二酸的

Process for the manufacture of a dialkylphenylethylmalonatewhich comprises adding to a quantity of sodium which is covered with a hydrocarbon solvent boiling above 100°C, at least a chemically equivalent proportion of methyl, ethyl or a propyl alcohol, subsequently adding an approximately equivalent proportion of a dialkylcarbonate and of an alkyl phenylacetate, the alkyl groups in these two last-mentioned compounds being preferably the same as the alkyl radical of the above –mentioned lower aliphatic alcohol, heating the mixture to induce reaction and continually distilling out the alcohol formed from the reaction zone and finally causing the sodio diethyl phenylmalonate so formed to interact with an ethylating agent.

生产二烷基苯基丙二酸酯的工艺过程：这包括这包括把至少处于化学平衡的甲醇，乙醇或丙醇添加到覆盖着沸点超过一百摄氏度的碳氢化合物溶剂中，接着加入大约相同当量的二烷基碳酸酯和烷基乙酸苯酯，在刚才提到的化合物中，其烷基集团最好是和刚才提到的低级别脂肪族醇相同，然后加热反应混合物从而引导反应的进行，在反应区域通过连续蒸馏移除形成的醇类。最后使所形成的钠代二乙基苯基丙二酸酯和乙基化试剂反应。

With sulfosalicylic acid, oxalic acid or salicylic acid used as additives, the isolated yield of adipic acid increased with increasing reaction time, but after 6 h, it did not increase obviously.

当使用磺酸水杨酸、草酸、水杨酸为有机酸性添加剂时，随反应时间的增加，己二酸分离产率均升高，但反应6 h以后，己二酸分离产率随时间的变化不明显。

The results showed that in acetone and ethanol, solubilities of 3, 28-di-O-glutaryl-betulin were 33.52 and 22.65 times of those of betulin respectively; In water, solubility of 3, 28-di-O-glutaryl-betulin was 0.0021 g (100 mL water), and in PBS, solubility of 3, 28-di-O-glutary-betulin was 0.0015 g (100 mL PBS), the hydrophilicity of 3, 28-di-O-glutaryl-betulin was significantly increase.

结果表明，在丙酮和无水乙醇中，桦木酐戊二酸酯的溶解度是桦木醇的33.52和22.65倍；在水中，桦木醇戊二酸酯的溶解度为0.0021g（100mL水）；在PBS中，桦木醇戊二酸酯的溶解度约为0.0015g(100mL PBS)，目标产物的亲水性有了显著的改善。

A small molecule core (TMP-SK3)with three terminal carboxyl groups was synthesized successfully by the reaction of 1,1,1-trihydroxymethylpropane with the excessive sebacic acid diacetic anhydride.

以1，1，1-三羟甲基丙烷与过量癸二酸二乙酸酐反应，制得了端羧基的三官能度小分子核三癸二酸三羟甲基丙烷酯（TMP-SK3）。

Single dibasic acid can be identified by infrared spectroscopy while mixed dibasic acids have to be differentiated by paper chromatography in isopro-pan...

用顺丁烯二酸酐固化的环氧树脂经水解与分离后得到的主要是反丁烯二酸和少量顺丁烯二酸，前者的含量随固化温度的提高而增多，因而确证这一顺-反异构化反应是在固化过程中受热，而不是在水解，酸化时受化学试剂的作用产生的。

ABSTRACT In this paper, by employing dicarboxylic acids with special conformation, i.

利用几个结构上有特点的二元羧酸，即2，6-吡啶二甲酸、三个异构体苯二甲酸，顺丁烯二酸和4，4'-联苯甲酸作为首要桥基配体，并结合使用含氮中性配。。。

The chemical constituents of extracts of Tamarindus indica L were determined by GC-MS. The relative contents of constitutes were determined by area normalizing method. 48 compounds were identified, amounting to total mass fraction 98.5%. The main compounds were 5-methyl-2(3H)-furanone, diethyl succinate, furfural, hexadecanoic acid, linolenic acid, 5-methylfurfural, oleic acid, linoleic acid, etc.

并利用气相色谱仪-质谱仪对罗望子萃取物的化学组成进行了分析鉴定，并用面积归一化法测定了各种成分的质量分数，共鉴定了48种成分，占总质量分数为98.35%，其中主要成分为：5-甲基-2(3H)-呋喃酮、丁二酸二乙酯、糠醛、十六酸、亚麻酸、5-甲基糠醛、油酸、亚油酸等。

The synthesis method of the invention is as follows: first, 5-amino-2-(p-aminophenyl)- benzoxazole and aliphatic diacid are respectively recrystallized; NMP is distilled; solubilizer is dried; second, in an atmosphere of nitrogen, after Py and NMP are mixed evenly and added to a sealed reactor, the solubilizer is added into the reactor, followed by the 5-amino-2-(p-aminophenyl)- benzoxazole, then the mixture in the reactor is stirred; second, in an atmosphere of nitrogen, the mixture in the second step is stirred and heated to 50-150 DEG C, then the aliphatic diacid is added, followed by TPP for condensation; fourth, after methanol is poured into the reactor, the sediment is separated out from the mixture, filtered, washed and dried, so the semi-aromatic polyamide containing oxazole ring is obtained.

本发明的合成方法如下：一、分别重结晶5-氨基-2-苯并唑与脂肪族二酸；蒸馏NMP；干燥增溶剂；二、在氮气气氛下，Py与NMP混匀后加入密封的反应器中，再加入增溶剂，然后加入5-氨基-2-苯并唑，搅拌；三、在氮气气氛下，将步骤二的混合液搅拌并升温至50℃～150℃后加入脂肪族二酸，再加入TPP后缩聚；四、再倾入甲醇析出沉淀，过滤，清洗沉淀，再干燥；即得到含唑环半芳香聚酰胺。

Dibutyl succinate was synthesized catalyzed by a strong acid cation exchange resin from succinic acid and n-butyl alcohol.

用强酸性阳离子交换树脂催化丁二酸和正丁醇的酯化反应，合成了丁二酸二丁酯。

The novel process of preparation of DNS by means of dioxygen liquid-phase oxidation of NTS with synthesized metal phthalocyanine complex catalyst in alkali solution under mild condition were systematically investigated for the first time.

首次以金属酞菁络合物为模拟酶催化剂，在碱性水溶液中，于温和条件下，研究了4-硝基甲苯-2-磺酸催化氧化制取4，4'-二硝基二苯乙烯-2，2'-二磺酸的方法和工艺。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新