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Acetanilide,hexane diacid and potassium hydrogen phthalate were used as additives to improve polyvinyl chloride crystallinity.

通过傅里叶转换红外光谱、差示扫描量热法及广角X射线衍射法研究了乙酰苯胺、己二酸和邻苯二甲酸氢钾与聚氯乙烯的相容性及对聚氯乙烯结晶度的影响。

The results of clinical assessment showed that levosimendan was safe and effective which could improve the prognosis of the patients and kept normal blood kinetics. By improving the reported synthetic route, levosimendan was synthesized from acetanilide via eight steps of reaction.

本论文探索了左西孟旦的合成路线,对文献报道的合成工艺进行了合理有效的改进,以乙酰苯胺为原料,最终经Friedel-Crafts反应,羰基α-位溴代,丙二酸二乙酯缩合,水解,脱羧,环合,拆分及重氮化加成等八步反应合成了左西孟旦。

In this paper,acetanilide,adipic acid and potassium hydrogen phthalate were chosen as additives to advance polyvinyl chloride to crystallize. The effects of compress mold,annealing temperature and time,additive property and loading on the crystallization,microscopicmorphology and mechanical properties of PVC were studied by means of wide angle X-ray diffraction,differential scanning calorimetry,fourier transform infrared spectrophotometer,scanning electron microscopeand tensile test.

本文利用乙酰苯胺、己二酸和邻苯二甲酸氢钾作为聚氯乙烯结晶改性的添加剂,通过广角X-射线衍射法、差示扫描量热法、傅立叶转换红外光谱、扫瞄电镜和万能电子实验机研究了热压、热处理温度和时间、添加剂结构和质量分数对PVC结晶、微观形态和宏观机械性能的影响。

Waste minimization in ammonolysis process of O,O-dimethylphosphorochloridothioate;2. An Investigation on the Micelle-Catalytic Hydrolysis and Ammonolysis of Carboxylic Acid Esters;3. The final product is generated by ammonolysis of the compound under high pressure.

以4-溴-1,8-萘酐为原料,用2,4-二甲基苯胺在醋酸中与之反应得到N-2′,4′-二甲基苯基-4-溴-1,8-萘酰亚胺,然后将NDNA在高压下用氨水进行氨解得到最终产品。

Activaed organic substrate react with carbon dioxide,which can be changed carboxylic acid in the way.

合成了二苯乙二酮缩双苯胺锰的配合物,研究了其对CO2的固定及催化CO2同有机底物反应。

This invention discloses an intermolecular charge transfer chromogen with triphenylamine group, with a formula indicated by (1), wherein: R1 is hydrogen atom or methyl group or methoxyl group, R2 is hydrogen atom or 2-(5,5-dimethyl-3-vinylcyclohexenyl-2-enylidene)propanedinitrile group.

本发明公开的含三苯胺基团的分子内电荷转移生色团,具有式1所示的结构式,其中R 1 为氢原子或甲基或甲氧基,R 2 为氢原子或2-(5,5-二甲基-3-乙烯环己烯基-2-烯亚基)丙二腈基。

First, the precursor polymer with azobenzene groups on main-chain was obtained by condensation polymerization between 4,4'-dihydroxyazobenzene and N,N-(2-bromoethyl)aniline through Williamson reaction. Then the azo polymer containing azobenzene groups both on main-chain and side-chain was prepared through an azo-coupling reaction between the precursor polymer and the diazonium salt of 4-nitroaniline.

设计并合成了一种新型的主侧链均含偶氮生色团的聚合物,首先通过4,4'-二羟基偶氮苯与N,N-二溴乙基苯胺之间的Williamson反应缩聚得到主链含偶氮苯基团的先驱聚合物,再通过重氮偶合反应得到目标产物,并利用核磁共振、红外光谱、紫外可见光谱、热分析等手段确认了所制备聚合物的结构。

Then sodium ethoxide was used as base,the nucleophilic substitution of 2-pyrrolidone with the intermediate provided nefiracetam.

以碳酸钠为缚酸剂,摩尔比为1︰1的2,6-二甲基苯胺与氯乙酰氯反应合成了中间体2-氯-N-(2,6-二甲基苯基)乙酰胺;在强碱乙醇钠作用下,2-吡咯烷酮再与2-氯-N-(2,6-二甲基苯基)乙酰胺经亲核取代合成了目标化合物奈非西坦。

Two novel aromatic diamines consisting of triphenylamine and 1,3,4-oxadiazole groups were successfully synthesized.

本研究成功合成二种含有三苯胺及1,3,4-恶二唑结构的新型芳香族二胺单体。

To estimate the bioconcentration factor of benzene derivatives in fish by gas chromatography retention time, this paper measured the BCF of chlorobenzene, o-chloro-toluene, p-dichlorobenzene, m-dichlorobenzene, 1,2-dichlorobenzene, nitrobenzene, p-chloro-aniline, p-chloro-nitrobenzene, and 4-chlorodiphenyl in grass crap, and the t_R of test derivatives on the stationary phases of six kinds polarity.

为了用气相色谱保留时间估算取代苯类化合物在鱼体内的生物富集系数,测定了草鱼对氯苯、邻氯甲苯、对二氯苯、间二氯苯、邻二氯苯、硝基苯、对氯苯胺、对硝基氯苯、4-氯联苯9种取代苯类化合物的BCF和不同取代苯化合物在6种不同极性固定相上的tR,建立了tR与BCF的一元回归方程及tR一阶分子连接性指数(1XV)与BCF的二元回归估算方程。

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