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A phospho molybdic acid catalyst was investigated for the esterification of fumaric acid with methanol in this paper.

研究了以磷钼酸为催化剂,富马酸和甲醇为原料合成富马酸二甲酯,探讨了酸醇量比、反应时间、催化剂用量等工艺参数对 DMF收率的影响。

As an intermediate for preparing vanillin derived from glyoxylic acid, 3, 4-dihydroxymandelic acid is synthesized based on condensation of catechol and glyoxylic acid in alkaline aqueous solution.

以邻苯二酚和乙醛酸为原料,在碱性条件下发生缩合反应,合成了3, 4-二羟基扁桃酸,此物质是多种香料和药物合成的重要中间体。

The preparation method comprises the steps as follows: houghite ZnAl-NO3-LDHs is taken as the precursor, ion exchange method is adopted to insert the 2- naphthylamine-1, 5-disulfonic acid to the interlayer of ZnAl-NO3-LDHs, thereby assembling and acquiring the ZnAl-NADA-LDHs of good crystalling phase structure and splendid performance.

超分子结构2-萘胺-1,5-二磺酸插层材料,简写为ZnAl-NADA-LDHs,其分子式为:[Zn 2 1-x Al 3 x 2 ](C 10 H 7 NO 6 S 2 ) 2- x/2 mH 2 O,是以水滑石ZnAl-NO 3 -LDHs为前体,采用离子交换法将2-萘胺-1,5-二磺酸插入到ZnAl-NO 3 -LDHs层间,组装得到晶相结构良好、性能优异的ZnAl-NADA-LDHs。

The methods of synthesizing polyurethane (Toluene, 2, 4-diisocyanate TDI and Isophorone diisocyanate IPDI) with paper were investigated.

研究了甲苯-2,4二异氰酸酯,异佛尔酮二异氰酸酯对纸张聚氨酯化处理的方法及反应机理。

A reversed-phase high performance liquid chromatographic method was established for determination of isothiocyanates in human urine , which used the reaction of propyl isothiocyanate with 1,2-benzenedithiol as reference instead of the synthesis of 1,3-benzodithiole-2-thione.

省去合成1,3 苯二硫杂环五烯 2 硫酮这一步骤,直接用异硫氰酸丙基酯与1,2 苯二硫酚反应作标准,建立了尿液中异硫氰酸酯的反相高效液相色谱测定方法。

The result of analysis by GC-MS was shown that fatty acid constituents of oat oil were myristic, palmitic, stearic, oleic, linoleic, linolenic and eicosenoic acids.

通过GC-MS分析,燕麦油的主要成分有豆蔻酸、棕榈酸、硬脂酸、油酸、亚油酸、亚麻酸、二十碳一烯酸。

Results13 compounds were identified, which accounted for 100 % of the essential oil of the skins of stem. The major compositions were n-Hexadecanoic acid (46.13%); Octadecanoic acid (15.44%),-9-Octadecenoic acid (13.73%), and-9,12-Octadecadienoic acid (7.79%).

结果通过计算机检索、图谱分析法鉴定出13种化合物,占总油量的100%,其主要成分为正十六烷酸(46.13 %)、十八烯酸(15.44 %)、-9-十八烯酸(13.73 %)及-9,12-十八碳二烯酸(7.79 %)。

Effects of the mass ratio of organic phosphonic acid to zinc biphosphate, compound system amount, corrosion time and temperature, and pH value on the anticorrosive efficiency were investigated.

以四乙烯五胺、甲醛和亚磷酸为原料合成了有机膦酸类缓蚀剂,与磷酸二氢锌复配,考察了有机膦酸类缓蚀剂与磷酸二氢锌质量比、复配体系加量、腐蚀时间、腐蚀温度及体系pH值对复配体系缓蚀效果的影响。

The results showed:the fatty acid composi- tion of crude fish oil and refined fish oil of Rachycentron canadum Linnaeus muscle have not the obvious change,mainly the 18 kinds of fatty acids of C_(14)~C_(22);the content of unsaturated fatty acid was 44.31% and 48.53% respectively;the total content of eicosapentaenoic acid and doconsahexaenoic acid...

结果表明:军曹鱼鱼肉粗鱼油和精制鱼油脂肪酸组成没有明显变化,主要由C14~C22的18种脂肪酸组成,不饱和脂肪酸含量分别为44.31%、48.53%;二十碳五稀酸和二十二碳六稀酸总量分别为13.67%、14.88%;酶解蛋白粉粗蛋白含量为95.77%,脂肪含量0.32%,灰分5.45%,具有高蛋白、低脂肪、矿物元素丰富的特点;必需氨基酸占氨基酸总量的41.58%,必需氨基酸之间比例适宜,符合FAO/WHO推荐的理想蛋白质模式。

Methods This study contained a total of 16 culture groups, including one group as control and 5 groups treated by 5 drugs (calcium L-threonate, sodium L-threonate, alendronate, 17β-estradiol and calcium gluconate) each at the final concentrations of 10^(-9)mol/L, 10^(-7)mol/L, 10^(-5)mo1/L respectively. After 7 days, eight bone slices of every group were stained with toluidine blue and the areas of resorptive pits were analyzed under light microscope; the concentrations of C-telopeptide of type Ⅰ collagen CT(subscript x or Crosslaps in culture supernatants were measured by ELISA.

制备骨磨片,培养OC,并分别加入高中低浓度10^(-5、10^(-7)、10^(-9)mol/L的L-苏糖酸钙、L-苏糖酸钠、阿仑麟酸钠、17β-雌二醇、葡萄糖酸钙,实验设以上各浓度组及对照组(共16组,每组n=8),甲苯胺蓝染色一光镜观察分析骨片上骨吸收陷窝面积,ELISA测定上清液Ⅰ型胶原C-末端肽(CTx或Crosslaps)浓度。

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