二硝基苯

Is a high-tech private enterprise, located in Laohekou City, Hubei Province, the main products are: 3,4 - dichloro-nitrobenzene; 3,4 - dichloroaniline; 2,4 - dimethyl-nitramine p; 2,4 - dimethylaniline; 2,6 - dimethyl-nitrobenzene; 2,6 - dimethylaniline; 3,5 - dimethyl-nitrobenzene; 3,5 - dimethyl Aniline; acrolein; Glutaraldehyde and other fine chemical products.

老河口联谊化工有限公司为一家高科技民营企业，位于湖北省老河口市，主要产品有：3，4-二氯硝基苯；3，4-二氯苯胺；2，4-二甲基硝基苯；2，4-二甲基苯胺；2，6-二甲基硝基苯；2，6-二甲基苯胺；3，5-二甲基硝基苯；3，5-二甲基苯胺；丙烯醛；戊二醛等精细化工产品。

First, the preparation of l,2-dichloro-4-nitrobenzene, which l-chloro-4-nitrobenzene reacted with chlorine in a self-designed chlorinator, in presence of Lewis acid catalyst,.was investigated. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the yield of l,2-diehloro-4-nitrobenzene was 83.26%.

为此，本文首先在自行设计的塔式氯化器中，以对硝基氯苯为原料，路易氏酸作催化剂，分子氯氯化合成3，4-二氯硝基苯(合成3-氯-4-氟-硝基苯的原料)，根据该氯化过程特征，利用正交试验设计方法结合单因素实验考察了有关因素对氯化过程的影响，优化得到了最佳的氯化工艺条件，3，4—二氯硝基苯的收率可达83.26％。

Chemical corporations within this region may provide matching chemical products and raw materials such as citric acid, starch sugar, L-lactic acid, nitrochlorobenzene, paranitrophenol sodium salt sodium para-nitro phenolate, pphenylenediamine , sodiumhydroxide, benzene anhydride, carbonic acid propylene grease, polyacrylamide ,2.4- dinitrochlorobenzene, 2.4- dinitrosixchlorin, and sodium cyanide.

区内化工企业可配套提供柠檬酸、淀粉糖、 L —乳酸、硝基氯苯、对硝基酚钠、对苯二胺、烧碱、苯酐、碳酸丙烯脂、聚丙烯酰胺、2.4—二硝基氯化苯、2.4—二硝基6氯、氰化钠等化工产品或原料。

The method comprises following steps: taking diphenol and 3- trifluoromethyl- 4- chloronitrobenzene as raw material, salt precipitating for diphenol and potash, refluxing with water- containing toluene, reacting with 3- trifluoromethyl- 4- chloronitrobenzene and getting dinitro monomer; taking dinitro monomer, ferro powder and HCl as raw material, ethanol and water as disslovant for refluxing and ethanol recrystallization, getting fluorine- containing aromatic diamido monomer.

合成方法是以二酚与3-三氟甲基-4-氯硝基苯作原料，先将二酚与碳酸钾成盐，甲苯带水回流反应，然后与3-三氟甲基-4-氯硝基苯反应制得二硝基单体；再以二硝基单体，铁粉，HCl为原料，乙醇和水做溶剂，回流反应、乙醇重结晶，得到含氟芳香二胺基单体。

Dinitro- benzene, all

二硝基苯，所有

Methods The inhibitory effects of Taurine (50 mmol·L-1) on glycolaldehyde (0.1 mmol·L-1) induced DNA damage in spleen lymphocytes of mice were studied in vitro using single cell gel electrophoresis,and 2,4-dinitrophenylhydrazine measurement was used to detect quantitatively the effects of Taurine on carbonyl compound contents in a reactive system.

采用单细胞凝胶电泳技术检测牛磺酸（50 mmol·L-1）对乙醇醛（GA， 0.1 mmol·L-1）所致小鼠脾淋巴细胞DNA损伤的抑制作用，并用2，4-二硝基苯肼法定量检测牛磺酸对反应体系中乙醇醛含量的影响，同时设乙醇醛阳性对照组和PBS阴性对照组。

Glyoxal in cosmetic sample was extracted by the solution of acetonitrile and water.

样品用乙腈－水溶液溶解，与2，4-二硝基苯肼在弱酸条件下衍生化反应，衍生物直接用HPLC测定，用外标法定量。

A sample (660 mg ) of an oligomeric protein of Mr 132,000 was treated with an excess of l-fluoro-2,4-dinitrobenzene (Sanger's reagent) under slightly alkaline conditions until the chemical reaction was complete.

一分子量为132，000的660mg寡聚蛋白样品，在弱硷性条件下用过量的1-氟-2，4-二硝基苯处理，直到反应完成。

The calculated results with B3LYP/6-31G-DFT show:(1)the molecular total energy of benzofuroxan is lower than that of o-dinitrosobenzene;(2)the activation energy(Ea+=51.0kJ/mol)of forward reaction that benzofuroxan isomerises into o-dinitrosobenzene,is in agreement with the experimental(58.6kJ/mol)provided by reference,and the activation energy(Ea-=4.6kJ/mol)of back-ward reaction is very small.It is concluded thereby that benzofuroxan is more stable than o-dinitrosobenzene.In addition,the corresponding ab initio calculations at the level of HF/3-21G,HF/6-31Gand MP2/6-31G//6-31G were completed,and it was found that the calculated results by B3LYP-DFT method are superior to those from ab initio calculation.

结果表明，苯并氧化呋咱的分子总能量比邻二亚硝基苯的低；由苯并氧化呋咱异构为邻二亚硝基苯的正向反应活化能（Ea+=51.0kJ/mol），与文献实测值（58.6kJ/mol）较接近，而其逆向反应活化能（Ea-=4.6kJ/mol）很小，从而揭示了苯并氧化呋咱比邻二亚硝基苯更稳定·此外，进行了HF/3-21G、HF/6-31G和MP2/6-31G//6-31G水平下相应的计算，发现B3LYP-DFT的结果较abinitio为优。

In this paper, we have initiated the relationship between molecular connectivity index and retention value in TLC for ten amino acids, eleven sulfides, six mercaptans and twenty 2,4-dinitrophenylhydrazones of aldehydes or ketones respectively.

把分子连接性指数法应用到10种氨基酸、11种硫醚、6种硫醇和20种醛、酮的2，4－二硝基苯腙薄层色谱保留值的相关性研究中。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失