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At first, Polyaniline was synthesized by the improved chemical oxidation technique, then, PANI/HCl, PANI/TSA and PANI/DBSA were obtained by doping emeraldine with HCl, 4-methyl benzene sulfonic acid and dodecylbenzene sulfonate acid, separately. Leucoemeraldine was obtained in the N-dimethylformamide by using phenylhydrazine deoxidizing emeraldine in N_2 atmosphere.

本文首先通过改进合成条件的化学氧化法合成了聚苯胺,经氨水脱掺杂获得本征态聚苯胺,再经盐酸、对甲苯磺酸、和十二烷基苯磺酸掺杂,分别获得到质子酸掺杂的聚苯胺样品,然后在N,N-二甲基甲酰胺中,利用苯肼,在N_2氛围下还原本征态聚苯胺得到还原态的聚苯胺。

All the complex series based on 4',4''-dicarboxy-1,6-diphenoxyhex- ane (C6-2COOH) and 4',4''-dicarboxy-1,10-diphenoxydecane (C10-2COOH) possessed higher melting and clearing points, usually showed soft crystal or crystalline smectic phases and crystal polymorphs except C10-2COOH/ p -PhBPy complex displaying also an enantiotropic nematic phase, while the complexes based on 4,4'-dicarboxy-α,ω-diphenoxy tetraethyleneglycol ether (C8O4-2COOH) with a longer flexible spacer exhibited monotropic fluidic smectic SmA and/or nematic phases.

研究表明,分别具有较短的6或10个亚甲基的烷烃间隔基的双苯甲酸衍生物4',4''-二羧酸-1,6-二酚氧基己烷(C6-2COOH)和4',4''-二羧酸-1,10-二酚氧基癸烷(C10-2COOH)的系列复合物具有较高的熔点和清亮点,一般都只出现结晶近晶相和多晶型转变现象。

The effects of ultrasonication and HF washing on SiC nano-particles were analyzed by Zeta potential, particle size distribution and SEM. The stability of suspension of SiC in ethanol, ethanediol and mixture of the two medias with PEG as dispersant at different pH were compared. The optimum ultrasonication time for SiC nano-particles was obtained. The influence of HF washing on SiC nano-particles was discussed; and high stability of SiC nano-particles suspension was achieved at pH=10 in ethanediol with 1wt% PEG as dispersant.

本文中采用Zeta电位、粒度分析、SEM等测试技术分析了超声震荡和HF酸洗对SiC纳米粉体的影响:对比研究了乙醇、乙二醇以及75%乙醇和25%乙二醇混合液作为分散介质,聚乙二醇为分散剂时纳米SiC粉体在不同pH下的分散稳定性,确定了粉体最佳超声震荡的最佳时间;探讨了酸洗的作用;并在乙二醇中,以1% PEG为分散剂,pH=10条件下获得了纳米碳化硅粉体的高稳定分散悬浮液。

To observe the effects of EPA and DHA on the proliferation and apoptosis of glomerular mesangial cells induced by lipopolysaccharide.

目的 观察二十碳五烯酸和二十二碳六烯酸对正常及在脂多糖诱导下的肾小球系膜细胞增殖和凋亡的影响。

The nautre of ester bond and sedimentary medium condition control the distribution pattern of organic acid ester in strong reductional environment and water-washed oxidized crude oils. The former features higher contents both of 9, 11-Octadecadienoic acid, methyl ester and Hexadecanoic acid, showing the non-reversible hydrolysis reaction of ester bond in condition of basicity; the later features higher contents of Hexadecanoic acid and Octadeanoic acid, and lower contents of nonsaturated and side-chain acid ester, indicating the reversible hydrolysis reaction of ester bond in acid condition.

酯键的化学性质和沉积环境中介质条件,决定了强还原咸水盐湖相和淡水湖沼相经水洗氧化次生变化的原油有机酸酯的分布特征,前者9,11-十八二烯酸甲酯与正十六烷酸为主,反映酯键在碱性条件的不可逆水解过程,后者以正十六烷酸和正十八烷酸为主,烯酸和支链酸很少,反映酯键的酸性条件的可逆性水解,烯酸经氧化向正十八烷酸,正十六烷酸转化。

Prophenoloxidase is a key enzyme for mediating melanotic encapsulation of oocysts,which may be transformed into active phenoloxidase by limiting proteolysis.

而前酚氧化酶(Prophenoloxidase,PPO)是介导卵囊黑化包被反应的一种关键酶,活化后可催化酪氨酸羟基化为二羟基苯基丙氨酸,二羟基苯基丙氨酸和多巴胺可进一步氧化为具有活性的苯醌活性,苯醌即可介导蛋白交联并聚合成黑色素层固定、隔离或杀死入侵的病原体。

The method comprises the steps that the molybdenum bearing spent catalyst is roasted and comminuted, then the molybdenum bearing spent catalyst is leach and filter by adopting alkaline solution bearing ammonia, ammonium bicarbonate and oxyful, and the secondary roasting and leaching are performed to the solids after filtration, the twice leaching solution is acidified and the aluminum is precipitated out, then is acidified continuously to precipitate out the molybdenum in the form of molybdic acid, the molybdic acid is dissolved by using ammonia water further, the pH value is adjusted again to obtain ammonium molybdate deposition, and the ammonium molybdate product is obtained after dryness.

将含钼废催化剂进行焙烧、粉碎,然后采用含氨、碳酸氢铵和双氧水的碱性溶液浸取并过滤,过滤后的固体物进行二次焙烧和浸取,两次浸取液酸化沉淀出铝,然后继续酸化将钼以钼酸形式沉淀出来,钼酸进一步用氨水溶解,再次调节pH值获得钼酸铵沉淀,干燥后得到钼酸铵产品。

A series of newl naphthalenic sulfonated polyimides were synthesized using 1,4,5,8-naphthalenetetracarboxylic dianhydride, 2,2'-benzidinedisulfonic acid by one-step high temperature polymerization method. The sulfonated degree of SPI-X membranes was controlled through adjusting the molar ratio of BDSA to the non-sulfonated diamines.

采用1,4,5,8-萘四酸二酐、2,2′-联苯二胺双磺酸和APBA为单体,通过高温一步聚合法合成了含有噁唑环的新型磺化聚酰亚胺,通过调节二胺单体的比例控制磺化程度。

Polyethylene glycol ethers of alkyl alcohols having the general formula CH3(CH2)xCH2(OCH2CH2)nOH wherein x is 8 to 20 (of which ceteareth-20, steareth-20 and steareth-100 are preferred), poloxamer 185, poloxamer 407, N,N-dimethyl dodecylamine N-oxide, and mixtures thereof, are employed to increase follicular delivery and/or follicular residence time of certain water soluble ornithine decarboxylase inhibitors of which 2-2,5-diamino pentanoic acid and its pharmaceutically acceptable salts, hydrates, optical enantiomers and racemic mixture are preferred.

使用通式为CH3(CH2)xCH2(OCH2CH2)nOH的烷基醇的聚乙二醇醚,其中x为8-20(其中鲸蜡硬脂醇醚-20、硬脂醇醚-20和硬脂醇醚-100是优选的)、poloxamer 185、poloxamer 407、N,N-二甲基十二烷胺N-氧化物及其混合物来提高某些水溶性的鸟氨酸脱羧酶抑制剂的毛囊传输和/或毛囊停留时间,优选的抑制剂是2--2,5-二氨基戊酸及其药学上可接受的盐、水合物、光学对映异构体及外消旋混合物。

Pyromellitic dianhydride and Sodium tetrazodiphenyl-naphthionate, 1,4-diaminoanthraquinone and Benzoguanamine as aromatic diamines were selected to be polymerized under microwave irradiation.

本论文选用均苯四酸二酐和刚果红、1,4—二氨基蒽醌、苯代三聚氰胺三种芳香族二胺作为单体,采用微波辐射的方法合成了具有非线性光学性能的聚酰胺酸和聚酰亚胺。

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