二甲酸

Methods: The pesticides were extracted with acetone and dichloromethane. The extract was warmed with water at 80℃, circumrotated and evaporated until it was nearly dry. Then it was cleaned-up by Envi-Carb column and Sep-Pak-NH2 column.

本法采用丙酮、二氯甲烷提取，40℃水浴旋转蒸发近干，以Envi-Carb柱和Sep-Pak-NH2柱净化，以气相色谱－质谱选择离子监测方式分析检测有机磷、有机氯、氨基甲酸酯和除草剂等32种农药残留。

This article discussed the influence factors of productivity of formic acid such as the mol ratio of sodium formate and phosphoric acid, the addition of phosphorus pentoxide, vapouring temperature.

对原料配比、五氧化二磷加入量、蒸馏温度对甲酸产品浓度、产率的影响进行了实验。

Formic acid, hexyl ester and Z-3-Hexen-1-ol were preliminarily confirmed to be the important substances for attracting woolly apple aphid, but 4-methyl-1, 3-pentadiene and Z-3-hexen-1-ol, acetate were not.

初步确定，E-3-己烯－1-醇、甲酸己酯可能是对苹果绵蚜有较强引诱作用的重要物质；4-甲基－1，3-戊二烯、乙酸叶醇酯不是引诱苹果绵蚜的物质。

A new organic compound:N,N'-bis(1,10-phenanthroline-2-formacyl)-4,4'-diamino-diphenylmethane was synthesized via oxidation,esterification,substitution,hydrolysis, amidation of 1,10-phenanthroline as the starting material with chemical reagents (hydrogen peroxide,benzoyl chloride,potassium cyanide,sodium hydroxide solution,4,4'-diamino-diphenylmethane).

以邻菲啰啉为起始原料，与双氧水反应合成邻菲啰啉-N-氧化物，接着与苯甲酰氯、氰化钾、NaOH水溶液一一反应合成中间体邻菲啰啉-2-甲酸，再与4，4′-二氨基苯基甲烷进行酰胺化反应合成目标产物。

Methyl-l, 3-oxazine-2,4-dione are prepared from ethyl acetoacetate and ethyl carbamate at 140 for 6h, catalysted by zinc acetate, giving to 48.8% yields which is 33% more than the literature value.

选用醋酸锌作催化剂，使乙酰乙酸乙酯与氨基甲酸酯在140℃反应6h，合成6-甲基-1，3-噁嗪-2，4-二酮，产率达48.8％，较文献报道值高出了33％。

The nano-ionic liquid containing metal complex could be an effective catalyst for oxidative carbonylation of amines to carbamates and disubstituted ureas and for synthesis of unsymmetric ureas from amines and nitrobenzene, in which turn over frequencies exceeded 10000mol/mol/h.

以该系列纳米离子液体为催化剂高效的实现了胺类化合物催化氧化羰化制备氨基甲酸酯和二取代脲（转化频率＞10000mol/mol/h）以及胺与硝基苯通过一氧化碳羰化制备不对称脲的过程。

In order to solve the problem of produced waternot attaining quality standard and decrease pro cessing costs, the anthors synthesize a new type water processing chemicals and make quali tative analysis and effect test to the produot.

为了解决目前一些油田采出水处理达不到注水水质标准和降低处理费用的问题，我们合成了一种新型水处理药剂——二硫代氨基甲酸盐，并对合成的产品进行了定性分析和效果试验。

At present the company mainly engaged in natural fatty alcohol products (C8-10, C12-14, C16-18 and various pure distillate), fatty alcohol polyoxyethylene ether, the basic sub-nonyl polyoxyethylene ether, polyethylene glycol and penetrant series over 100 varieties and zinc powder Insurance Law, Insurance Law sodium powder, hair bleaching agent, carved white block , carved white zinc, zinc oxide, zinc borate, sulfur dioxide and so on.

目前公司主要经营产品有天然脂肪醇（C8-10、C12-14、C16-18及各种纯馏分）、脂肪醇聚氧乙烯醚（AEO、OS及平平加O）、壬基本分聚氧乙烯醚、聚乙二醇和渗透剂系列100多个品种和锌粉法保险粉、甲酸钠法保险粉、漂毛剂、雕白块、雕白锌、氧化锌、硼酸锌、二氧化硫等。

The protein level of NF-kB in nucleus peaks at 8h after stimulating with LBP (200μg/ml). In addition, PDTC, an inhibitor of NF-kB, whose effective concentration for NF-kB inhibition without any toxicity on cells is up to 100μmol/L, can significantly block NO production induced by LBP.

另外，NF-κB抑制剂吡咯烷二硫代氨基甲酸盐作用于RAW264.7细胞90min，然后加入200μg／ml剂量的枸杞多糖对巨噬细胞进行刺激，发现PDTC在各个时间点(6、12、18、24h)都明显抑制枸杞多糖对巨噬细胞释放NO的诱导作用。

By one-pot method,with p-toluenesulfonic acid as catalyst,trimethyl orthoformate and cyclohexanone reacted in isopropanol to form 1,1-dimethoxycyclohexane,which,without separation,reacted furthur with isopropanol to form the title compound by distilling off the low-boiling product.

用一锅法，以对甲苯磺酸为催化剂，在异丙醇中原甲酸三甲酯与环己酮反应，其产物不经分离直接与异丙醇交换，得到1，1-二异丙氧基环己烷。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。