二硝基苯

It was concluded that the addition of Hydroquinone can accelerate the reaction drastically.

在一定范围内硝基苯降解率与对苯二酚的加入量成正比。

Some research and analysis on the reaction of 2,4-difluoronitrobenzene and nucleophilic reagent alcohol sodium (methyl alcohol ,ethyl alcohol, propyl alcohol, n-butyl alcohol, t-butyl alcohol, et hl) and the reaction choice of opposite -F in different solvent and conditions have done in this paper.

论文以2，4-二氟硝基苯为主要原料，研究了其与亲核试剂醇钠(甲醇、乙醇、丙醇、正丁醇、叔丁醇等)在不同溶剂中的反应情况，讨论了在几种代表性的溶剂——醇、四氢呋喃、苯、N，N-二甲基甲酰胺中亲核取代反应的情况，研究了温度、反应时间、亲核试剂、溶剂等条件对亲核取代反应的影响。

The synthetic organic chemicals, such as phenol, m cresol, phloroglucinol, phenylamine, 3,5 xylenol, p tertiary butyl phenol, nitrobenzene, tert butanol and chloral were oxidized in supercritical water system.

研究了超临界水氧化系统中合成有机化学品，如酚、间苯三酚、对叔丁基酚、间甲酚、3 ，5-二甲酚、苯胺、硝基苯、叔丁醇、三氯乙醛等的氧化作用。

The antioxidant activity of the dried extracts was characterized by peroxide value assay in lard and 1, 1-diphenyl-2-picryl hydrazyl radical method.

采用油脂过氧化值法和二苯三硝基苯肼自由基法研究了提取物的抗氧化活性。

The resin is prepared by swelling chlorine balls in a solvent such as nitrobenzene; adding catalyst to obtain polystyrene-divinylbenzene adsorptive resin; removing reaction mother solution; washing to remove residual solvent and catalyst; swelling; adding pyrane reagent to further react with chloromethyl residual on inner and outer surfaces of the resin to obtain the pyranyl modified adsorptive resin with the composite function.

该树脂的制备方法：将氯球溶胀于硝基苯等溶剂中，加入催化剂，得到聚苯乙烯-二乙烯苯吸附树脂；抽尽反应母液，洗去残留的溶剂和催化剂；溶胀，加入吡喃试剂与树脂内外表面残留氯甲基进一步反应，可制得吡喃基修饰复合功能吸附树脂。

The stereochemical structures of two new compounds, 5-(3-chlorophenyl)-2-furfur-aldehyde-N-4-methylphenyloxyacetylhydrazone and 5-(3-chlorophenyl)-2-furfuraldehyde-N-4-nitrophenyloxyacetylhydrazone, were determined by DPFGSE-NOE experiments performed in DMSO-d\-6 at 25 ℃ and variable-temperature ~1H NMR The ~1H chemical shifts of the compounds were completely assigned at 25 ℃ and 90

利用变温实验和DPFGSE NOE实验，确定了 5 (3 氯苯基) 2 呋喃甲醛 N 4 甲基苯氧乙酰腙和5 (3 氯苯基) 2 呋喃甲醛 N 4 硝基苯氧乙酰腙两个新化合物25 ℃时在二甲基亚砜中的空间构型，并对这两个新化合物在 25 ℃和 90 ℃时的质子的化学位移进行了全归属。

The calculations of harmonic vibrational frequencies with B3LYP/6-31Gtheoretically supported that o-dinitrosobenzene is the intermediate of "self-self"tautomeric rearrangement of benzofuroxan.

谐振动频率的B3LYP/6-31G计算还支持了邻二亚硝基苯为苯并氧化呋咱&自-自&互变重排反应的中间体。

The active stability and amount of the catalyst were studied and the influential factors ,such as solvent, temperature and pressure were investigated,and then the optimal process parameters were given∶Raney∶ethanol∶3,4-methylene-dioxy nitrobenzene is 0.15∶6∶1;the reaction temperature is 40℃;the hydrogenation pressure is 0.45～0.50 MPa;the stir velo...

对催化剂用量和活性稳定性进行了研究，讨论了溶剂用量、温度、压力等因素对加氢反应的影响。结果表明最佳工艺参数为：雷尼镍∶乙醇∶3，4 亚甲二氧基硝基苯=0.15∶6∶1，反应温度40℃，氢压0.45～0.50MPa，搅拌速度450r/min，反应至不再吸氢为止，产品收率在97%以上，纯度为98%。

The engine ran on a special mixture of methyl alcohol (63%), benzene (16%), ethanol (12%), acetone (4.4%), nitrobenzene (2.2%), avgas (2%), and ether (0.4%) with MW (methanol-water) injection for charge cooling and as an anti-detonant.

特别混合物燃料为引擎运转提供动力，甲醇(63%)，苯(16%)，对氨基苯甲酸二(12%)，丙酮(4.4%)，硝基苯(2.2%)，飞机用燃料(2%)和乙醚(0.4%)，以100W充电冷却射入并作为抗爆剂。

A chiral phase transfer catalyst, N-benzyl quinine bromide, was synthesized from natural chiral compound. And 2,5-bimethyl-4-(3-nitrobenzene)-1,4-bihydrogenation pyridine-3--4-methyl formate (viz. nitrendipine) was synthesized by this chiral phase transfer catalysis, and characterized by elemental analysis, infrared spectrum,1H nuclear magnetic resornace, and X-ray single-crystal diffraction.Key words: ammonium; chiral phase transfer catalyser; crystal structure

通过对天然手性物质进行修饰合成手性相转移催化剂N-苄基溴化奎宁，并对目标分子2，5-二甲基-4-(3-硝基苯)-1，4-二氢吡啶-3-甲酸乙酯-5-甲酸甲酯进行不对称催化合成，并通过红外光谱和核磁共振氢谱对化合物进行了表征，用X射线单晶衍射法测定了该化合物的晶体结构。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失