二聚的
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The invention relates to a process for producing polyethylene terephthalate 1, 3-propanediol, which comprises the following steps: using titanic acid ester as major catalyst, using germanium compounds and cobalt compounds as synergic catalyst, conducting esterification reaction for poly terephthalic acid and 1, 3-propanediol according to the molar 1:1.05-2.2 under the nitrogen pressure of 0.1-0.4MPa and 230-265 DEG C, or conducting ester exchanging reaction for poly terephthalic acid and 1, 3-propanediol according to the molar ratio 1:1.8-2.2 in 160-220 DEG C, decompressing reaction to high vacuum 10-150Pa, wherein the final temperature of reaction is 265-275 DEG C, recovering to normal pressure with nitrogen to obtain the PTT product.
本发明涉及一种生产聚对苯二甲酸1,3-丙二醇酯的方法,采用以钛酸酯为主催化剂,锗化合物和钴化合物为协同催化剂,对苯二甲酸二甲酯和1,3-丙二醇按摩尔1∶1.05-2.2,在0.1-0.4MPa氮气压力和230-265℃下进行酯化反应,或对苯二甲酸二甲酯和1,3-丙二醇按摩尔比1∶1.8-2.2,在160-220℃进行酯交换反应,将反应减压至高真空10-150Pa,反应终温在265-275℃,用氮气恢复到常压,得到本PTT产品;大大缩短了反应时间,直接聚合制备特性粘度在0.7-1.05dL/g的PTT切片,使反应产物色相良好,PTT产品可用于纤维加工及工程塑料领域。
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The intermediate decyl-glycidol ether of Gemini phosphate surfactant was synthesized with decanol and epichlorohydrin in the presence of phase-transfer catalyst; the intermediate decyl digomeric glycol of Gemini phosphate surfactant was prepared by opening ring reaction of decyl glycide ether and glycol in the presence of potassium as catalyst; and the influence of type and dosage of phase-transfer catalysts was studied.
以正癸醇与环氧氯丙烷为原料在相转移催化剂存在的条件下合成Gemini磷酸酯表面活性剂的中间体I-正癸基缩水甘油醚,讨论催化剂种类及用量对反应的影响;以乙二醇和正癸基缩水甘油醚为原料,金属钾为催化剂合成Gemini磷酸酯表面活性剂的中间体Ⅱ-正癸基低聚二醇,讨论催化剂种类与用量对反应的影响;以P2O5与正癸基低聚二醇为原料合成Gemini磷酸酯表面活性剂,讨论投料比、反应温度和反应时间等因素对反应的影响。
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A new cationic polyelectrolyte has been synthesized by the modification of polyacrylamide with formaldehyde and dicyanodiamide.
用甲醛和二氰二胺改性聚丙烯酸胺,制得新型阳离子聚电解质PAm·MG,对PAm·MG的合成和表征进行了研究。
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A novel type of amphiphilic tri-block copolymers with both pH and temperature sensitiveness: poly-poly (dimethylamino ethyl methacrylate)-poly (ε-caprolactone)(PEG-PDMAEMA-PCL) was synthesized via sequential oxyanionic polymerization of macro-molecular: PEG, with a hydroxyl at one end, and dimethylamino ethyl methacrylate andε-caprolactone, with the potassium naphthalene as the initiator.
在本文中,报道了一类新型的兼具pH和温度敏感的双亲性嵌段共聚物:聚乙二醇-聚甲基丙烯酸N,N-二甲氨基乙酯-聚己内酯(PEG-PDMAEMA-PCL)及聚甲基丙烯酸N,N-二甲氨基乙酯-聚己内酯(PDMAEMA-PCL)的制备;并利用动态光散射和氢核磁共振光谱(~1H NMR)对该嵌段共聚物的水溶液性质进行研究;在此研究结果的基础上,初步探讨了其在仿生物矿化中的应用。
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The copolycondensation type polyamic acid was synthesized by using 3,3', 4,4'-Benzophenonetetracarboxylic dianhydride as the dianhydride monomer, 4,4'-Diamino diphenylmethane and 4,4'-Oxydianiline as the diamine monomer under microwave irradiation in Dimethylformamide.
在微波辐射条件下,采用3,3',4,4'-二苯酮四羧酸二酐、4,4'-二氨基二苯甲烷和4,4'-二氨基二苯醚为单体,N,N'-二甲基甲酰胺为溶剂,低温合成一种共缩聚聚酰亚胺的前驱体聚酰胺酸,化学亚胺化脱水环化生成BTDA型共缩聚聚酰亚胺。
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These pathways include the production of advanced glycation end products, alterations in the sorbitol, hexosamine and protein kinase C pathways and activation of poly-ADP ribose polymerase.
代谢和血管通道的缺陷包括三个方面,一是糖基化终未产物形成,二是山梨醇、氨基己糖和蛋白激酶 C 改变,三是多聚二磷酸腺苷核糖多聚酶激活。
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We researched the high molecular polyether,polyamide hot melt adhesive, 2-phenoxy ethanol phenyl cellosolve,propylene glycol phenylate,etc,which have passed appraisal of the provincial science and technology achievement.the company gains higher economy profit after putting into production.
公司设有专业科研机构从事新产品的开发研制工作。先后研制开发成高分子聚醚,聚酰胺热熔胶,乙二醇苯醚,丙二醇苯醚等十多项新产品,均通过省级科技成果鉴定。
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Methods: According to the relationship between psychophysiologic disorders and constipation, 114 patients with STC were divided into three groups which received venlafaxion hydrochloride , polyethylene glycol 4000(PECA000) or both of them respectively.
根据便秘与精神心理异常的因果关系,将STC患者分为三组,分别服用文拉法辛、聚乙二醇4000及文拉法辛和聚乙二醇4000,比较治疗前后HAMA、HAMD评分、大便性状、排便次数及胃肠通过时间测定变化。
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Polyols can be divided into latex polyol and dispersion polyolaccording to the way of preparation. In this paper, acrylic latex polyol and acrylic dispersionpolyol were synthesized respectively. One kind waterborne polyisocyanate, which was waterbornehexamethylenediisocyanate trimer, was obtained by hydrophilic modification. Andisophorone diisocyanate trimer (T1890E), which can formulate into 2K-WPU coatings withpolyols, was selected from the unmodified polyisocyanates.
本文合成了两种羟基组分:丙烯酸乳胶多元醇和丙烯酸分散体多元醇,亲水改性得到了一种水性多异氰酸酯组分:水性六亚甲基二异氰酸酯三聚体,同时在未改性的多异氰酸酯组分中遴选了一种多异氰酸酯:异佛尔酮二异氰酸酯三聚体(T1890E),可用来组成双组分水性聚氨酯涂料。
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OBJECTIVE: To evaluate use of peginterferon-alpha2a plus ribavirin to re-treat nonresponders to peginterferon-alpha2b plus ribavirin.
目的:评价聚乙二醇干扰素α-2b联合利巴韦林治疗无应答的患者接受聚乙二醇干扰素α-2a联合利巴韦林再治疗。
- 推荐网络例句
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We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.
索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称;三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起,称之为挽歌体诗人或者史诗诗人,他们被称为诗人,似乎只是因为遵守格律写作,而非他们作品的模仿本质。
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The relationship between communicative competence and grammar teaching should be that of the ends and the means.
交际能力和语法的关系应该是目标与途径的关系。
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This is not paper type of business,it's people business,with such huge money involved.
这不是纸上谈兵式的交易,这是人与人的业务,而且涉及金额巨大。