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In the first part, chemical synthesis, including by acraldehyde, malonic ester, ami no lactone and others were discussed and synthesis by hydantoin was emphasized.

第一部分讨论了DL-蛋氨酸及其衍生物的化学合成,包括丙烯醛法、丙二酸酯法,氨基内酯法等,并着重介绍了海因法。

The effects of AX8900 as a compatibilizer introduced on the mechanical properties, thermal performance and section morphology of the blends poly and poly (butylene adipate-co-terephthalate) were investigated.

研究了AX8900作为增容剂对聚乳酸/对苯二甲酸、己二酸、1, 4-丁二醇三元共聚酯复合材料的力学性能、热性能、动态力学性能和断面形貌的影响。

The influences of different surfactants (sodium dodecyl sulfate, sodium cholate and sodium deoxycholate), different electrolytes (sodium phosphate monobasic, sodium tetraborate and 3-cyclohexylamino-1-propane sulfonic acid), buffer pH and organic modifiers on the determination of sialic acid were studied.

其次建立了一种测定唾液酸的在线富集CZE法,该方法用40 mM磷酸二氢钠为缓冲溶液电解质,通过将样品溶解在乙腈:水=2:1的样品基体中,进样时间增加到100 s来达到样品富集的效果,并考察了样品基体中乙腈浓度和进样时间对富集效果的影响,研究了用硼砂或3-环己胺-1-丙烷磺酸作为电解质、缓冲溶液pH值和有机修饰剂的加入对唾液酸检测的影响。

The cornhusk dilute acid hydrolysate after detoxification can be the substitution of glucose as a carbon source for producing succinic acid by anaerobic fermentation.

发酵试验表明脱毒的玉米籽皮稀酸水解液作为碳源厌氧发酵制备丁二酸具有可行性。

Single crystal of Arginine dichloride dihydrate was studide by x-ray diffraction expriments in emphasis of main influence factors of arginine conformational variation,and was also compared with its other conformations in the existence of different anions.

以X光衍射实验对二水合氯酸的晶体结构进行了研究,重点讨论了影响精氨酸构象变化的主要因素并比较了在不同阴离子存在条件下精氨酸构象的变化情况。

Cycloalkylation of diethyl malonate and ethyl cyanoacetate with alkyl halide was investigated in the presence of toluene.

以甲苯为溶剂及带水剂,用粉末K2CO3代替常规使用的乙醇钠,在季铵盐和聚乙二醇混合相转移催化剂的存在下,含有活泼氢的丙二酸二乙酯和氰乙酸乙酯与二卤代物进行缩合反应,得到相应的环化物。

In this process, the electrolylic bath with cationic exchange membrance and leas electrode is used. The cathode liquor is oxalic acid, the anode liquor is diluted sulfuric acid. The process above has following advantages with high yield, top quality, lower cost, no "three wastes" pollution, and no oxalic aldehyde in the product. It is a cleaner and environment-friend technology, and is a development trend for production of glyoxalic acid. Complete analytical process for raw materials, intermediate and final products were established.

本论文通过对乙醛酸合成路线的研究,确定了草酸电解法制乙醛酸的工艺路线,此法采用装有阳离子交换隔膜和铅电极的电解槽,阴极电解液为草酸溶液,阳极电解液为稀硫酸,该工艺具有产品收率高、质量好、成本低、无三废污染、产品中无乙二醛等特点,是一条清洁、绿色工艺,是生产乙醛酸的主要发展方向。

Besides, the efficacious concentration of either morrhuic acid or sodium morrhuate was 0.1%, so they contained more docosahexaenoic acid and eicosapentaenoic acid and were ideal spermicides in vitro.

所以,含有较多廿二碳六稀酸、廿碳五烯酸的鱼肝油酸和它的钠称是较为理想的体外杀精子剂。

In order to check the corresponding compound at 31P NMR –45.4 ppm, stable pentacoordinate spirobicyclic 2-phenoxy-1,3-phenylene-dioxo-1,3,2-iminoacetoxyphosphoranes were synthesized through a new and efficient method whereby phosphorus pentachloride was displaced stepwise by catechol, N,O-bisamino acid and phenol, or catechol, phenol and N,O-bisamino acid, their 31P NMR chemical shifts are at about 31P NMR –45.0 ppm, the results showed that the compound 4 at 31P NMR –45.4 ppm was pentacoordinate phosphorane containing amino acid residue.

采用磷谱跟踪来研究上述成肽反应机理。例如在氮气保护下,0.1mmol O,O-亚苯基磷酰氯(1)和0.15mmol N,O-二苯丙氨酸(2)苯溶液加入0.6ml核磁管中,混合均匀,反应过程用磷谱检测。反应1分钟后,起始原料1(δp=19ppm)很快转变成N-磷酰苯丙氨酸的三甲基硅基酯(3)(δp=19.8ppm),在8分钟内,3完全转变成苯丙氨酸磷烷4(δp =-45.4ppm),同时出现环磷三酯(6)(δp=3.5ppm)。随着反应的进行,对应于化合物4的峰逐渐变小,而6逐渐变大。

Malonyloxyborohydride,a hydroboration reagent,is prepared by reaction of malonic acid and sodium borohydride,and is used to react with dihydromyrcene in THF.

用一种硼氢化试剂———丙二酸与硼氢化钠反应生成的丙二酰氧基硼氢化钠在THF中与二氢月桂烯反应制备香茅醇。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。