二聚

The method is realized by that polyether ether ketone is added into concentrated sulfuric acid to carry out sulfonation reaction, thereby obtaining sulfonated polyether ether ketone, then the sulfonated polyether ether ketone is dissolved in organic solvent, N, N (1)-Carbonyldiimidazole is added to stir for one to three hours, coupling agent is mixed for stirring the reaction for 1.5 to 4 hours, then inorganic crosslinking agent is mixed to react under the temperature of 50 to 80 DEG C. Proton conductors are mixed to continue getting the mixed solution of the sulfonated polyether ether ketone or the inorganic crosslinking agent or proton conductors under the temperature. Finally the proton exchange membrane for a direct methanol fuel cell is obtained by that the mixed solution of the sulfonated polyether ether ketone or the inorganic crosslinking agent or proton conductors is/are processed through membrane forming, drying and exuviation.

该方法首先将聚醚醚酮加入浓硫酸中进行磺化反应得到磺化聚醚醚酮；然后将磺化聚醚醚酮溶于有机溶剂中，加入N，N′-羰基二咪唑搅拌1～3小时后加入偶联剂搅拌反应1.5～4小时，再加入无机交联剂在50～80℃下反应，然后加入质子导体继续在此温度下反应得到磺化聚醚醚酮/无机交联剂/质子导体的混合溶液；最后将磺化聚醚醚酮/无机交联剂/质子导体的混合物溶液成膜，干燥，脱膜即得到所述的直接甲醇燃料电池用质子交换膜。

The last section of Chapter 3 discusses the flux distribution of a quasi-single stage solar furnace which consists of a non-imaging focusing heliostat as the primary stage and a much smaller spherical concentrator as a secondary.

第三章的最后一节分析了准一阶聚光(quasi-single stage)太阳炉的聚光比分布。这种太阳炉的组成是由一个非成像聚光定日镜作为主要聚光装置，一个小的球面镜(来源：ABC论文5e网www.abclunwen.com)做为二次反射聚光装置。

Objective To study the pH and temperature sensitive properties of sulfamerazine oligomers-polyε-caprolactone-co- DL -lactide-b-ethyleneglycol- b -ε-caprolactone-co-DL-lactide-sulfamerazine oligomers（OSM1-PCLA-PEG-PCLA-OSM1）block copolymer and evaluate sustained release effect of 5-fluorouracil release from the loaded hydrogel in vitro.

摘要目的为嵌段共聚物磺胺甲嘧啶低聚物-聚-ε-己内酯-丙交酯-聚乙二醇-聚-ε-己内酯-丙交酯-磺胺甲嘧啶低聚物（sulfamerazine oligomers-poly(ε-caprolactone-co- DL -lactide-b-ethyleneglycol- b-ε-caprolactone-co-DL-lactide)-sulfamerazine oligomers，OSM1-PCLA-PEG-PCLA-OSM1作为缓控释给药系统的载体提供依据。

The method is simple, rapid, and accurate, and is suitable for the determination of melamine, ammeline, ammelide, and cyacuric acid in milk and milk powder.

该方法简便、快速、准确，可满足牛奶及奶粉中三聚氰胺、三聚氰酸、三聚氰酸一酰胺、三聚氰酸二酰胺测定的需要。

A HILIC-MS/MS method was developed to determine melamine and its three derivatives, cyanuric acid, ammelide and ammeline in milk and milk powder. The milk sample was directly extracted by acetonitrile with the help of ultrasonic, and milk powder was resolved in water before extraction by acetonitrile.

建立了牛奶和奶粉中三聚氰胺及其3种衍生物（三聚氰酸、三聚氰酸一酰胺、三聚氰酸二酰胺）的亲水色谱－串联质谱检测方法(HILIC-MS/MS)。

After centrifugation, the extracts were separated on HILIC column by using acetonitrile-water as mobile phase. The analytes were identified and quantitated by LC-tandem MS under the positive/negative electrospray ionization and multiple reaction monitormode. The calibration curves showed good linearity in the range of 25-5000 μg/kg for melamine and cyanuric acid, and 50-10000 μg/kg for ammeline and ammelide. The limits of detection and limits of quantification were in the range of 5-20 μg/kg and 50-100 μg/kg, respectively.

牛奶样品直接用乙腈超声波提取；奶粉样品先用水溶解后再加乙腈超声波提取，高速离心后以乙腈－水为流动相，采用亲水作用色谱柱分离这4种化合物，在电喷雾正、负电离切换多反应监测模式下进行定性与定量分析，三聚氰酸一酰胺与三聚氰酸二酰胺含量在50~10000μg/kg之间、三聚氰胺与三聚氰酸在25~5000μg/kg之间，均获得良好的线性。

A series of sulfonated poly(arylene thioether/ether phosphine oxide)s was prepared by direct polycondensation of sBFPPO and BFPPO with the diphenol-type or dimercapto-type monomers such as hydroquinone, bisphenol-A, 4,4'-biphenol, 4,4'-diphenol (6F), 1,5-dihydroxynaphthalene, 4,4'-dihydroxybiphenyl, and 4,4'-thiobisbenzenethiol, respectively.

将BFPPO与sBFPPO分别与多种二羟基或二巯基单体，如对苯二酚、双酚A、4，4'-二苯酚、双酚F、1，5'-二羟基萘、4， 4'-二羟基二苯硫醚和4，4'-二巯基二苯硫醚，直接共聚制备了一系列磺化聚芳醚三苯基氧膦，侧重考察了二羟基和二巯基单体结构单元对产物的耐氧化性能的影响。

A novel type of amphiphilic tri-block copolymers with both pH and temperature sensitiveness: poly-poly (dimethylamino ethyl methacrylate)-poly (ε-caprolactone)(PEG-PDMAEMA-PCL) was synthesized via sequential oxyanionic polymerization of macro-molecular: PEG, with a hydroxyl at one end, and dimethylamino ethyl methacrylate andε-caprolactone, with the potassium naphthalene as the initiator.

在本文中，报道了一类新型的兼具pH和温度敏感的双亲性嵌段共聚物：聚乙二醇-聚甲基丙烯酸N，N-二甲氨基乙酯-聚己内酯(PEG-PDMAEMA-PCL)及聚甲基丙烯酸N，N-二甲氨基乙酯-聚己内酯(PDMAEMA-PCL)的制备；并利用动态光散射和氢核磁共振光谱(~1H NMR)对该嵌段共聚物的水溶液性质进行研究；在此研究结果的基础上，初步探讨了其在仿生物矿化中的应用。

In order to improve its solubility and conductivity, the chemical oxidation method was used to prepare emeraldine salt type conductive polyaniline co-doped with nitric acid (HNO3) and dodecylbenzene sulfonic acid.

本研究使用化学氧化聚合法，以硝酸与十二烷基苯磺酸共掺杂制备导电性聚苯胺，采用共掺杂的方法不但可改善聚苯胺难溶的特性，更可兼顾聚苯胺之导电性。

The paper introduces the injection molding equipment, mold and molding technique for the thermotolerant engineering thermoplastic polyphenylene ether sulphone .

介绍耐高温热塑性工程塑料聚苯醚砜树脂的注射成型设备、模具和注射工艺等。相关：聚苯醚（聚2，6-二甲基苯醚），聚苯撑氧聚苯硫醚

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。