二甲酸

As a foundation raw material, propylene oxide was reacted with phosgene use the process tradition method that mean low temperature and high temperature two phosgenation sections to synthesis bis chloroformate .

以聚氧化丙烯为基础原料，与光气在合适的溶剂下经过传统的低温、高温两段法光气化反应合成氯甲酸二酯，然后再与芳香多胺在合适的溶剂和催化剂下反应，脱除溶剂后得到一种新型的端胺基聚醚。

After acid hydrolysis of urine, primary amino acids were derivatized with ortho-phthaldialdehyde and removed from the sample by use of silica gel, followed by devivatized of hydroxyproline with 9-fluorenylmethyl chloroformate, and then injected into a C8 reversed-phase column.

采用邻苯二甲醛和芴甲基氯甲酸酯两个衍生剂，先后处理尿标本，以国产C8柱为固定相，在醋酸钠缓冲液中加入23%的乙腈作为洗脱液，3，4-脱氢脯氨酸作为内标。

RESULTS: Sixteen compounds, ursolic acid (1), indole-3-carboxaldehyde (2), indole-3-carboxylic acid (3), p-coumaric acid (4), azelaic acid (5), N-trans-feruloyl tyramine (6), blumenol A (7), 2-hydroxy-3-methylanthraquinone (8), rubiadin l-methyl ether (9), rubiadin (10), quercetin (11), luteolin (12), chrysoeriol 6-C-β-boivinopyranosyl-7-O-β-glucopyranoside (13), alternanthin (14), stigmasta-5, 22-dien-3β-ol (15), and α-spinasterol (16) were obtained from the EtOAc extract of Alternanthera philoxeroides.

结果：得到并鉴定了16个化合物，分别为乌苏酸(1)、吲哚-3-甲醛(2)、吲哚-3-甲酸(3)、对-香豆酸(4)、壬二酸(5)、N-反式阿魏酰基酪胺(6)、布卢姆醇A(7)、2-羟基-3-甲基蒽醌(8)、甲基异茜草素-1-甲醚(9)、甲基异茜草素(10)、槲皮素(11)、木犀草素(12)、柯伊利素-6-C-β-波伊文糖基-7-O-β-吡喃葡萄糖苷(13)、莲子草素(14)、豆甾醇(15)和α-菠甾醇(16)。

The synthesis of 4,5,7-trichloroquinoline makes use of ethyl orthoformate, cyanoacetic ester and 3,5-dichloroaniline as the raw materials. The synthesis is completed by four steps: condensation, cyclization, hydrolyzation and chlorination. Several conditions concerned in the process are studied, the whole yield of 4,5,7-trichloroquinoline is about 53%, and the purity of it is about 96%. All the products are testified by IR, NMR and HPLC.

介绍了以3，5-二氯苯胺、原甲酸三乙酯和氰乙酸乙酯为原料，经过缩合、成环、水解和氯代4步反应制备4，5，7-三氯喹啉的方法，对相关的试验条件进行了考察，通过红外光谱、核磁共振谱和液相色谱对4，5，7-三氯喹啉的结构和纯度进行表征和测定，试验结果为4，5，7-三氯喹啉的纯度大于96%，总收率达到53%。

Omeprazole racemate was resolved respectively by simulated moving bed chromatography and batch chromatography with the coated cellulose triphenylcarbamate as chiral stationary phase and ethanol containing 0.1% diethylamine as mobile phase.

用纤维素三苯基氨基甲酸酯涂敷型手性固定相和含0.1%二乙胺的乙醇溶液，研究了模拟移动床色谱和间歇色谱对奥美拉唑对映体的拆分。

A catalyst for obtaining pyromellitic dianhyride by catalytic gaseous phase oxidation from durene are developmented.

开发了一种由均四甲苯空气气相氧化制均苯四甲酸二酐过程所需的催化剂，该催化剂活性组分为Ce-Mo-Ti-V。

The glycidol is protected by ethyl vinyl ether first to form 2,3-epoxypropyl-1-ethoxyethyl ether, then polymerized or copolymerized with EO by initiation with the mixture of diphenylmethylpotassium and triethylene glycol to give the well-defined poly.

得到的聚合物用甲酸水解去保护，并在二氧六环和甲醇的混合溶剂中用氢氧化钾溶液皂化后，得到了聚合物链的侧端挂有羟甲基官能团的线形聚醚linear Polyglycidol和poly。

Allantoin was synthesized from glyoxylic and urea as raw materials using organic acid such as formic acid,oxalic acid and organic sulfonic,and one or two of organic acids such as hydrchloric acid,sulfuric acid and acetic acid catalyst.

以乙醛酸和尿素为原料，有机酸(如甲酸、乙二酸、有机磺酸等)、无机酸(如盐酸、硫酸、磷酸、醋酸等中的一种或两种)作催化剂合成了尿囊素产品。

Aim To study the relationship between the structures of a series of 4,4-diaryl-3-butenyl derivatives of nipecotic acid and guvacine and their inhibition activity of the γ-aminobutyric aciduptake.

目的研究3-哌啶甲酸和四氢烟酸的4，4-二芳基-3-丁烯衍生物结构和对γ-氨基丁酸摄取抑制活性之间的关系。

These values indicate that the CoMFA model derived is significant and might have a good prediction for the inhibition activity of 4,4-diaryl-3-butenyl derivatives of nipecotic acid and guvacine compounds.

结论这些数值表明所得的CoMFA模型有实际意义，并且对3-哌啶甲酸和四氢烟酸的4，4-二芳基-3-丁烯衍生物抑制活性具有较好的预测能力。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。