二苯胺

Two kinds of di aniline derivative s connected with oxamethylene bridge or azamethylene bridge were synthesizied by condensation of o nitrophenol and ethylene dibromide (1,4 dibromobutane)or 4 chloro 3,5 dinitrobenzotyifluoride and ethylene diamine(1,6 hexandiamine)and consequent reduction.

由邻硝基苯酚和二溴乙烷以及由4－氯－3， 5－二硝基三氟甲苯和乙二胺为原料通过桥接、还原合成两类由氧亚甲基或氮亚甲基桥联的双苯胺衍生物。

The poly with p-aminophenyl-ethynyl as a side-group was synthesized through Pd-catalyzed Sonogashira coupling reaction between 4-[(2,5-dibromophenyl)ethynyl] aniline and 1,4-diethynyl-2,5-bis benzene.

通过单体4-[(2，5-二溴苯)乙炔基]苯胺和1，4-二乙炔基-2，5-二戊氧基苯之间的Sonogashira偶合反应合成了带有p-氨基苯乙炔基共轭侧基的聚对苯撑乙炔。

The 1,5-Bis(4-aminophenylazo) anthraquinone, 1,5-bis(4-hydroxyphenyl azo) anthraquinone and 1,5-bis(3-methyl-4-hydroxyphe nylazo) anthraquinone were synthesized by diazotizing 1,5-biaminoanthraquinone with nitrosyl sulfuric acid and coupling with aniline, phenol and o-cresol.

合成以1，5-二氨基蒽醌为原料，经亚硝酰硫酸重氮化，分别和苯胺、苯酚及邻甲酚偶合，得到双（4-氨基苯）－1，5-二偶氮蒽醌，双（4-羟基苯）－1，5-二偶氮蒽醌和双（3-甲基－4-羟基苯）－1，5-二偶氮蒽醌，反应产率达47%~62%。

Yuan[2]and Robarge[3]reported another method that utilizes 2,3-dichloroaniline and diethanolamine as raw material and phosphorus pentoxide and triethy-lamine hydrochloride as catalyst.

元[ 2 ]和robarge [ 3 ]报道的另一种方法，利用2，3 -二氯苯胺和二乙醇胺为原料，五氧化二磷和triethy -拉明盐酸为催化剂。

Their electrochemical behaviors for single solute and mixed systems of hydroquinone(H2Q) and pyrocatechol are investigated.A pair of redox peak of H2Q and two pairs of redox peaks of PC on the composite film electrodes can be obviously distinguished in their mixed systems,which show the composite film electrodes have excellent electrocatalytic activity for two ...

结果表明聚苯胺复合膜电极具有很好的电催化作用，在混合体系中对苯二酚的一对氧化还原峰和邻苯二酚的两对氧化还原峰能够清楚地区分；并且在一定的浓度范围内单组分的浓度与峰电流呈良好的线性关系，说明该电极对苯二酚的测定在定性、定量中具有潜在的应用价值。

Phenylenediamines, aminophenols, methoxyanil ines, and 1,4- hydroquinone, 1-naphthylamine were polymerized via the catalysis of horseradish peroxidase in mixed solvents of l,4-dioxane and water at amibient conditions by using hydrogen peroxide as the oxidant. Several factors influencing the polymer yield, such as the concentration of the substrate, pH value and oxidant amount were examined using a- phenylenediamine as substrate.

本文选择了苯二胺、氨基苯酚、甲氧基苯胺三个系列，以及对苯二酚、1-萘胺等单体，在二氧六环-水混合介质中以辣根过氧化物酶为催化剂，以双氧水为氧化剂进行了不同底物的室温酶促聚合，并以邻苯二胺为底物考察了溶剂用量、pH值、作为氧化剂的双氧水用量等条件对聚合物收率的影响。

In this paper,pyromellitic dianhydride,1,2,3,4-cyclobutanetetracarboxylic dianhydride,4[(4-aminophenyl)-bis(4-methoxyphenyl)methyl]benzeneamine,4-hexyloxy-biphenyl-3′,5′-diaminobenzoate,and additive ADD-34 were used to synthesize four PIs.

文章用均苯四甲酸二酐，4[(4-氨基苯基)-二(4-甲氧基苯基)甲基]苯胺，1，2，3，4-环丁烷四羧酸二酐，4-己烷氧基联苯酚-3′，5′-二胺基苯甲酸酯和不同含量的添加剂制备了聚酰亚胺液晶取向剂。

In the process, 2, 4-difluoroaniline is used to carry out ammoniated reaction. Then through a series of similar reactions, the important intermediate of temafloxacin, which is called 7-chloro-6-fluoro-1-(2, 4-difluorophenyl)-1, 4-dihydro-4-oxo-3-quinoline acid, is gained.

与环丙沙星和二氟沙星类似，用2，4-二氟苯胺进行胺化反应，再进行一系列类似的反应，制得合成替马沙星的关键中间体7-氯-6-氟-1-（2，4-二氟苯基）-1，4-二氢-4-氧代喹啉-3-羧酸。

The calculated results validate the rationality of molecular structure design for TPA-based organic dyes.5.Effects on DSCs performance by dye bath solvents were investigated,and dichloromethane is chosen for sensitizers' comparison.6.The Incident Photon-to-Ccurrent Conversion Efficiencyand Current-Voltage curves of the DSCs based on the as-prepared dyes were measured.The relationship between dye structures and photovoltaic performance of the DSCs were studied.

计算结果证明了三苯胺基染料分子结构设计的合理性。5、研究了TiO_2膜的染料敏化时所用溶剂对电池性能产生的影响，结果表明，二氯甲烷溶液敏化的膜电极，用于DSCs的测试，均表现出较好的光电性能。6、通过入射单色光光电转换效率以及电流-电压曲线的测试，系统表征了三苯胺基染料敏化的DSCs的光电转换性能，揭示了影响电池性能参数差异的因素。

The experimental results indicate that the reaction rate exhibited first-order with respect to aniline and half-order to APS and dodecylbenzene sulfonic acid.

研究结果表明，苯胺的乳液聚合反应速率对苯胺是一级反应；对APS和十二烷基苯磺酸均为0.5级反应。

What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢？

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我，一个心中布满虚荣的女孩子真实的想法。