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二硝基酚

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The invention discloses a preparing method of bacillus alcaligenes strain Alcaligenes sp., CCTCC No.M206121 of degraded o-nitrophenol, which comprises the following steps: allocating inorganic salt culture medium with dibasic sodium phosphate, monobasic potassium phosphate, manganese sulfate, copperas, addex-magnesium, calcii chloridum, blue copperas, white copperas and hydrogen dioxide solution; adjusting pH value; sterilizing under high temperature; enriching bacterial; sampling from sludge; allocating suspending liquid with soil sample and inorganic salt; seeding into ortho-nitrophenol fresh organic salt culture medium with finite volume seeding quantity; keeping the temperature; culturing on shaker; getting enriched culture; separating and purifying enriched culture in LB solid culture medium.

本发明公开了一种降解邻硝基酚的产碱杆菌菌株及制备方法,产碱杆菌为Alcaligenes sp。,CCTCC No.M206121。其制备步骤是:首先是配制无机盐培养基,成分为磷酸氢二钠、磷酸二氢钾、硫酸锰、硫酸亚铁、硫酸镁、氯化钙、硫酸铜、硫酸锌和双蒸水,调pH值高压灭菌;其次是菌种的富集,从污泥中取样,将土样与无机盐培养基配制成悬浮液,将悬浮液以一定体积接种量接种到含邻硝基酚的新鲜无机盐培养基中,恒温,摇床培养,获富集培养物;第三是将富集培养物在LB固体培养基中分离和纯化。

Dinitrophenol, when applied to the leaf, reduced sucrose transport.

二硝基酚施于叶子时,减少了蔗糖的的运输。

Through indraught the way of table function to improve on the way of experiment in dynamic mensuration, DYNAMO software was used to process the data and simulate the inhibition phenomena of 2,4 dinitrophenol.

通过引进表函数方法,对动力学测定实验方法提出了改进,采用DYNAMO软件进行数据处理。对2,4-二硝基酚抑制现象进行模拟研究。

The catalyst, palladium supported with chitosan condensated with salicylaldehyde, was studied in hydrogenation ofα-octene, nitrobenzene, 4-nitrophenol and m-dinitrobenzene, it was active and good selectivity forα-octene and nitrobenzene, when the activation time is 90 min, the catalyst showed the best hydrogenation active.

壳聚糖缩水杨醛负载不同比例PdCl_2的催化剂对α-辛烯、硝基苯、4-硝基酚和间二硝基苯的催化性能进行了研究,结果表明该催化剂活化90 min时加氢催化活性最好,对α-辛烯,硝基苯的催化选择性在催化5 h时达到了100%。

Chemical corporations within this region may provide matching chemical products and raw materials such as citric acid, starch sugar, L-lactic acid, nitrochlorobenzene, paranitrophenol sodium salt sodium para-nitro phenolate, pphenylenediamine , sodiumhydroxide, benzene anhydride, carbonic acid propylene grease, polyacrylamide ,2.4- dinitrochlorobenzene, 2.4- dinitrosixchlorin, and sodium cyanide.

区内化工企业可配套提供柠檬酸、淀粉糖、 L —乳酸、硝基氯苯、对硝基酚钠、对苯二胺、烧碱、苯酐、碳酸丙烯脂、聚丙烯酰胺、2.4—二硝基氯化苯、2.4—二硝基6氯、氰化钠等化工产品或原料。

The chemical structure of the product was characterized by means of the melting point and IR. The results show that tetraethylammonium bromide which was used as a phase transfer catalyst in this reaction had optimization effect on the interfacial diffusive reaction of BTC and PNP. Higher concentration of sodium hydroxide, lower temperature and a higher dosage of BTC produced a small amount of 4-nitrophenyl chloroformate, while lower concentration of sodium hydroxide and a lower dosage of BTC made reaction incomplete, which affected the yield.

结果表明,在碳酸二(4-硝基苯基)酯合成中使用的相转移催化剂四乙基溴化铵对受界面扩散控制的BTC气与对硝基酚钠反应有良好的相转移催化效果;氢氧化钠质量分数较低时,酚钠盐向溶有BTC的油相扩散速度较小,较高时会产生氯甲酸对硝基苯酯;温度较低、BTC量较高时,会产生少量氯甲酸对硝基苯酯,BTC用量较低会使反应不完全,这些都影响着收率。

The method comprises following steps: taking diphenol and 3- trifluoromethyl- 4- chloronitrobenzene as raw material, salt precipitating for diphenol and potash, refluxing with water- containing toluene, reacting with 3- trifluoromethyl- 4- chloronitrobenzene and getting dinitro monomer; taking dinitro monomer, ferro powder and HCl as raw material, ethanol and water as disslovant for refluxing and ethanol recrystallization, getting fluorine- containing aromatic diamido monomer.

合成方法是以二酚与3-三氟甲基-4-氯硝基苯作原料,先将二酚与碳酸钾成盐,甲苯带水回流反应,然后与3-三氟甲基-4-氯硝基苯反应制得二硝基单体;再以二硝基单体,铁粉,HCl为原料,乙醇和水做溶剂,回流反应、乙醇重结晶,得到含氟芳香二胺基单体。

The simultaneous determination of m nitrophenol and p nitrophenol in binary mixtures had been studied with differential pulse voltammetry in the paper.

用微分脉冲伏安法同时测定了水样中含间硝基酚和对硝基酚的混合体系,在 0 1mol·l- 1 乙二胺 0 5mol·l- 1 氯化铵(pH =8 5 0 )底液中于- 0 5 0V和- 0 69V处出现两个灵敏度高且互不干扰的吸附波。

The effects of an uncoupler on the result of the treatment by activated sludge process and the yield of sludge were analyzed and studied using batch-sequential test method with 2,4-dinitrophenolas the uncoupler,and the mechanism of the generation of such effects was expounded.

简介: 以2,4_二硝基酚为解偶联剂,采用序批式实验分析研究了投加解偶联剂dNP对活性污泥法处理效果和污泥产率的影响,并阐述了这种影响产生的机理。

The effects of an uncoupler on the result of the treatment by activated sludge process and the yield of sludge were analyzed and studied using batch-sequential test method with 2,4-dinitrophenolas the uncoupler,and the mechanism of the generation of such effects was expounded.

以2,4_二硝基酚为解偶联剂,采用序批式实验分析研究了投加解偶联剂dNP对活性污泥法处理效果和污泥产率的影响,并阐述了这种影响产生的机理。

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