二盐基的

Alkylamine reaction with dialkyl cyanodithioiminocarbonate was catalyzed by quaternary ammonium salts at room temperature to yield 3-alkylamine-5-amino-1,2,4-triazole in good quality and high yields. After imidization and reaction with an α,β-unsaturated acid derivative, the reaction intermediate was hydrolyzed in the presence of a Lewis acid to obtain the target product.

烷基胺与氰基亚胺硫代二甲酯在季氨盐催化作用下得到质量好、收率高的3-烷氨基-5-氨基-1，2，4-三氮唑，进一步经过亚胺中间体并与α，β-不饱和酸酯作用后，中间产物在Lewis酸催化作用下水解得到三唑嘧啶酮。

CA-CTSs including N,O-carboxymethyl chitosan,N,O-1-carboxyethyl chitosan (N,O-1-CEC),N,O-2-carboxyethyl chltosan(N,O-2-CEC),N-carboxymethyl chitosan and N-1-carboxyethyl chitosan(N-1-CEC) are quaternized using active quaternary salts prepared in laboratory.5 series including 25 kinds amphoteric chitosans characterized with polymeric ampholyte,in which 24 kinds are synthesized firstly,are obtained, 2-Hydroxypropyl dimethylbenzyl ammonium N,O-(1-carboxyethyl) chitosan chloride (GDMBA-N,O-1-CEC) is hydrolyzed into serial low molecular weight GDMBA-N, O-1-CEC with acid as catalyst and microwave as assistant instrumentality innovately.

以合成的活性季铵盐改性了N，O-羧甲基壳聚糖、N，O-1-羧乙基壳聚糖(N，O-1-CEC)、N，O-2-羧乙基壳聚糖(N，O-2-CEC)、N-羧甲基壳聚糖和N-1-羧乙基壳聚糖(N-1-CEC)等羧烷基壳聚糖，得到5个系列25种具有两性高分子电解质特征的新季铵化羧烷基壳聚糖，其中24种为首次合成；创新提出以微波辅助酸催化的方法催化2-羟丙基二甲基苄基-N，O-(1-羧乙基)壳聚糖氯化铵(GDMBA-N，O-1-CEC)水解，得到了低分子量的GDMBA-N，O-1-CEC。

Further research indicates that the polymerization of HEMA was induced by the disproportionation of dihydropyridinium. From results above, the mechanism of Gluma as a desensitizer could be proposed as follows.

发现戊二醛与牛血清蛋白之间的反应可以使水溶液中的HEMA聚合，进一步研究发现HEMA的聚合与二氢吡啶盐歧化过程所产生的自由基有关。

The load carrying capacity and antiwear property of S,P containing benzotriazole derivative (BM 3) were evaluated using a four ball test machine,and compared with those of zinc salt di(T 202 ) and amine salt of complex ester thiophosphate (T 307 ). The antiwear mechanism of BM 3 were studied by investigating the chemical states and the mass fraction of elements on the rubbed surfaces using X ray photoelectron spectroscopy and electron probe microanalysis and the thermal decomposition products using gas chromatography mass spectrograph.

在四球机上对照评价了含硫、磷苯并三氮唑衍生物（BM－3）和二丁辛基二硫代磷酸锌（T202）及硫磷酸复酯胺盐（T307）的承载能力和抗磨性能，用X射线光电子能谱仪和电子探针微分析仪等对磨斑表面元素N，S和P的存在形式及表面膜的组成进行了分析，用气相色谱－质谱联用仪对BM－3的热分解产物进行了分析，并且还对其极压抗磨作用机理作了探讨。

Ten kinds of metal and three kinds of organic templates, including ethylenediamine, 1,4-butylenediamine and pyrazine were used in the synthesis of metal phosphonate coordination polymers.

在所合成的16种金属有机膦酸盐配位聚合物中，有机配体为2-羟基乙酰基膦酸，用于配位的金属离子共10种，模板剂3种分别为乙二胺(en，1，4-丁二胺，哌嗪。

These chemical shifts in the aromatic region of the resulting nucleophilic adduct 2-F were consistent with the counterparts of 9,10-dihydro-9-methoxy-9-(4-methoxyphenyl)-10-methylacridine, 17b which was proven to be the adduct of the 9-phenyl acridinium salt formed with an excess of MeOH (Figure S7 in Supporting Information).

在最终的亲核加成化合物2-F的芳香族区中的这些化学位移与9，10二氢-9-甲氧基-9-(4甲氧基苯基)-10-甲基吖啶的对应物是一致的，17b 这被证明是与过量的MeOH形成的9-苯基吖啶盐的加成化合物（支持信息中的图S7）。

The complexation behavior of these compounds with linear or aromatic dicarboxylate was investigated by the means of absorption, emission spectra,〓H-NMR and molecular dynamics.

结果显示，二羧酸盐阴离子与双链萘基脲／硫脲哌嗪化合物发生络合形成新的物种导致双链萘基脲／硫脲哌嗪化合物的吸收和荧光光谱行为的变化。

Double chain naphthyurea/thiourea piperazine derivatives could act as a fluorescent chemosensor not for aromatic dicarboxylate but for linear dicarboxylate especially for pimelate anion.

双链萘脲基或硫脲基哌嗪化合物与直链二羧酸盐络合具有较高的稳定常数和1∶1的化学计量比，两者通过六个氢键形成双点结合的络合物。

The largest chemical shifts were observed for the proton 1.48 ppm adjacent to the central pyridinium ring and para-protons 1.47 ppm with respect to the nitrogen of pyridinium.

在最终的亲核加成化合物2-F的芳香族区中的这些化学位移与9，10二氢-9-甲氧基-9-(4甲氧基苯基)-10-甲基吖啶的对应物是一致的，17b 这被证明是与过量的MeOH形成的9-苯基吖啶盐的加成化合物（支持信息中的图S7）。

An unusual substitution of 5-fluorouracils by the reaction of lithium salts of 1,3-dialkyl-5-fluorouracil with benzyl bromide is described.

1，3-二烷基-5-氟尿嘧啶的锂盐与苄基溴进行苄基化反应时产生了异常的反应结果。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。