二羧基的

CA-CTSs including N,O-carboxymethyl chitosan,N,O-1-carboxyethyl chitosan (N,O-1-CEC),N,O-2-carboxyethyl chltosan(N,O-2-CEC),N-carboxymethyl chitosan and N-1-carboxyethyl chitosan(N-1-CEC) are quaternized using active quaternary salts prepared in laboratory.5 series including 25 kinds amphoteric chitosans characterized with polymeric ampholyte,in which 24 kinds are synthesized firstly,are obtained, 2-Hydroxypropyl dimethylbenzyl ammonium N,O-(1-carboxyethyl) chitosan chloride (GDMBA-N,O-1-CEC) is hydrolyzed into serial low molecular weight GDMBA-N, O-1-CEC with acid as catalyst and microwave as assistant instrumentality innovately.

以合成的活性季铵盐改性了N，O-羧甲基壳聚糖、N，O-1-羧乙基壳聚糖(N，O-1-CEC)、N，O-2-羧乙基壳聚糖(N，O-2-CEC)、N-羧甲基壳聚糖和N-1-羧乙基壳聚糖(N-1-CEC)等羧烷基壳聚糖，得到5个系列25种具有两性高分子电解质特征的新季铵化羧烷基壳聚糖，其中24种为首次合成；创新提出以微波辅助酸催化的方法催化2-羟丙基二甲基苄基-N，O-(1-羧乙基)壳聚糖氯化铵(GDMBA-N，O-1-CEC)水解，得到了低分子量的GDMBA-N，O-1-CEC。

One method of preparation new membrane materials was presented with putting multi-wall carbon nanotube and carboxylic multi-wall carbon nanotube in collodion solution.

分别将碳纳米管和羧基化碳纳米管均匀分散在火棉胶溶液中，采用流涎法制备出碳纳米管复合膜；并用分光光度法对样液、滤液中的间苯二酚和茜素红的吸光度进行了对比测定，以考察膜的吸附性能。

The fragment m/z 132 is 19 amu above the standard fragment mass for leucine or isoleucine, respectively; therefore, one of these amino acids has to be the C-terminal part of the dipeptide.

破片 m/z 132 分别比亮氨酸或亮氨酸残留物的标准破片质量多19个原子质量单位。因此，这些氨基酸中的一个个只能是二肽中的羧基末端。

The conjugation of MMS and Ab (ready for Reagent 1, R1): Chose the 3μm diameter Carboxyl MMS and use the carbodiimide cross-link technique activate the MMS with EDC and NHS in different concentration, then linked mice anti-HBsAg-IgG and mice anti-HCcAg-IgG on them.

磁微粒的活化及其与抗体的连接：选择粒径3μm的羧基化磁微粒，采用碳二亚胺共价交联法，在活化剂EDC与NHS的不同浓度组合条件下活化磁微粒，选择最适的活化剂浓度组合。

The present invention discloses a polycarboxylic acid copolymer which is obtained by copolymerization of monomer components comprising a polyalkyleneimine unsaturated monomer (A2) and an unsaturated carboxylic acid monomer, the polyalkylene glycol unsaturated monomer (A2) having an oxyalkylene group bonded to a polyhydric alcohol residue, and the monomer component containing an unsaturated monocarboxylic acid monomer.

公开了一种多元羧酸共聚物，它是通过单体组分共聚制得的，所述单体组分包括聚二醇不饱和单体(A2)和不饱和一元羧酸单体，所述聚二醇不饱和单体(A2)具有使氧化烯基结合到多元醇残基上的结构，所述多元醇残基平均每个分子具有不少于3个羟基。

This paper builtup esterification model, pre-polycondensation model, polycondensationmodel, and successfully built up monitoringon-line system of some key quality tar gets as well as operation systemmodel according to the polycondensation technique of NOY company.

本文在软测量技术的基础上，建立了酯化反应控制模型、预缩聚反应控制模型、终缩聚反应控制模型，并成功开发出在线控制系统，对生产过程中的关键质量指标如粘度、二甘醇、端羧基进行在线控制，控制精度达到小于2.5％。

In the thesis, a series of novel single and multi-armed oxadiazole bridging ligands and pyridyl-4, 5-imidazole dicarboxylic acid ligands have been synthesized. The coordination chemistry of these novel ligands with transition metal ions was investigated. In addition, two 1, 3, 4-oxadiazole bridging ligands end-capped by chelating Schiff-base coordination sites have been designed and synthesized. The coordination chemistry based on one of the two ligands with metal ions was primarily investigated.

本文报道了一系列新颖的含1， 3， 4-Oxadiazole杂环的单臂及多臂有机配体，研究了它们与过渡金属离子的配位反应化学；合成了吡啶基-4，5-咪唑二羧酸有机配体，研究了它们在水热条件下与过渡金属离子的配位反应化学；另外，还合成了1， 3， 4-Oxadiazloe杂环桥联的双Schiff-base有机配体，初步探讨了其与过渡金属离子的配位反应化学。

By using isopropyl benzene as the internal standard material, using Agilent 1100 HPLC, using methanol-acetonitrile-water as mobile phase ,using three-component grade elution program, the components that contain benzene such as TALD,PT,4-CBA,TA,BA,PX and internal standard material isopropyl benzene in liquid phase product was analysed. Shimazu6A GC was used to analyse the solvent acetic acid and internal standard material isopropyl benzne in liquid phase.

以异丙苯为内标物，应用Agilent1100高效液相色谱仪，用甲醇－乙腈－水为流动相，采用三元梯度洗脱程序分析液相产物中的含苯环组分对甲基苯甲醛、对甲基苯甲酸、对羧基苯甲醛、对苯二甲酸、苯甲酸、对二甲苯和内标物异丙苯，应用Shimazu6A气相色谱仪分析液相中的溶剂醋酸和内标物异丙苯。

In the third chapter, eight new complexes of 4, 6-dimethylpyrimidine 2-thioacetic acid with rare earth metals has been synthesized and characterized by means of elemental analysis, molar conductivity, IR,〓 NMR and TG-DTA. The general formula of the complexes is Ln〓(n=4 or 5). In the complexes, the deprotonated ligand coordinated to the rare earth metal ions in chelate bidentate mode. 4 or 5 molecular of crystal water existed in the complexes.

第三章合成了八种4，6-二甲基嘧啶-2-硫代乙酸的稀土配合物，通过元素分析、摩尔电导、红外光谱、核磁共振氢谱和热重-差热对配合物进行了表征，研究结果表明，配合物的组成为Ln〓n=4或5），在配合物中配体羧基脱去质子后采用螯合双齿的方式与稀土离子形成配位键，同时，配合物中含有4或5个结晶水。

These two types of coupling reagents can effectively promote the condensations between N-methyl or Ca,Ca-dialkyl amino acids, and the yields are usually more than 90%. The reactions can be carried out using the so-called ￠one-pot￠ procedure without the preactivation of the carboxylic components.

这两类新型缩合剂可以高效地促进N-甲基氨基酸间或Ca，Ca-二烷基化氨基酸间的缩合，产物的收率一般在90%以上，反应可以采用&一锅法&进行，无须首先对羧基组份预活化。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。