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In this paper, a series of low cross-linking polyurethanes are synthesized using polycaprolacton or polybutamethylene adipate or polyethylene-propylene adipate, MDI and glycerin. Their mechanical, thermal and dynamical properties and shape memory function are studied.

采用聚己二酸乙丙二醇酯、聚己二酸丁二醇酯、聚己内酯和 4,4'-二苯基甲烷二异氰酸酯为原料,以丙三醇为交联剂合成了一系列低度交联的聚氨酯,讨论了组成、配比等对性能的影响,比较了它们和线型聚氨酯在性能上的差别。

hydantoin was synthesized from diethyl malonate comprising condensation with 1, 2-dichloroethane, ammonolysis to diamide, Hoffmann degradation to give 5-cyclopropanespirohydantoin, and ring-opening with 40% hydrobromic acid.

以丙二酸二乙酯为原料,先与1, 2-二氯乙烷缩合生成1, 1-环丙烷二羧酸二乙酯,再经氨解生成1, 1-环丙烷二甲酰胺,然后在次氯酸钙溶液中进行Hoffmann降解成环生成5-环丙螺海因,最后在40%氢溴酸中开环得到5-溴乙基海因。

An experiment was conducted to study the antifeeding effects of ethanol, ethyl acetate and water solutions of linoleic acid, pimelic acid, suberic acid, azelaic acid, and n-nonanoic acid against imago of Pissodes punctatus. Absolute antifeeding rate and relative antifeeding rate were used to appraise the antifeeding effects of organic acids.

为了寻找华山松木蠹象(Pissodes punctatus Langor et Zhang)环境友好的防治方法,研究了亚油酸、庚二酸、辛二酸、壬二酸、壬酸的酒精溶液、乙酸乙酯溶液和水溶液对华山松木蠹象成虫的拒食作用,采用了完全拒食虫率与相对拒食率来评价有机酸的拒食效果。

The results showed that there were 8 kinds of aliphatic, 5 kinds of esters, 2 kinds of aldehydes, 2 kinds of nitrogen sulfur heterocyclic rings and one kind of hydrocarbon, alcoholics, ketone, lactones respectively in the analyzed 21 kinds of aroma components, and the content of furfural,β-methyl valeric acid, palmitic acid, nicotine, neohytadiene were higher, next were acetyl ethyl propionate, caleric acid, phenyl ethyl acetate, hydroxylic diethyl succinate.

结果表明,在分析出的21种香气成分中,分别有脂肪酸类8种,酯类5种,醛类2种,氮硫杂环类2种,烃类、醇类、酮类、内酯类各l种,其中相对含量较高的物质成分是糠醛、β-甲基戊酸、十六碳酸、烟碱、新植二烯,其次是乙酰丙酸乙酯、异戊酸、苯乙酸乙酯、羟基丁二酸二乙酯等。

Undecanedioic acid, dodecanedioic acid, brassylic acid, tetradecanedioic acid, pentadecanedioic acid, nylon 1212 resin, nylon 1212 salt, nylon 1212 powder, pa 1212 adhesives and sealants, zirconium dioxide, zirconium dioxide powder, zirconium oxychloride, 1,10-decanediol, 1,12-dodecanediol, dimethyl sebacate, dodecanedioic acid dimethyl ester, dodecane diamine etc.

十一碳二元酸,十二碳二元酸,十三碳二元酸,十四碳二元酸,十五碳二元酸,十二碳二元胺,十二碳二元醇,癸二醇,癸二酸二甲酯,十二碳二酸二甲酯,PA尼龙1212型高档热熔胶;以及二氧化锆,氧氯化锆等。

M treatment materials, and also tartaric acid and no maleic acid detected in G. v treatment materials. Inoculation also increased the content of organic acid secretion (increased by 19.80~56.87 mg/kg) of trifoliate root, and the application of AlPO4 greatly increased organic acid content (increased by 20.06~21.84 mg/kg); uninoculated plant root secreted a bit of organic acid; Mycorrhizal poncirus trifoliata seedlings excreted malic acid (42.87%), citric acid (39.22%) and oxalic acid (12.06%).

接种AM真菌的根系分泌的有机酸种类与对照有所不同,未接种处理枳分泌的有机酸有草酸、苹果酸、乳酸、乙酸、顺丁烯二酸和柠檬酸等6种,而接种G.m的则检测到草酸、酒石酸、苹果酸、乳酸、乙酸、柠檬酸、丁二酸等7种,G.v处理的检测到酒石酸,接种处理均未检测到顺丁烯二酸;接种丛枝菌根真菌增加了枳根系分泌有机酸的量比未接种处理增加19.80~56.87 mg/kg,且施用AlPO4后有机酸含量显著增加(增加20.06~21.84 mg/kg;未接种植株根系仅分泌少量有机酸;接种植株根系分泌的有机酸以苹果酸(42.87%)、柠檬酸(39.22%)和草酸(12.06%)为主。

The OH-terminated linear aliphatic polyester polybutylene sebacate was synthesized by sebacic acid and butancdiol using solution polycondensation combined with melt polycondensation. The composition and construct characteristic of the product were analyzed by GPC, FT-IR and 1HNM.

以丁二酸和丁二醇为原料,采用溶液与熔融结合法合成了端羟基聚丁二酸丁二醇酯,用甲苯-2,4-二异氰酸酯对PBS封端,合成了线性遥爪型纸张增强剂TDI-PBS。

Intermidiate 1, 2-propanediol-sebacate was synthesized with 1, 2-propanediol and sebacic acid, then a novel degradable elastomer, poly, was synthesized by melt phase polycondensation of 1, 2-propanediol-sebacate and citric acid under under certain conditions.

通过癸二酸与1,2-丙二醇反应,生成中间体癸二酸聚酯二元醇,然后将中间体与柠檬酸在一定条件下熔融缩聚制得了一种可降解弹性体聚癸二酸丙二醇柠檬酸酯。

They were two new compounds, [cyclo(Pro-Val-Phe-Phe-Pro-Val-Phe-Ser-Leu),7],[2-N-(1-methoxycarbonylethyl)guanosine, 10], and eight known compounds,(p-hydroxybenzoic acid, 1),(methyl succinate, 2),(russulaceramide, 3),(phenylalanine, 4),(guanine, 5),(β-carboline, 6),(uridine, 8), and (adenosine, 9). All the compounds were isolated from Amanita exitialis for the first time.

分别为:对羟基苯甲酸(p-hydroxybenzoic acid,1)、丁二酸二甲酯(methyl succinate,2)、神经酰胺(russulaceramide,3)、苯丙氨酸(phenylalanine,4)、鸟嘌呤核苷(guanine,5)、β-咔啉(β-carboline,6)、环(脯氨酸-缬氨酸-苯丙氨酸-苯丙氨酸-脯氨酸-缬氨酸-苯丙氨酸-丝氨酸-亮氨酸) [cyclo(Pro-Val-Phe-Phe-Pro-Val-Phe-Ser-Leu),7]、尿嘧啶核苷(uridine,8)、腺嘌呤核苷(adenosine,9)、2-N-(1-甲氧羰基乙基)鸟苷[2-N-(1-Methoxycarbonylethyl)guanosine, 10]。10个化合物均为首次从致命鹅膏中分离得到,其中化合物7和10为新化合物。

When the molar ratio of tungstic acid∶acidic organic additive∶cyclohexene∶ hydrogen peroxide was 1∶1∶40∶176 (tungstic acid, 2.5 mmol) and the tungstic acid/resorcinol used as catalyst, the isolated yield of adipic acid was up to 90.9% for 8 h.

当使用磺酸水杨酸、草酸、水杨酸为有机酸性添加剂时,随反应时间的增加,己二酸分离产率均升高,但反应 6 h 以后,己二酸分离产率随时间的变化不明显。当磺酸水杨酸用量为 2.5 mmol 时,己二酸分离产率和纯度均较高。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。