二磷酸

A process based upon solvent extraction has been developed for the recovery of phosphoric acid from a leaching liquor obtained by decomposition of phosphate rock with sulfuric acid.

本文采用二丁基亚砜作为萃取剂，对于用硫酸分解磷矿而得的粗磷酸进行多级逆流萃取及反萃取，以获得高纯度的磷酸和磷酸盐。

In this paper , two fluorocarbon amphoteric phosphate surfactants were synthesized and their performances were determined.

首先，磷酸二氢钠与环氧氯丙烷开环加成合成2-羟基-3-氯丙基磷酸酯钠，分离提纯后，分析其红外。

By methods of indirectly labelling with NaH〓PO〓 and directly labelling in atomic pile, Ca〓-P, Ca〓-P, Ca〓-P, Fe-P and A1-P were isotopically labelled.

试验结果进一步证明，菌丝际的土壤pH有所降低（0.2-0.4个单位）；磷酸二钙和磷酸八钙处理的菌丝际土壤溶液中磷浓度显著地高于基他处理。

Two kinds of water-soluble biomimetic chitosan derivatives with a phosphoramide linkage between glucosamine and choline were prepared through Atherton-Todd reaction under the mild conditions, including zwitterionic phosphorylcholine bound chitosan and acetyl-phosphorylcholine bound chitosan with positive charge. The interaction between chitosan derivatives and calf thymus DNA were inversigated by UV alsorption spectra and circular dichroism spectra.

采用Antherton-Todd反应制备了两种水溶性的磷酰化壳聚糖仿生衍生物：两性的N-磷酸胆碱磷酰化壳聚糖和带正电荷的N-乙基磷酸胆碱磷酰化壳聚糖，并用紫外吸收光谱和圆二色光谱研究了两种胆碱磷酰化壳聚糖衍生物与小牛胸腺DNA的相互作用。

Under high dilution,the cross-coupling reactions of 4,5-dicyano-1,3-dithiol-2-one(6) and dithia crown-ether annulated tetrathiafulvalenes(3a～3c) in toluene gave asymmetrical dicyano tetrathiafulvalene derivatives(7a～7c) in the presence of triethyl phosphite.The compounds 7a～7c were characterized by(~1HNMR,EA,MS and IR.

在甲苯溶液中，在亚磷酸三乙酯存在下，采取高度稀释的方法，使4，5-二氰基-1，3-二硫杂环戊二烯-2-酮分别和多缩硫杂冠醚进行交叉偶联反应，成功地得到了不对称的2，3-二氰基四硫富瓦烯衍生物。

For pre-selection of iron compounds that ferrous sulfate, ferrous chloride, ferrous fumarate, carbonyl iron, amino acid chelated iron, iron asporotate, fenic chloride and ferric pyrophosphate were added in reconstituted skim milk to undergo in vitro digestion, respectively, and then the selected iron compounds were added in reconstituted whole milk to compare the iron bioavailability by estimating dialyzable ferrous iron, dialyzable total iron, nondialyzable and total ferrous iron, respectively.

取硫酸亚铁、反丁烯二酸亚铁、氯化亚铁、艰基铁、Iron asporotate、Amino acid chelated iron、氯化铁与焦磷酸铁等不同铁剂添加於脱脂还原乳中进行体外消化试验，并筛选生物利用性佳之铁剂分别添加於全脂还原乳中，以可透析二价铁、可透析总铁、未透析二价铁及总二价铁等作为评估之指标。

For pre-selection of iron compounds that ferrous sulfate, ferrous chloride, ferrous fumarate, carbonyl iron, amino acid chelated iron, iron asporotate, fenic chloride and ferric pyrophosphate were added in reconstituted skim milk to undergo in vitro digestion, respectively, and then the selected iron compounds were added in reconstituted whole milk to compare the iron bioavailability by estimating dialyzable ferrous iron, dialyzable total iron, nondialyzable and total ferrous iron, respectively.

取硫酸亚铁、反丁烯二酸亚铁、氯化亚铁、艰基铁、Iron asporotate、Amino acid chelated iron、氯化铁与焦磷酸铁等不同铁剂添加於脱脂还原乳中进行体外消化试验，並筛选生物利用性佳之铁剂分别添加於全脂还原乳中，以可透析二价铁、可透析总铁、未透析二价铁及总二价铁等作为评估之指標。

The result showed that the thermal decomposition temperature of chlorinated paraffin reached 133℃ by adding 0.3% composite stabilizer in which the weight percentages of ethylene glycol diglycidyl ether, methyl stannic, triphenyl phosphate, exoxidized soybean oil were 72%, 3%, 10%, 15%, respectively. It is 15℃ more than that of using pure ethylene glycol diglycidyl ether.

结果表明：当复合稳定剂中乙二醇二缩水甘油醚、甲基锡、亚磷酸三苯酯、环氧大豆油的质量分数分别为72%，3%，10%，15%，复合稳定剂的添加量为氯化石蜡的0.3%时，氯化石蜡的热分解温度为133℃，比单独使用乙二醇二缩水甘油醚提高了15℃，热稳定效果较好。

Relative retentions of 12 S-compounds on 4 different liquid phases were given.

给出了十二种硫化物在沙鱼烷、苯二甲酸二壬酯、磷酸三甲苯酯及亚氨基二丙腈四种柱子上的相对保留值。

With the aid of 〓P NMR examination for the process and ESI-MS/MS analysis of the derivatized products from the reaction intermediate, it is found that the corresponding phosphoryl chloride is generated after mixing the hydrogen phosphonate derivative with chlorodiisopropylamine, and they react with amino acid, amino acid methyl ester, dipeptide methyl ester or N-methyl imidazole carboxyl alkyl diamine respectively to form the desired products.

利用〓P NMR对反应过程监测以及对反应中间体衍生化后产物的ESI-MS／MS检测分析发现，氢亚磷酸二酯与氯代二异丙胺反应首先生成了磷酰氯中间产物，它继续与氨基酸、氨基酸甲酯、二肽甲酯、1-甲基咪唑-2-酰基烷基二胺等反应生成了目标产物。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。