二酸的

The results indicate that it is possible to identify and distinguish these siccative oils because the unsaturated acid had changed into azelaic due to oxidation and polymerization during the drying process to make the chromatogram of siccative oils have a typical peak of C9 compound and provide a finger marker of m/z 217, and the concentration ratio of palmitic acid to stearic acid remains constant with time to facilitate the differentiation of oils.

分析时采用了热裂解与甲基化同时进行的技术。分析结果显示，4种干性油的不饱和脂肪酸在成膜后的甲基化产物均为壬二酸二甲酯，离子质量与离子电荷量比值为217，是干性油的特征检测峰。4种油中不同含量的软脂酸和硬脂酸在干性油成膜前后的比值不变，为干性油的甄别提供了可能性。

The chemical analysis result of modified lignin by alkaline-oxygen treatment is as following:The chemical analysis result of modified lignin by alkaline-oxygen treatment showed that the carboxyl group of modified lignin increased, since muconic acid type structure were generated from phenolic structure by ring-open reaction during alkaline-oxygen treatment.

氧碱处理改性木素的化学分析结果见下表；┌────┬────┬─────┬────────────────┬────┐│改性本素│OCH_3│总糖│C_9单元式│COOH │├────┼────┼─────┼────────────────┼────┤│O_4 │8.49 │0.07 │C_9H_(10.45)O_(3.7)(OCH_3)_(053)│10.82 │└────┴────┴─────┴────────────────┴────┘氧碱处理改性木素的化学分析结果表明，改性木素的羧基含量明显增加，在氧碱处理的过程中，由于芳环的开裂，(来源：ABCe6论6d文网www.abclunwen.com)形成了己二烯二酸结构，因此改性木素具有较高的反应活性，易与Al~(3+)形成络合。

After getting two systems'GLE, absorption experiment was operated in laboratorytype equipment and the operation condition of dibutyl sebacate as absorbent were studied, the relationship of 〓 and the content of maleic anhydride in gaseous mixtures, the temperature of gaseous mixture, the liquid and gases ratio, the temperature of absorbent and the content of maleic anhydride in absorbent were studied respectively.

在获得气液平衡关系后，在自行设计的小型实验设备上分别就癸二酸二丁酯吸收顺酐的操作条件：进塔气中顺酐含量的变化、进塔气体温度的变化、液气比的变化、进塔溶剂温度的变化和吸收剂中顺酐含量的变化等对吸收效率的影响进行了初步探讨，推荐了合适的操作条件。

Based on the investigation of the transesterification between dimethyl sebacate and 1,2,2,6,6-pentamethyl-4-piperinol, the synthetic technologies of Tinuvin292 and Tinuvin 765 were established. The two kinds of hindered amine light stabilizers were obtained in the yield of 93.3% and 92.4% respectively and qualified as the advanced level of the kindred overseas products.2. The synthetic technology of Tinuvin123 was studied and established. Using 2,2,6,6-tetramethyl-4-piperinol as the starting material, the product was synthesized successfully through oxidation, free-radical reaction and transesterification in overall yield of 57.6%.

本文研究建立了三个受阻胺类光稳定剂的合成工艺，探索了聚合型受阻胺类光稳定剂生产过程中不溶性副产物产生的原因，并设计、合成了一系列具有抑菌活性的新型受阻胺类光稳定剂。1、在研究癸二酸二甲酯与1，2，2，6，6-五甲基哌啶醇的酯交换反应的基础上，建立了受阻胺类光稳定剂Tinuvin292、Tinuvin765的合成工艺，分别以93.3%和92.4%的收率得到了光稳定剂Tinuvin292、Tinuvin765，所得产品质量达到了国外同类产品的水平。2、研究建立了受阻胺类光稳定剂Tinuvin123的合成工艺。

The synthetic technologies of three hindered amine light stabilizers were established, the reason for the insoluble side products formed in the production of polymerized hindered amine light stabilizers were studied, and a series of novel hindered amine light stabilizers with antibacterial properties were designed and synthesized in this present paper.1. Based on the investigation of the transesterification between dimethyl sebacate and 1,2,2,6,6-pentamethyl-4-piperinol, the synthetic technologies of Tinuvin292 and Tinuvin 765 were established. The two kinds of hindered amine light stabilizers were obtained in the yield of 93.3% and 92.4% respectively and qualified as the advanced level of the kindred overseas products.2. The synthetic technology of Tinuvin123 was studied and established.

本文研究建立了三个受阻胺类光稳定剂的合成工艺，探索了聚合型受阻胺类光稳定剂生产过程中不溶性副产物产生的原因，并设计、合成了一系列具有抑菌活性的新型受阻胺类光稳定剂。1、在研究癸二酸二甲酯与1，2，2，6，6-五甲基哌啶醇的酯交换反应的基础上，建立了受阻胺类光稳定剂Tinuvin292、Tinuvin765的合成工艺，分别以93.3%和92.4%的收率得到了光稳定剂Tinuvin292、Tinuvin765，所得产品质量达到了国外同类产品的水平。2、研究建立了受阻胺类光稳定剂Tinuvin123的合成工艺。

Several main non-ionic surfactants (AEO、TX、SpanTweem、EL) was used to emulsify liquid paraffin and di octyl sebacate and the anti-coalescence stability of the corresponding emulsion was studied, the impact of the presence of benzene and double bond in lyophobic moiety of surfactant and its length and matching with dispersed phase upon the interfacial viscosity and Gibbs elasticity was analyzed.

本文采用了几种主要的非离子活性剂(AEO、TX、Span-Tween、EL)来乳化白油和癸二酸二辛酯，通过对各乳液体系抗聚并稳定性的考察，分析了活性剂亲油链段的长度、苯环和双键的存在、及亲油链段与被乳化对象分子结构的匹配关系对界面粘度和Gibbs弹性的影响。

Base played a crucial role in this reaction: in the Pd2/L1 catalyzed α-arylation of ethyl malonate, K3PO4 is the base of choice; in the α-arylation of ethyl acetoacetate, K2CO3 is the most effective base.

在这类催化反应中，碱的选择具有重要的影响：以K3PO4为碱， Pd2/L1催化体系在丙二酸二乙酯的α-芳基化中，富电子溴代芳烃显示较好的活性； Pd2/L1催化的乙酰乙酸乙酯α-芳基化时，以 K2CO3为碱，催化体系显示较好的活性，这个催化体系可控制反应得到α-芳基乙酰乙酸乙酯，而不是脱乙酰基的产物。

TpRu(PPh3)(CH3CN)2PF6 (10mol%) catalyst effected the nucleophilic addition of water,alcohols,aniline, acetylacetone, pyrroles, and dimethyl malonate to unfunctionalized enediynes under suitable conditions (100 °C, 12 24 h) and gave functionalized benzene products in good yields.

TpRu 2PF6 （ 10mol ％）催化剂的影响的亲核加成的水，醇，苯胺，丙酮，吡咯和二甲基丙二酸对unfunctionalized enediynes适当的条件下（ 100 ℃， 12日24小时），并官能苯产品良好的收益。

Different from many other researches the Henkel-Esterification process was studied here which starts from 1,8-naphthalenedicarboanhydride. In the Henkel reaction of 1,8-naphthalenedicarboanhydride to 2,6-naphthalenedicarboxylic acid (abbreviated as 2,6-NDA) non-cadmium catalytic system was used. In atmosphere of carbon dioxide 1,8-naphthalenedicarboanhydride can be effectively converted to 2,6-NDA in the temperature range of 300~340℃ with zinc carbonate as catalyst and the yield of 2,6-NDA can reach more over 62%.

和国内外绝大多数研究不同的是，论文结合公司自身的原料资源优势和长远规划，提出了从工业苊深加工产品—1，8-萘二甲酸酐出发，经过非镉系催化剂催化转位，然后再进行非酸催化酯化合成2，6-萘二甲酸二甲酯的工艺路线，并对工艺过程中涉及的成盐过程、催化转位反应、酯化反应等进行工艺参数的重点考察，对合成产物进行分析确证。

Measurement of some physiological factors related to salt-tolerance in wheat cultivars SW12 Using HPLC-ESI-MS technique, Glycinebetaine, proline and malondialdehyde in leaves, which collected from wheat cultivars SW12, Ningchun 4 and Chinese Spring exposed to salt treatments with concentration ranges of NaCl s of 0, 100, 200, 300, 400 and 500 mmol/L and sampling for 1, 3, 5, 10, 20 and 30 days, respectively, were measured.

小麦SW12耐盐种质生理指标测定 HPLC-ESI-MS分析表明，SW12和两个对照品种宁春4号和中国春在6个不同盐浓度（0、100、200、300、400和500mmol/L NaCl）和6个不同的盐胁迫时段中（1、3、5、10、20和30d），随着盐胁迫强度的增加，它们叶片组织中甜菜碱、脯氨酸和丙二醛的含量均有不同程度的增加，3个品种在5种不同盐浓度下，甜菜碱和丙二醛的含量存在很大差异。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。