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Chlorpyrifos mehtyl with different dosages of 3,5,10 mg/kg compared with malathion 15 mg/kg in grain silo,each contented 40 thousand kilograms of rice was studied.To be sprayed by machine when loading to silo and to be observed two years through all experiment,the effective control to sitophilus zeamais of chlorpyrifos mehtyl 5 mg/kg can be protected more than six months,and 10 mg/kg over one year.

报道了甲基毒死碑(化学名称为二甲基O-3,5,6-三氯-2-吡啶基硫逐磷酸酯)3、5、10 mg/kg不同剂量,以防虫磷15 mg/kg作比较,在立筒库星仓内,每筒40000 kg稻谷,机械喷雾法处理,储藏二年,经生物测定对玉米象药效,甲基毒死蜱5 mg/kg可达半年以上,10 mg/kg可达一年以上防护期。

The composite stabilizer of chlorinated paraffin was made from ethylene glycol diglycidyl ether, methyl stannic, triphenyl phosphate, exoxidized soybean oil. The influences of components in the composite stabilizer for thermal stability of chlorinated paraffin were investigated.

以乙二醇二缩水甘油醚和甲基锡为主稳定剂、亚磷酸三苯酯和环氧大豆油为助稳定剂制备了氯化石蜡复合稳定剂,研究了各组分配比对氯化石蜡热稳定性的影响。

A four ball tester was used to evaluate the antiwear and extreme pressure properties of antimony dialkyldithiophosphate with friction reducer containing phosphorus, chlorinated paraffin(T301) and sulfurized isobutylene (T321), and their synergistic effects.

利用四球试验机评价了二烷基二硫代磷酸锑与含磷摩擦改进剂、氯化石蜡(T301)、硫化异丁烯(T321)3种添加剂的极压和抗磨性能,以及它们之间的极压和抗磨协同作用;利用市售演示仪评价了SbD-DP、T301和T321之间的协同抗擦伤能力。

The mobile phase was 0.1 mol/L ammonium oxalate + N,N-dimethylformamide + 0.2 mol/L diammonium phosphate (75+15+10, by vol) adjusted to pH 8 by aqueous ammonia. Column temperature was 30℃, flow rate was 0.8 ml/min, and detection wavelength was 365 nm.

使用C18反相柱和二极管阵列检测器,以0.1mol/L草酸铵溶液+二甲基甲酰胺+0.2mol/L磷酸氢二铵溶液=75+15+10(用氨水调pH值至8.0左右)为流动相,柱温30℃,流速0.8ml/min,检测波长365nm,外标法对水合霉素的有效成分进行定量分析。

It was concluded that no aging time was the most beneficial to form colloid, when molar ratio of phosphoric acid to antimony was in the range from 0.8 to 1.0 and 1.0 to 1.3, the particle sizes of sol with the concentration of 10 % and 15 % antimony pentoxide by weight are both smaller, and with the molar ratio of 1.0, the average particle sizes are (36±5.6)nm nm and (164±32)nm respectively.

结果表明:氧化锑混合物不进行陈化对胶体五氧化二锑的形成最有利;磷酸与锑的摩尔比分别为0.8~1.0和1.0~1.3时,10%和15%的胶体五氧化二锑胶粒粒径较小,当摩尔比为1.0时,粒径分别为(36±5.6)nm和(164±32)nm。

The products include antioxidants,blowing agents,organic solvents, intermediates for pesticides,drugs and dyestuffs,perfumes,water glass,silicates,molybdenum compounds,graphite series,activated carbon,plasticizers,flame retardant,heat stabilizers,food additives and chemical reagents,etc.

注册商标有&鹿牌&合成樟脑,&桃浦&牌合成樟脑副产物和其他化工产品,&金牛&牌抗氧剂,发泡剂,水合肼,二甲基乙酰胺,二甲基乙醇胺,&海球&牌硅胶系列,&飞铃&牌磷氯,双乙烯酮衍生物,磷酸酯,乙烯利等,&泉字&牌,&水晶&牌各类泡化碱系列,&上胶&牌钼类化合物,石墨类产品系列。

Flow injection fluorometry for the determination of carbamazepine in pharmaceuticals and plasmaA simple, sensitive and specific spectrofluorimetric method has been developed for the determination of CBZ. The method was based on lead dioxide solid-phase reactor flow injection on-line oxidizing CBZ into fluorescent product in medium of phosphoric acid. The product has green-yellow fluorescence at excitation wavelength of 355 nm and emission wavelength of 478 nm, and the fluorescence intensity could be enhanced in the presence of acetone. The reaction conditions and experimental conditions were studied and optimized.

二、流动注射在线氧化荧光法测定卡马西平的研究利用卡马西平自身无荧光,经过氧化后可转变为在最大激发波长为355nm,最大发射波长为478nm的强荧光物质,而且丙酮对该荧光体系有增敏作用的现象,应用流动注射体系建立了以醋酸纤维素固定化的二氧化铅作为固相反应器、在磷酸介质中在线氧化荧光法测定卡马西平的新方法。

Potassium dihydrogen phosphate was used as catalyst in the synthesis of hexanoic acid 2-ethyl ester.

用磷酸二氢钾作催化剂,己酸与二乙氨基乙醇为原料,合成DA-6。

The attack causes the cleavage of P-S double bonds, then the decomposition products reacting with the surface of Fe metal lead to the formation of the anti-wear and anti-friction film largely composed of polyphosphates and sulphides.

计算表明二烷基二硫代磷酸锌的活性元素为6位和7位硫原子,其与铁发生摩擦化学反应时,最可能的断键位置是6位和7位硫原子的双键。

Peptide nucleic acid is a kind of new nucleic acid mimic invented in the early 1990s', in which the deoxyribose phosphate backbone has been replaced by a pseudo-peptide polymer to which the nucleobases are linked. PNA is uncharged, highly stable in chemical and biological environments, and binds complementary DNA and RNA targets with remarkably high affirnity and specificity.

肽核酸是二十世纪九十年代初合成的一种全新的核酸类似物,它以多肽骨架完全替代DNA中的脱氧核糖磷酸二酯键的骨架,呈电中性,具有极高的生物和化学稳定性、极强的核酸结合能力和特异性,在分子生物学的许多方面得到广泛应用。

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