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A process for preparing alkylene glycols including reacting an alkylene oxide with water in the presence of a combination of additives and an anion exchange resin, wherein the combination of additives comprises carbon dioxide and an organic or inorganic base provided in an amount sufficient to maintain a pH of the reaction mixture between about 5.0 and 9.0, with the proviso that, when the base is bicarbonate or carbonate, then the anion exchange resin is a trimethyl benzyl ammonium anion exchange resin.

制备亚烷基二醇的方法,包括让烯化氧与水在添加剂组合和阴离子交换树脂存在下进行反应,其中添加剂组合包括二氧化碳和以足以保持反应混合物的pH值在约5.0和9.0之间的量提供的有机或无机碱,前提条件是当碱是碳酸氢盐或碳酸盐时,阴离子交换树脂是三甲基苄基铵阴离子交换树脂。

Blood samples from 23 Huacaya alpacas ,3 males and 20 females ,were used to study chromosome karyotype ,so as to provide some effective cytogenetics basis for the selectioiymprovement by crossing and disease diagnosis of alpacas ,and genetic mechanisms of sex determination. Peripheral blood lymphocyte culture was used to prepare chromosome. Methods of trypsase-EDTA and BSG (Barium hydroxide / Saline / Giemsa)were used for G-banding and C-banding respectively . The results showed as follows:Firstly , the number of diploid chromosomes was in the alpacas 2n=74,with the karyotype 74, XY and 74, XX for males and females respectively.

为了从选种、杂交改良、疾病诊断以及性别决定的遗传机制等方面为羊驼的繁育与推广提供更为有效的细胞遗传学资料,本试验采用外周血淋巴细胞培养法制备染色体,分析了23只胡阿基亚型羊驼(Huacaya alpaca,雌20只,雄3只)的染色体及其核型,并通过BSG法(Barium hydroxide/Saline/Giemsa,氢氧化钡-盐溶液-吉姆萨,也即Sumner BSG法)与胰酶-EDTA法分别对羊驼的C-分带和G-分带进行分析,结果表明:(1)羊驼二倍体染色体数目为2n=74,雄性羊驼核型为74,XY;雌性羊驼核型为74,XX。

Stable pharmaceutical compositions containing 8-chloro-6,11-dihydro-11-(4-piperidylidene)-5H-benzo[5,6] cycloheptic [1,2-b] pyridine and a DCL protective amount of a pharmaceutically acceptable basic salt such as calcium dibasic phosphate and an amount of at least one disintegrant, preferably two disintegrates such as microcrystalline cellulose and starch sufficient to provide dissolution of at least about 80% by weight of the pharmaceutical composition in about 45 minutes and suitable for oral administration to treat allergic reactions in mammals such as man are disclosed.

本发明公开了含有8-氯-6,11-二氢-11-(4-亚哌啶基)-5H-苯并[5,6]环庚三烯并[1,2-b]吡啶和DCL保护量的可药用碱性盐如磷酸氢钙以及其含量足以使至少约80%的药物组合物在约45分钟内溶解的至少一种崩解剂、优选两种崩解剂如微晶纤维素和淀粉并且适于口服给药以治疗哺乳动物、例如人的过敏反应的稳定的药物组合物。

The combination of ion-pair extraction technology with reversed-phase ion-pair chromatography method provide a effective inspection measure for the sulfonates in water.

样品的四丁基溴化铵和二氯甲烷离子对萃取方法与反相离子对色谱分离联用,为水体中芳香族磺酸盐的检测提供了可靠的监测手段。

Resorcin biodegradation was studied by acclimated anaerobic sludge with sucrose,glucose,butyrate and ethanol as co-metabolism substrates in ASBR reactor.

分别用蔗糖、葡萄糖、丁酸盐和乙醇作为驯化好的厌氧污泥的共代谢基质,在厌氧序批式反应器中对间苯二酚的降解进行研究。

P-π conjugated polyamic acid was synthesized by the poly-condensation of benzoguanamine and pyromellitic dianhydride under microwave irradiation. Then PAA was grafted with different side-chain containing azobenzol groups through azo coupling reaction.

选取苯代三聚氰胺和均苯四酸二酐为单体进行微波辐射溶液聚合反应,所得的聚酰胺酸与对位取代基不同的苯胺重氮盐偶合接枝,从而合成了一系列新的具有三阶非线性光学活性的侧链型聚合物。

This paper deals with making stop bleeding sponge with dried small shrimps. Firstly breaking away with inorganic salt and proteir in the dried small shrimps with acid and NaOH, secondly, taking off vinyl-in the chitin with 50% NaOH, temperature is 110 ℃. the last, reacting with chitosamine and PVA-124 make stop bleeding sponge were produced, catalyst is PdCl 2. The sponge film and sparkce is setatisfaction.

用虾壳经除盐,去蛋白处理后,用50%的NaOH溶液在110℃的温度下脱乙酰基制备壳聚糖;以1∶9的稀醋酸溶作溶剂,氯化钯作催化剂,甲苯二异氰酸酯作发泡剂、交联剂,使壳聚糖与PVA-124进行交联成膜,发泡用氨水洗成中性后在80℃的红外灯烘箱下烘干,制得止血海棉

On the basis of investigating the developments of inorganic mesoporous material's syntheses and applications, mesostructured tin oxide, bismuth oxychloride, lead sulfide, bismuth sulfide, titanium phosphate and zinc phosphate were synthesized by Sol-Gel and hydrothermal techniques, employing the neutral surfactant organic amine and anion surfactant alkyl sulfonate as templates.

中文题名非硅基介孔材料的合成与表征副题名外文题名论文作者周书喜导师李健民学科专业物理化学研究领域\研究方向学位级别博士学位授予单位中国科学技术大学学位授予日期2003 论文页码总数92页关键词介孔材料介孔分子筛馆藏号BSLW /2003 /O643.3 /50 在对无机介孔材料的合成、应用等方面的发展现状进行了充分调研的基础上,本文运用溶胶一凝胶法、水热法等合成手段,选用中性表面活性剂有机伯胺和阴离子表面活性剂烷基磺酸盐为模板,制备了二氧化锡、氯氧化铋、硫化铅、硫化铋、磷酸钛、磷酸锌等无机介孔材料。

Solid complexes of rare earth picrates with the ligand 2,6-bis(benzimidazol-2-yl)pyridine have been synthesized and characterized by elemental analysis, IR and electronic spectra. The crystal and molecular structures of the complex [CeL22]·(CH3OH)3 have been determined by single crystal X-ray diffraction.

合成了稀土苦味酸盐与配体2,6-二(2-苯并咪唑基)吡啶的配合物,通过元素分析、红外光谱及电子光谱对配体及配合物进行了表征,并用X射线单晶衍射测定了配合物[CeL22]·(CH3OH)3的晶体结构。

Moreover, the protein-free spreading-free spreading technique, involvingbenzyldimethyl-alkyammonium bromide and the denaturing agent formamide, wasestablished. With very low DNA concentration, the fully extended DNA samples for linearDNA can be prepared.

采用Sephadex色谱柱分离,保温稀释的DNA溶液,不仅可除去DNA链上吸附的盐,而且可使盘绕一起的DNA链部分展开;在此基础上,通过采用苯二甲基辛基溴化胺-甲酰胺微量展层技术,可使纳克级DNA完全展开到云母基底上。

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With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐,因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。

Closes the eye, the deep breathing, all no longer are the dreams as if......

关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。