二聚的

A new kind of copolyetherimide is synthesized, and effect of contents of this kind of COPEI resin on morphology of blends of COPEI/the diglycidyl ether of bisphenol A(the Epikote 828)/ 4,4'-diamino diphenyl sulphone and preparation of epoxy resin microspheres are researched .

采用共缩聚方法合成了一种新型聚醚酰亚胺，通过改变它在COPEI/双酚A二缩水甘油醚型环氧树脂(E828)／二氨基二苯基砜共混体系中的用量，考察了对共混体系的相结构以及对制备环氧树脂微球的影响。

The prepared PU was an elastic solid,which could dissolved in ethanol,and it exhibited strong deep purple fluorescence at the peak of 365 nm along with a shoulder at 386 nm as a thin film. Obviously,the prepared PU also was a kind of uncommon ultraviolet-emitting polymer materials.2.A novel water-soluble rod-coil block copolymer was designed and prepared successfully via the facile isocyanic acid polycondensation method using polyfluorene as rod segment and polyethylene glycol as coil segment in the main chain for the first time.

所制备的聚氨酯是一种弹性固体，可以溶解在乙醇中，同时又显示出具有半导体性质的荧光性能——最大荧光发射峰在365 nm并且在386 nm处有一个小的侧肩峰，可见它又是一种非常难得的紫外发光聚合物材料。2、首次采用了简单的异氰酸酯反应，成功地将聚芴作为刚性链段和聚乙二醇作为柔性链段，以嵌段方式连结到聚合物分子主链上，从而形成了一种新型的具有刚性链—柔性链结构的嵌段共聚物。

N,N '- ditertbutyl nitroxyl radical, 2, 2,6,6- tetramethyl-4 - hydroxyl piperdinehy droxylamine and its nitroxyl radical, as inhibitors of the BPO- initiated copolymerization of styrene (M 1 ) with acrylonitrile (M2 ), at 60℃,has been studied.

研究了二叔丁基羟胺，二叔丁基氮氧自由基，2，2，6，6－四甲基－4－羟基哌啶羟胺和2，2，6，6－四甲基－4－羟基哌啶－1－氧自由基对过氧化苯甲酰60℃引发的苯乙烯（M1）－丙烯腈（M2）共聚合的阻聚行为。

The aim of this study was to develop a novel amphiphilic functional block poly(ε-caprolactone) bearing ketone groups MPEG-b-P(OPD-co-CL. 2-oxepane-1, 5-dione was copolymerized with ε-caprolatone in which methoxy poly (MPEG, Mn=5 000) and stannous octoate were used as initiator and catalyst, respectively. The syntheses were conducted by bulk and solution polymerization. 1H NMR results showed that peak position and splitting of the polymers synthesized through solution polymerization were consistent with theoretical data, demonstrating the products were designed block copolymers. While in the bulk polymerization, polymer peak position was changed due to their high reaction temperature, suggesting their structural variation.

将带有羰基官能团的4-羰基己内酯和ε-己内酯分别在甲氧基聚乙二醇(MPEG，Mn=5 000)为引发剂，异辛酸亚锡为催化剂溶液和本体体系中开环聚合，合成了两亲性侧基带有羰基官能团的聚己内酯嵌段共聚物MPEG-b-P(OPD-co-CL.1H NMR结果表明采用溶液聚合法合成的聚合物各峰的峰位置和分裂情况与理论一致，证明了产物是实验所设计的嵌段共聚物，而采用本体聚合法合成的聚合物由于温度的影响，聚合物各峰的峰位置发生了变化，说明其结构发生了变化；差示扫描量热法分析结果表明随着OPD单体含量的增加，聚合物的熔点，玻璃化转变温度和熔融焓增加；热失重测试结果表明OPD单体的引入增加了聚合物的热敏感性。

The properties of single chain and pauci chain polystyrene microspheres and recent results on the electron microscopy and selected area electron diffraction of single chain monocrystals of polyethylene oxide, isotactic polystyrene, cis1,4 polybutadiene and gutta percha are presented and discussed.

介绍和讨论了单链和寡链聚苯乙烯玻璃体微球的性质以及聚环氧乙烷、同立构聚苯乙烯、－，4－丁二稀、－，4－异戊二烯单链单晶电子显微镜和选区电子衍射观察的最新结果。

Compounds were identified by means of physic-chemical property and spectral data including three new compounds: platyphyllin A (1), neochlorgeniclatone (2),(2E,6Z)-2,6-dimethyl-8-O-β-D-glucosyl-2,6-octadienoic acid (3). The known compounds included cyclic diarylheptanoids, phenylic acid, ect.

从白桦叶的水提取物中，利用各种色谱分离手段(硅胶柱色谱、聚酰胺柱色谱、凝胶柱色谱及制备薄层色谱等)，分离得到28个化合物，通过理化性质及各种波谱数据(NMR，MS，IR，etc)鉴定了23个化合物的结构，其中新化合物三个：platyphyllin A(1)，新绿原酸内酯(neochlorgeniclatone，2)，(2E，6Z)-2，6-二甲基-8-O--2，6-辛二烯酸(2E，6Z-2，6-dimethyl-8-O-β-D-glucosyl-2，6-octadienoic acid，3。

Based on 26B4APBN monomer, polyamic acid was obtained by polymerization with pyromellitic dianhydride, and further imidized into polyimide film by heating process.

由二胺单体和均苯四甲酸二酐进行聚合得到26B4APBN/PMDA聚酰胺酸，再经热亚胺化得到聚酰亚胺薄膜；测试了该薄膜的接触角，讨论了单体分子结构对聚合物接触角的影响。

The isotropy or anisotropy in some physical properties of the amorphous poly films uniaxially drawn at temperatures above its T g and then quenched to room temperature have been studied.

对非晶态聚对苯二甲酸乙二酯膜片经在Tg以上单轴拉伸然后淬冷至室温的试样，其物理性质的各向同性或各向异性进行了研究。

Amorphous PET film was uniaxially drawn over a wide range oftemperatures from below to above 〓 at a constant strain rate.

研究了非晶聚对苯二甲酸乙二酯膜在〓以下直至〓以上20℃范围内以恒定的速率单轴拉伸，拉伸温度，拉伸比对取向、弛豫、以及诱导结晶的影响。

A novel method to prepare Au nanorings by self-reduction of HAuCl4 in the soft template composed of sodium dodecyl sulfate-PEG 20000 cluster at ambient temperature and atmosphere was reported, in which no hard template and extra reducer was needed. TEM image displays that the diameter of Au nanorings is (500±50)nm.

介绍一种由十二烷基硫酸钠与聚乙二醇(PEG 20000)组成的团簇为软模板，在室温、常压、无硬模板及无外加还原剂条件下自还原HAuCl4合成金纳米环的新方法。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。