二酸的

Therelationship of the amount of catalyst and the ee% of product was seen to be negative nonlin-ear. Catalyst 3 was used in the enantioselective addition of diethylzinc to aromatic aldehydesand gave good results. The configuration of products was determined by the configuration ofthe catalysts' chiral carbon linked with hydroxy group. Using β- amino alcohols bearing only one chiral center as catalysts for the enantiose-lective addition were studied. D-N, N-dialkyl-2-amino butanol gave poor catalytic effect be-cause of their structure. The configuration of the product is the same as the catalyst. Anotherkind of β- amino alcohols - phenylglycine derivatives and valine derivatives have chiralcenter on the carbon linked with amino group. Catalyzed by-phenylglycine derivatives 6,7, 9, 10, the reactions gave satisfied results. The optical yields exceeded 80%.

在探讨了含有两个手性中心的β-氨基醇之后，选择了只有一个手性中心的β-氨基醇，一是手性中心为连羟基的手性碳原子：D-N，N-二烷基-2-氨基丁醇；二是手性中心为连氨基的手性碳原子：D-苯基甘氨酸衍生物和L-缬氨酸衍生物。D-2-氨基丁醇的催化效果不太好，这与其结构的空间位阻较小有关系，反应产物与连羟基手性碳构型一致；由苯基甘氨酸和缬氨酸出发合成五种β-氨基醇6-10，研究了不同ee％的-6作用下的二乙基锌-苯甲醛加成反应，发现该催化剂具有不对称放大效应；-7，9，lO的催化效果也比较令人满意，光学产率80％以上，所得产物构型与催化剂构型一致。

Sulfonated poly are prepared by direct polymerization of biphenol A, disodium 4, 4"-difluoro-3, 3"-disulfonate-1, 1-diphenylketone and 2, 6-difluorobezonitrile. The polymers are characterized with ~1H-NMR, FT-IR.

以双酚A，2，6-二氟苯腈和4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯酮采用直接缩合法合成了不同磺化度的磺酸型聚芳醚腈酮，通过FT-IR和~1H-NMR对聚合物进行了表征，证明其结构正确。

Sulfonated poly are prepared by direct polymerization of biphenol A, disodium 4, 4"-difluoro-3, 3"-disulfonate-1, 1-diphenylsulfone and 1, 3-(4-difluorophenyl)benzene. The polymers are characterized with ~1H-NMR, FT-IR.

以双酚A，1，3-二(4-氟苯基)苯和4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯砜采用直接缩合法合成了不同磺化度的磺酸型聚芳醚酮砜，通过FT-IR和~1H-NMR对聚合物进行了表征，证明其结构正确。

We devote in the research, development, production and marketing of precious metal compound and related products with reliable quality, such as; potassium gold noncyanide, Rhodium sulphate, potassium tetrabroaurate, Chloroplatinic acid, gold chloride, Ammonium chloropalladate, Ammonium tetrachloropalladate, recycled and refined precious metals etc.

公司主要从事贵金属材料相关产品的研究、开发、生产和销售，主要产品有无氰金盐和其他贵金属化合物，包括：硫酸铑、溴金酸钾、氯铂酸、三氯化金、二氯化二氨络钯、二氯化四氨络钯等，并提供贵金属资源二次回收服务。

Is a research and development, production, trade and service-based economy of foreign trade entities, chemical raw materials to the professional operation of the main company's existing production of AC blowing agent, ferric chloride, hydrated Hydrazine, p-nitrophenol, m-phenylenediamine, phosphorus trichloride, phosphorus oxychloride, 2,4 - diamino benzene sulfonate, sodium dichloro isocyanurate, N-methyl-o-phenylenediamine Second hydrochloride fine chemical products such as the ability, and are obtained ISO9001 international quality system certification.

济南华尔沃进出口贸易有限公司是一家集研发、生产、贸易、服务于一体的外贸型经济实体，以专业经营化工原料为主，公司现有生产AC发泡剂、三氯化铁、水合肼、对硝基苯酚、间苯二胺、三氯化磷、三氯氧磷、2，4—二氨基苯磺酸钠、二氯异氰脲酸钠、N-甲基邻苯二胺二盐酸盐等精细化工产品的能力，并且均以取得ISO9001国际质量体系认证。

A series of new DB21C7 derivatives with straight arm chains (crown 1 ~ 20) were firstly synthesized, and a thorough and systematic study about the influence of side arms which containing different length polymethylene and certain functional groups on extraction capacity of the parent DB21C7 was made.

本文利用DB21C7中苯环的活性，通过苯环上的亲电取代反应，首次设计合成了二苯并-21-冠-7桥连的二酮、直链烷烃、二醇、二酮酸、二烷酸以及二酰胺，共20个DB21C7取代衍生物，并以IR、~1H NMR、MS和元素分析进行了表征。

The invention provides a foliar fertilizer specially used for Chinese gooseberries, which has the functions of cold resistance and consists of the following raw materials according to weight percentage: 0.1 to 8 percent of DMSO, 0.05 to 5 percent of trimethylene glycol, 0.05 to 5 percent of salicylic acid, 0.05 to 2 percent of compound ammonium nitrate, 1 to 15 percent of humic acid, 0.5 to 10 percent of chitosan, 1 to 10 percent of citric acid, 2 to 15 percent of urea, 1 to 10 percent of borax, 1 to 20 percent of zinc sulfate, 0.5 to 10 percent of ferrous sulfate, 0.05 to 5 percent of ammonium molybdate, 1 to 15 percent of manganese sulfate, 0.1 to 2 percent of SDBS and 35 to 80 percent of water.

本发明提供一种具有抗寒作用的猕猴桃专用叶面肥，它由下述各组分重量百分比的原料组成：二甲基亚砜0.1％～8％、丙二醇0.05％～5％、水杨酸0.05％～5％、复硝铵0.05％～2％、腐殖酸1％～15％、壳聚糖0.5％～10％、柠檬酸1％～10％、尿素2％～15％、硼砂1％～10％、硫酸锌1％～20％、硫酸亚铁0.5％～10％、钼酸铵0.05％～5％、硫酸锰1％～15％、十二烷基苯磺酸钠 0.1％～2％、水35％～80％。

The amount of Na(superscript +), NH4(superscript +), K(superscript +), Mg(superscript 2+), Ca(superscript 2+), Zn(superscript 2+) in fruits and juice (sports water, green tea , pear juice, carrot juice and carrot and orange juice) were respectively separated and detected by non-suppressed ion chromatography. And pyridine-2, 6-dicarbexylic was used as mobile phase to separated monovalent cations and pyridine-2, 6-dicarbexylic-ethylenedi-amine-oxalic acid was used as mobile phase to separated divalent cations.

采用非抑制型离子色谱法测定了水果以及饮料（运动型饮料、绿茶、水蜜桃汁、胡萝卜汁和胡萝卜橙汁）中Na、NH4、K、Mg(上标 2+)、Ca(上标 2+)、Zn(上标 2+)的含量，其中一价阳离子以吡啶－2，6-二羧酸为淋洗液测定，二价阳离子以吡啶－2，6-二羧酸+乙二胺+草酸为淋洗液测定。

The amount of Na+, NH4+, K+, Mg2+, Ca2+, Zn2+ in fruits and juice (sports water, green tea , pear juice, carrot juice and carrot and orange juice) were respectively separated and detected by non-suppressed ion chromatography.

采用非抑制型离子色谱法测定了水果以及饮料(运动型饮料、绿茶、水蜜桃汁、胡萝卜汁和胡萝卜橙汁)中Na+、NH4+、K+、Mg2+、Ca2+、Zn2+的含量，其中一价阳离子以吡啶-2，6-二羧酸为淋洗液测定，二价阳离子以吡啶-2，6-二羧酸+乙二胺+草酸为淋洗液测定。

The environmental black direct dye stuff without carcinogensis was prepared by 4,4'-diamino-dibenzidine-2-sulfonicacid,1-hydroxy-7-aminonaphthalene-3,6-dusuifonicacid,m-benzoic-diamine and aniline.

以4，4'-二氨基-二苯胺-2-磺酸代替苯胺，与1-羟基-7-氨基-3，6-二萘磺酸、间苯二胺、苯胺等合成无致癌作用的环保型黑色直接染料。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。