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Hydroxy-2,3-dihydro-4-quinolone is synthesized by the basic material of 4-nitrochloro-benzene. It has investigated the routes, conditions and purifies methods in this paper, which provides bases to lucubration and industrialization. This study belongs to the field of medical intermediates.

本文以4-硝基氯苯和丙烯酸为基础原料合成6-羟基-2,3-二氢-4-喹啉酮,并对6-羟基-2,3-二氢-4-喹啉酮的合成条件和纯化方法进行了实验研究,为后续的深入研究和工业化生产提供依据。

According to the differences of the materials, there are many methods of synthesis for benzofuranol , such as the pyrocatechol method, the cyclohexanone method, the o-chlorophenol method, the nitrophenol method, the methoxy phenol method, and so on.

根据原料的不同,呋喃酚合成方法可分为邻苯二酚法、邻氯苯酚法、环己酮法、硝基苯酚法、愈创木酚法、邻异丙基酚法、羟基苯异酮法等,文章对前几种较常见的合成方法的原理及工艺进展进行了详细的综述,并展望了呋喃酚合成方法的发展趋势。

Resorcinol and 2-nitrodiphenylamine may be used as stabilizers.

间苯二酚和2-硝基二苯胺可用作安定剂。

The influence of temperature on the spectra and nonlinear optics properties of the 4--4'-aminoazobenzene compound Langmuir-Blodgettfilms were investigated using UV-visible absorption spectra and second harmonic generation technique.

采用紫外-可见吸收谱和二次谐波产生技术研究了温度对4-硝基-4'-氨基偶氮苯分子Langmuir—Blodgett单层和多层膜的光谱和二阶非线性光学特性的影响。

Xinquan HuTwo new chiral backbones R-- and S--2-amino-2"-hydroxy-4,4",6,6"-tetra methyl-1,1"-biphenyl were synthesized via nitration, diazotation/iodination, Ulhnann coupling, selective reduction, diazotation/hydrolysis, hydrogenation and resolution from 2,4-dimethyl-aniline in seven steps.

以2,4-二甲基苯胺为起始原料,经过硝化反应、重氮化碘代反应、Ullmann缩合反应、选择性双硝基单还原反应、重氮化水解反应、催化氢化反应和拆分,首次合成了--2-氨基-2'-羟基-4,4',6,6'-四甲基-1,1'-联苯和--2-氨基-2'-羟基-4,4',6,6'-四甲基-1,1'-联苯两个对映体。

In this dissertation, electrophilic reactions of Nitrosonium with imines, aza-Diels-Alder reactions of N-arylimines with a variety of electron rich olefinic compounds induced by NO~+, and photoreactions of N-nitrosodiphenylamine with aromatic amines were studied.

本文研究了:(1)NO~+与亚胺双健发生的亲电反应;(2)NO~+引发的芳香亚胺和富电子碳碳双键作为亲二烯体的氮杂Diels-Alder反应,高选择性地得到了一系列四氢喹啉的衍生物;(3)N—亚硝基二苯胺与芳香胺发生光化学反应得到了一系列偶氮苯类化合物。

The charges on the substituents affected OWF〓 greatly for some azobenzene derivatives, pyridone derivatives, nitrodiphenylamine derivatives, some reactive dyes and 1, 4-diamino anthraquinone derivatives, in this instance, OWF〓 changed linearly with the change of the charges.

2给电子取代基或吸电子取代基的电荷对OWF〓有较大的影响,OWF〓随电荷的变化而线性变化,如某些偶氮苯衍生物、吡啶酮类染料母体、硝基二苯胺类化合物、偶合组分和重氮组分之间夹角α变化不大的活性染料、1,4—二氨基蒽醌衍生物等。

A new monomer,4-hexanoxyl-4′-undecylene-[10]-acyloxyazobenzene was synthesized using the main materials:phenol,underlenic acid,1-bromo- n -hexane, p -nitrophenol,thionyl chloride,by the substitution,reduction,couping and diazotization methods.A new polymer was prepared by hydrosilation reaction of poly (methylhy-drosiloxane) with the monomer.

以苯酚、十一烯酸、正溴己烷、对硝基苯酚和二氯亚砜为主要原料,通过取代、还原、重氮化和偶合等反应,合成了一种新的液晶单体 4-己氧基-4′-十一烯-[10]-酰氧基偶氮苯,并与聚通过硅氢加成生成一种新的高分子液晶。

Experimental results showed that aerosol created by 1,3,5-trimethylbenzene photooxidation can be classify with five distinct chemical particle classes, the predominant components of these five particles are aromatic aldehyde, phenol, nitrophenol and carboxylic acid compounds.

利用该算法对OH自由基启动1,3,5-三甲苯光氧化形成的二次有机气溶胶单粒子质谱数据进行了聚类分析,在得到的五个聚类中包含了芳香醛、酚类化合物、硝基酚和羧酸等重要的光氧化产物,为研究苯系物光氧化机理提供了新的信息。

Series of ternary and quadruple doping complexes of europium with benzoic acid ,p-aminobenzoic acid,phthalic acid , m-phthalic acid, and 1,10-phenanthroline were synthesized.

合成了铕与以苯甲酸、对氨基苯甲酸、对硝基苯甲酸、邻苯二甲酸和间苯二甲酸等为第一配体,邻菲咯啉为第二配体的掺杂配合物。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。