二聚的

2A series of alternating polyamide-imideswith fluorenyl cardo structure was synthesized by "one-pot" polycondensation of cardo diamines,trimellitic anhydride and various aromatic diamines including p-phenylene diamine,m-phenylene diamine, 4,4\'-oxydianiline,3,4\'-oxydianiline,2,2-bis[4-(4-aminophenoxy)phenyl]propane, 2,2-bis[4-(3-aminophenoxy)phenyl]propane respectively using triphenyl phosphite as condensing agents.

采用"一锅法"(One—pot Synthesis)，由Cardo二胺、偏苯三酸酐和不同二胺包括对苯二胺、间苯二胺、4，4\'—二氨基二苯醚、3，4\'—二氨基二苯醚、2，2—双[4—(4—氨基苯氧基苯基]丙烷和2，2—双[4—(3—氨基苯氧基)苯基]丙烷合成了一系列含有芴基Cardo结构的交替聚酰胺酰亚胺。

Polyethersulfone with cardo was a developed engineering thermoplastic and membrane material with high glass transition temperature,PES-C ultrafiltration membranes were prepared by phase inversion method using dimethylacetamide as solvent and oxalic acid and polyethylene glycol as additives.The membrane morphology forming and evolution could be observed by the experimental system and method.The effect of additive and polymer concentration on cast solution and the gelation kinetics of polyethersulfone with cardo asymmetric membrane were studied.

采用耐高温工程塑料——含酚酞侧基的聚芳醚砜为膜材料，草酸和聚乙二醇为添加剂， N，N -二甲基乙酰胺为溶剂，并利用改进的凝胶动力学实验装置和方法，使之能真实地再现不同膜孔结构生长及发展演化的过程，借助相关软件对图像进行处理，考察了添加剂、聚合物浓度对铸膜液凝胶速度的影响，对酚酞基聚芳醚砜非对称膜的凝胶过程的动力学进行研究。

Effect of heat treatment on the ndcrophase separation of a segmented poly copolymer based on poly diol, 3, 5 dithyltoluene diandne and 4,4'-diphenylmethane diisocyanate has been studied bymeans of fourier transform infrared spectroscopy.

用傅里叶变换红外光谱方法研究了热处理对由聚环氧丙烷聚醚多元醇、3.5－二乙基甲苯二胺和4，4－二苯基甲烷二异氰酸酯组成的多嵌段聚氨酯脲的微相分离行为的影响。

The method is realized by that polyether ether ketone is added into concentrated sulfuric acid to carry out sulfonation reaction, thereby obtaining sulfonated polyether ether ketone, then the sulfonated polyether ether ketone is dissolved in organic solvent, N, N (1)-Carbonyldiimidazole is added to stir for one to three hours, coupling agent is mixed for stirring the reaction for 1.5 to 4 hours, then inorganic crosslinking agent is mixed to react under the temperature of 50 to 80 DEG C. Proton conductors are mixed to continue getting the mixed solution of the sulfonated polyether ether ketone or the inorganic crosslinking agent or proton conductors under the temperature. Finally the proton exchange membrane for a direct methanol fuel cell is obtained by that the mixed solution of the sulfonated polyether ether ketone or the inorganic crosslinking agent or proton conductors is/are processed through membrane forming, drying and exuviation.

该方法首先将聚醚醚酮加入浓硫酸中进行磺化反应得到磺化聚醚醚酮；然后将磺化聚醚醚酮溶于有机溶剂中，加入N，N′-羰基二咪唑搅拌1～3小时后加入偶联剂搅拌反应1.5～4小时，再加入无机交联剂在50～80℃下反应，然后加入质子导体继续在此温度下反应得到磺化聚醚醚酮/无机交联剂/质子导体的混合溶液；最后将磺化聚醚醚酮/无机交联剂/质子导体的混合物溶液成膜，干燥，脱膜即得到所述的直接甲醇燃料电池用质子交换膜。

Utilizing 6 and several kinds of diazides prepared in our lab, polys containing 1,2,3-triazolyl and perfluorocyclobutane units were synthesized by "Click chemistry". Utilizing the polycondensation reaction between 6 and several commercially available aromatic diphenol or copolymerization reaction after adding another active aromatic dichloride, fluorinated polys containing phenylphosphine oxide units were synthesized. Utilizing the polycondensation reaction between 6 and several commercially available aromatic dianhydride, fluorinated polys containing PPO units were synthesized.Secondly, structure characterization of fluorinated polys.

利用化合物6同各种自制的二叠氮化合物，通过&Click chemistry&，合成了具有1，2，3-三唑环结构单元的全氟环丁基类聚芳醚；利用化合物22同各种商业化的芳香二元酚类化合物进行缩聚反应或者再加入另外一种活性芳香二氯代物进行三元共聚反应，制备了具有苯基氧膦结构单元的含氟聚芳醚；通过化合物25同各种商业化的芳香二元酸酐类化合物进行缩聚反应，得到了具有PPO结构单元的含氟聚醚酰亚胺。

2A series of alternating polyamide-imideswith fluorenyl cardo structure was synthesized by "one-pot" polycondensation of cardo diamines,trimellitic anhydride and various aromatic diamines including p-phenylene diamine,m-phenylene diamine, 4,4\'-oxydianiline,3,4\'-oxydianiline,2,2-bis[4-(4-aminophenoxy)phenyl]propane, 2,2-bis[4-(3-aminophenoxy)phenyl]propane respectively using triphenyl phosphite as condensing agents.

采用&一锅法&(One—pot Synthesis)，由Cardo二胺、偏苯三酸酐和不同二胺包括对苯二胺、间苯二胺、4，4\'—二氨基二苯醚、3，4\'—二氨基二苯醚、2，2—双[4—(4—氨基苯氧基苯基]丙烷和2，2—双[4—(3—氨基苯氧基)苯基]丙烷合成了一系列含有芴基Cardo结构的交替聚酰胺酰亚胺。

2A series of alternating polyamide-imideswith fluorenyl cardo structure was synthesized by "one-pot" polycondensation of cardo diamines,trimellitic anhydride and various aromatic diamines including p-phenylene diamine,m-phenylene diamine, 4,4\'-oxydianiline,3,4\'-oxydianiline,2,2-bis[4-(4-aminophenoxy)phenyl]propane, 2,2-bis[4-(3-aminophenoxy)phenyl]propane respectively using triphenyl phosphite as condensing agents.

采用&一锅法&O(来源：88AB57C论文网www.abclunwen.comne—pot Synthesis，由Cardo二胺、偏苯三酸酐和不同二胺包括对苯二胺、间苯二胺、4，4\'—二氨基二苯醚、3，4\'—二氨基二苯醚、2，2—双[4—(4—氨基苯氧基苯基]丙烷和2，2—双[4—(3—氨基苯氧基)苯基]丙烷合成了一系列含有芴基Cardo结构的交替聚酰胺酰亚胺。

A novel bis (o-aminobenzophenone) s monomer is synthesized, and is used to get three different polyquinolines containing phenylamine moiety through Frieldlander reaction. The solubilities, thermal stabilities and luminescent properties of the polymers were evaluated. All the polymers are thermal-stable, and are soluble in common organic solvents. The emission of their thin film is from excimer emission.

合成了一种新型的二邻氨基二苯酮单体，通过Frieldlander反应，可以构造出不同结构的含有类三芳胺基元的发光聚喹啉，对其溶解性、热性能进行了研究，结果表明这类聚喹啉在常用有机溶剂中的溶解性有了很大提高，同时保持了聚喹啉较高的热稳定性；研究了它们在溶液态和薄膜态的紫外可见吸收光谱和荧光发射光谱，发现它们在薄膜态下的荧光发射主要来自于分子间激基复合物发射。

Pyromellitic dianhydride and Sodium tetrazodiphenyl-naphthionate, 1,4-diaminoanthraquinone and Benzoguanamine as aromatic diamines were selected to be polymerized under microwave irradiation.

本论文选用均苯四酸二酐和刚果红、1，4—二氨基蒽醌、苯代三聚氰胺三种芳香族二胺作为单体，采用微波辐射的方法合成了具有非线性光学性能的聚酰胺酸和聚酰亚胺。

Dissolve 50.0g of polyethylene glycol in 75ml of diphenyl ether, previously warmed, if necessary, just to melt the crystals, in a 250ml distilling flask.

你的理解好像是必要时加入聚乙二醇和二苯醚后一起加热，而我的理解是必要时加入聚乙醇后用预先加热的二苯醚溶解。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。