二酸

To enhance the yield of adipic acid, The reactions towards formation of NA and decomposition of dione should be promoted to eliminate side reactions.

为提高己二酸收率，应使反应向生成硝脑酸方向进行，促进双酮分解成己二酸，减少副反应。

With sulfosalicylic acid, oxalic acid or salicylic acid used as additives, the isolated yield of adipic acid increased with increasing reaction time, but after 6 h, it did not increase obviously.

当使用磺酸水杨酸、草酸、水杨酸为有机酸性添加剂时，随反应时间的增加，己二酸分离产率均升高，但反应6 h以后，己二酸分离产率随时间的变化不明显。

A series of 3 - aryl - 3 -( 5,5 - dimethyl - 3 - hydroxy - 2 - cyclohexene - 1 - one - 2 - yl) propanoic ester s were synthesized by reaction between aromatic aldehydes ,5,5- dimethyl -1,3-cyclohexanedione and isopropylidene malonate catalyzed by KF - Al2O3 in alcohols.

在KF-Al_2O_3催化下，将芳香醛3，5-二甲基-1，3-环己二酮及丙二酸亚异丙酯在醇中反应，一锅式合成了一系列的3-芳基-3-(5，5-二甲基-3-羟基-2-环己烯-1-酮-2-基)丙酸酯。

The synthesis method of the invention is as follows: first, 5-amino-2-(p-aminophenyl)- benzoxazole and aliphatic diacid are respectively recrystallized; NMP is distilled; solubilizer is dried; second, in an atmosphere of nitrogen, after Py and NMP are mixed evenly and added to a sealed reactor, the solubilizer is added into the reactor, followed by the 5-amino-2-(p-aminophenyl)- benzoxazole, then the mixture in the reactor is stirred; second, in an atmosphere of nitrogen, the mixture in the second step is stirred and heated to 50-150 DEG C, then the aliphatic diacid is added, followed by TPP for condensation; fourth, after methanol is poured into the reactor, the sediment is separated out from the mixture, filtered, washed and dried, so the semi-aromatic polyamide containing oxazole ring is obtained.

本发明的合成方法如下：一、分别重结晶5-氨基-2-苯并唑与脂肪族二酸；蒸馏NMP；干燥增溶剂；二、在氮气气氛下，Py与NMP混匀后加入密封的反应器中，再加入增溶剂，然后加入5-氨基-2-苯并唑，搅拌；三、在氮气气氛下，将步骤二的混合液搅拌并升温至50℃～150℃后加入脂肪族二酸，再加入TPP后缩聚；四、再倾入甲醇析出沉淀，过滤，清洗沉淀，再干燥；即得到含唑环半芳香聚酰胺。

The inhibition effects of di-(2-ethylhexyl)-sebacate on the corrosion behavior of reinforcing steel bar were investigated by electrochemical polarization curves and electrochemical impedance spectroscopy in simulated pore solution.

采用动电位极化曲线和电化学阻抗谱研究了癸二酸二异辛酯在模拟混凝土孔隙液中对钢筋的保护作用。癸二酸二异辛酯的加入导致混凝土钢筋的腐蚀电位正移，对钢筋的阳极电化学过程有抑制作用。

The liner for double-based propellant was prepared from HTPB,toluene diisocyanate,diisooctyl sebacate,1,4-butanediol and mica.

以端羟基聚丁二烯、癸二酸二异辛酯、1，4 丁二醇、绢云母、甲苯二异氰酸酯等为原材料，制备了双基药柱用包覆层。

High molecular weight poly was obtained from succinic acid and 1,4-butanediol through a polycondensation process.

以丁二酸、丁二醇为原料，通过直接缩聚反应合成了高分子量聚丁二酸丁二醇酯。

Three fullerene derivatives including a bisadduct of tetraethyl methano[60] fullerenediphosphona- te、a dimalonic acid[60]fullerene (DMA C60and fullerol were used to study the relationship between their photo-induced GSH depletion and structures.

采用二加成亚甲基富勒烯[60]二膦酸四乙酯、二加成富勒烯[60]丙二酸(DMA C60)和富勒醇 3种富勒烯衍生物研究富勒烯衍生物的结构与光诱导细胞内GSH耗竭的关系。

Segmented polyester polyurethaneurea based n 4, 4'-disphenylmethane diisocyanate, ethylene diamine and polybutylene adipate elastomers and their deuterated polymers were studied by means of IR spectroscopy.

用红外光谱法对基於4，4'-二苯基甲烷二异氰酸酯、乙二胺和聚己二酸丁二醇酯的嵌段聚酯型聚脲氨酯弹性体及其氘化產物进行了研究。

The premixing self-assembly solution of horseradish peroxide with poly(sodium 4-styrenesulfonate) is made by blending HRP and polyelectrolyte PSS,and the active.enzyme muhilayer biofilm is fabricated by altemate deposition of and PDDA on the surface of negative ionized PET.

以阳离子化的辣根过氧化物酶和阴离子聚苯乙烯磺酸钠的预混合溶液，与阳离子聚电解质聚二甲基二烯丙基氯化铵通过逐层组装，在阴离子化聚对苯二酸乙二酯表面构建了多层生物活性膜。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。