所述双子烷基羧酸盐表面活性剂是由以下方法制得的,以有机酸和氯化亚砜为原料首先进行酰氯的合成,再用乙二胺与氯乙酸钠反应合成中间体乙二胺二乙酸钠,将中间体乙二胺二乙酸钠与酰氯反应合成终产物。

ABSTRACT Immobilized penicillin acylase (from E.coli) was used to catalyze 7 phenylacetamido 3 E propenyl cephalosporanic acid hydrolyzation into 7 amino 3 E propenyl cephalosporanic acid. Then, trans APRA was acylated with hydroxyethyl ester of 4 hydroxy D phenylglycine to obtain trans cefprozil.

以7 苯乙酰氨基 3 E 丙烯基 3 头孢菌素 4 羧酸为原料,在青霉素酰化酶作用下,首先酶法水解得到3 E 丙烯基 3 头孢菌素 4 羧酸,过滤固相酶,滤液调pH分离得到反式APRA固体;在青霉素酰化酶作用下,反式APRA再与对羟基苯甘氨酸乙二醇酯缩合,得到反式头孢丙烯;酶法合成所得的产品与进口反式头孢丙烯对照品一致。

The effect of the ultraviolet-visible light transmittance,doping amount of thorium dioxide and neodymium sesquioxide,pH value of the aqueous solution of sodium dodecyl benzenesulfonate and some other factors on the ph.

以玻璃珠为载体,用溶胶-凝胶法制备二氧化钍和三氧化二钕复合二氧化钛膜对水溶液中的十二烷基苯磺酸钠进行了固定相光催化氧化实验。

Seven compounds have been isolated from hard coral Acropora pulchra. These compounds are:pentadecoic acid, heptadecyl ester;(2)n-cetanol;(3)batyl alcohol;(4) N- [ 1 --2-hydroxyl--3,7-heptad-ecadienal] -hexadecanamide;(5)1 -0-hexanoyl-glycerol ester;(6)thymine;(7)uracil. Their structures were determined by IR, MS, HNMR, 13CNMR analysis.

从北海佳丽鹿角珊瑚Acropora pulchra乙醇提取液的乙酸乙酯部分分离出七个化合物,经IR、MS、~1HNMR、~(13)CNMR等波谱方法鉴定,其结构分别为:(1)十五酸十七酯,(2)正十六碳醇,(3)鲨肝醇,(4)N-1-羟基甲基-2-羟基—-3,7-十七碳二烯基十六酸酰胺,(5)1-正十六酸甘油酯,(6)胸腺嘧啶,(7)尿嘧啶。

The method is simple, rapid, and accurate, and is suitable for the determination of melamine, ammeline, ammelide, and cyacuric acid in milk and milk powder.

该方法简便、快速、准确,可满足牛奶及奶粉中三聚氰胺、三聚氰酸、三聚氰酸一酰胺、三聚氰酸二酰胺测定的需要。

A HILIC-MS/MS method was developed to determine melamine and its three derivatives, cyanuric acid, ammelide and ammeline in milk and milk powder. The milk sample was directly extracted by acetonitrile with the help of ultrasonic, and milk powder was resolved in water before extraction by acetonitrile.

建立了牛奶和奶粉中三聚氰胺及其3种衍生物(三聚氰酸、三聚氰酸一酰胺、三聚氰酸二酰胺)的亲水色谱-串联质谱检测方法(HILIC-MS/MS)。

After centrifugation, the extracts were separated on HILIC column by using acetonitrile-water as mobile phase. The analytes were identified and quantitated by LC-tandem MS under the positive/negative electrospray ionization and multiple reaction monitormode. The calibration curves showed good linearity in the range of 25-5000 μg/kg for melamine and cyanuric acid, and 50-10000 μg/kg for ammeline and ammelide. The limits of detection and limits of quantification were in the range of 5-20 μg/kg and 50-100 μg/kg, respectively.

牛奶样品直接用乙腈超声波提取;奶粉样品先用水溶解后再加乙腈超声波提取,高速离心后以乙腈-水为流动相,采用亲水作用色谱柱分离这4种化合物,在电喷雾正、负电离切换多反应监测模式下进行定性与定量分析,三聚氰酸一酰胺与三聚氰酸二酰胺含量在50~10000μg/kg之间、三聚氰胺与三聚氰酸在25~5000μg/kg之间,均获得良好的线性。

A novel liquid crystalline compound named p-phenylenediamine di 4-[2- benzamide] was synthesized from allyl 2-hydroxyethylether, ethyl 4-hydroxybenzoate and p-phenylenediamine.

以乙二醇单烯丙基醚、对羟基苯甲酸乙酯、对苯二胺为原料合成了末端为不饱和双键的芳香聚酰胺溶致型液晶化合物——二对烯丙氧基乙氧基苯甲酰对苯二胺,最佳合成的摩尔比为∶羧酸∶对苯二胺∶吡啶=2。

Discussion Diphenylacetic acid can be prepared by the reduction of benzilic acid with hydriodic acid and red phosphorus,1 by carbonation of the reaction product of phenylsodium and diphenylmethane,2 and by hydrolysis of 1,1-dichloro-2,2-diphenylethylene.3

讨论 Diphenylacetic酸可编写的减少benzilic酸hydriodic酸和红磷, 1碳化反应产物phenylsodium和二苯基甲烷,第2和水解1,1 -二氯- 2 ,2 - diphenylethylene 0.3

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