二磷酸

The results show that: the fillers of SiO_2 based investment consist of SiO_2,Al_2O_3 and MgO,and the binder is NH_4H_2PO_4;for SiO_2 based investment,the bulk density and the compression strength decrease,the apparent porosity and the thermal expansion increase,when the specimens are heated to 900 ℃;the fil.

结果表明：氧化硅系包埋料的骨料是氧化硅、氧化铝、氧化镁，结合剂为磷酸二氢铵，其900℃煅烧后显气孔率增加，体积密度下降，耐压强度降低，热膨胀增大；氧化铝系包埋料的骨料是氧化铝和氧化镁，结合剂为磷酸二氢铵，其900℃烧后显气孔率增加，体积密度下降，热膨胀变化不大；氧化镁系包埋料的骨料是氧化镁和氧化铝，结合剂是铝酸钙水泥，其900℃烧后耐压强度明显降低，热膨胀明显增大。

The results showed that:(1) 5'-nucleotide contents in yeast autolysate was slightly increased by adding RNase frommalted barley roots;(2) higher pH did not improve the 5'-nucleotide contents even in the presence of RNase from malted barleyroots, but at the pH 8.0, the addition of Acalase could increase the final yield, soluble protein contents and 5'-nucleotide inthe presence of RNase from malted barley roots.

酵母核酸酶的pH稳定性和温度稳定性均比麦芽根核酸酶的要差。这说明自溶法生产酵母提取物时，即使外加5'-磷酸二酯酶不能有效提高呈味核苷酸的原因并非由于外加的5'-磷酸二酯酶性质不稳定，而是另有其它原因。

The invention discloses a preparing method of bacillus alcaligenes strain Alcaligenes sp., CCTCC No.M206121 of degraded o-nitrophenol, which comprises the following steps: allocating inorganic salt culture medium with dibasic sodium phosphate, monobasic potassium phosphate, manganese sulfate, copperas, addex-magnesium, calcii chloridum, blue copperas, white copperas and hydrogen dioxide solution; adjusting pH value; sterilizing under high temperature; enriching bacterial; sampling from sludge; allocating suspending liquid with soil sample and inorganic salt; seeding into ortho-nitrophenol fresh organic salt culture medium with finite volume seeding quantity; keeping the temperature; culturing on shaker; getting enriched culture; separating and purifying enriched culture in LB solid culture medium.

本发明公开了一种降解邻硝基酚的产碱杆菌菌株及制备方法，产碱杆菌为Alcaligenes sp。，CCTCC No.M206121。其制备步骤是：首先是配制无机盐培养基，成分为磷酸氢二钠、磷酸二氢钾、硫酸锰、硫酸亚铁、硫酸镁、氯化钙、硫酸铜、硫酸锌和双蒸水，调pH值高压灭菌；其次是菌种的富集，从污泥中取样，将土样与无机盐培养基配制成悬浮液，将悬浮液以一定体积接种量接种到含邻硝基酚的新鲜无机盐培养基中，恒温，摇床培养，获富集培养物；第三是将富集培养物在LB固体培养基中分离和纯化。

The steps for preparing insecticide include: first shaking flask for fermentation, adding amidon, soya bean cake powder, cotton cake powder, protease leather, yeast powder, maize milk, magnesium sulfate heptahydrate, monobasic potassium phosphate, dibasic potassium phosphate, calcium carbonate alpha-amylase and make-up water by ratio in culture medium with 100 unit volumes; secondarily filling 100ml culture mediums in triangular bottle, then seeding BTH-13 after disinfection and culturing them until the brood-cell pulls off under finite temperature; third adopting the selected culture medium and fermenting them in full-automatic fermentation tank, acidifying the fermentation liquor after the fermentation, adding the emulsifier, and directly performing spray-drying after the compression of the fermentation liquor to prepare the wettable powder.

制备杀虫剂的步骤是：首先是摇瓶发酵，在100单位体积的培养基中，按比例加入淀粉、豆饼粉、棉饼子粉、蛋白胨、酵母粉、玉米浆、七水硫酸镁、磷酸二氢钾、磷酸氢二钾、碳酸钙、及α-淀粉酶，补充水；其次是在三角瓶中装100ml培养基，灭菌后接种BTH-13，在一定温度培养至芽孢脱落；第三是采用筛选出来的培养基，在全自动发酵罐中进行发酵，发酵结束后发酵液酸化，加入乳化剂，酵液浓缩后直接喷雾干燥制备可湿性粉剂。

Result The application of 3 mg/L potassium dihydrogen phosphate could promote potted seedlings of Arizona to flower earlier; the effect of 3 mg/L potassium dihydrogen phosphate +20 mg/L N 6-benzyladenine was the best. The flower bud differentiation was early and more, with the flowering rate of 90%, and the flowering branches were long and sturdy; when N6-benzyladenine was 40 mg/L, the growth of potted seedlings of Arizona was inhibited; N6-benzyladenine had a certain inhibition on leaf etiolation of potted seedlings of Arizona.

结果］喷施3 mg/L的磷酸二氢钾可促进亚丽桑那组培苗提早开花；3 mg/L磷酸二氢钾＋20 mg/L 6-苄基嘌呤的处理效果最好，花芽分化早、多，成花率高达90%，花枝长且粗壮；当6-苄基嘌呤浓度为40 mg/L时，亚丽桑那盆栽苗生长受抑制；6-苄基嘌呤对亚丽桑那盆栽苗的叶片黄化有一定的抑制作用。

Methods: The chromatographic separation was performed on a Hypersil ODS2 column(250 mm×4.6 mm, 5 μm) with mobile phases of potassium dihydrogen phosphate hexyl amine solution-acetonitrile(74∶26) for the determination of its related substances and methanol-0.05 mol/L potassium dihydrogen phosphate solution(1∶1) for the determination of dexbetamethasone sodium phosphate. The flow rate was 0.8 ml/min, the detection wavelength was 254 nm, the column temperature was 25℃ and the sample size was 20 μl.

色谱柱为Hypersil ODS2柱(250 mm×4.6 mm，5 μm)；有关物质测定的流动相为磷酸二氢钾己胺溶液-乙腈(74∶26)，含量测定的流动相为甲醇-0.05 mol/L磷酸二氢钾溶液(1∶1)；流速为0.8 ml/min，检测波长为254 nm，柱温为25℃，进样量为20 μl。

Examined the prospect of multiple kenaf forage harvests during a single growing season, harvesting kenaf at 85, 92, and 99 DAP and then reharvesting the same plants at 179 DAP.

1995检验红麻前景多在单一种植牧草丰收季节，在收割红麻85、92、 99、磷酸二铵reharvesting然后在同一厂磷酸二铵179。

The load carrying capacity and antiwear property of S,P containing benzotriazole derivative (BM 3) were evaluated using a four ball test machine,and compared with those of zinc salt di(T 202 ) and amine salt of complex ester thiophosphate (T 307 ). The antiwear mechanism of BM 3 were studied by investigating the chemical states and the mass fraction of elements on the rubbed surfaces using X ray photoelectron spectroscopy and electron probe microanalysis and the thermal decomposition products using gas chromatography mass spectrograph.

在四球机上对照评价了含硫、磷苯并三氮唑衍生物（BM－3）和二丁辛基二硫代磷酸锌（T202）及硫磷酸复酯胺盐（T307）的承载能力和抗磨性能，用X射线光电子能谱仪和电子探针微分析仪等对磨斑表面元素N，S和P的存在形式及表面膜的组成进行了分析，用气相色谱－质谱联用仪对BM－3的热分解产物进行了分析，并且还对其极压抗磨作用机理作了探讨。

Separation and recovery process principles of tail gases in producing dimethyl phosphite were introduced; Separation and recovery courses of hydrogen chloride and methyl chloride in tail gases were also analyzed. The percent recovery for hydrogen chloride and methyl chloride is over 99.9% and 93%, respectively, by using the process of combining stage recycle of solvent with lower temperature.

介绍了亚磷酸二甲酯生产中尾气回收的工艺原理，对尾气中氯化氢及氯甲烷的分离回收过程进行了分析；提出了采用吸收剂分段循环和降温相结合的回收工艺，将此工艺应用于3万t/a的亚磷酸二甲酯的生产装置的尾气回收上，可使氯化氢的回收率达99.9%，氯甲烷的回收率达93%以上，盐酸质量分数大于30%，尾气中氯甲烷的质量分数小于5%。

Methods: P-toluenesulfonic acid diethoxyphosphorylmethyl ester (4) was prepared from diethyl phosphate and paraformaldehyde by condensation and esterification.

以亚磷酸二乙酯和多聚甲醛经缩合、酯化得到对甲苯磺酸羟甲基磷酸二乙基酯(4)。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。