二甲酸

This catalyst was applied for the liquid phase oxidation of glyoxal to glyoxylic acid.

研究结果表明，V_2O_5/C催化剂对乙二醛的氧化具有良好的催化活性和乙醛酸选择性，反应过程中无需控制溶液pH值即可得到乙醛酸，乙醛酸在V_2O_5/C催化剂作用下不存在过度氧化，乙二醛的氧化产物主要是甲酸和乙醛酸，它们是一平行反应。

Glyoxylic acid can be obtained without pH regulation during the reaction, and glyoxylic acid can not be oxidize...

研究结果表明，乙二醛的催化氧化副产物甲酸对乙二醛和乙醛酸的分析没有干扰。

Objective To evaluate and compare the ability to detect tumor by bis (N-ethoxy-N-ethyl dithiocarbamato) nitrido 99mTc [ 99mTcN 2 ] and 99mTc hexakis-2- methoxyisobutyl isonitrile [ 99mTc-MIBI ].

目的 探讨99mTc-氮-二(N-乙基-N-乙氧基二硫代氨基甲酸盐)[99mTcN2]应用于肿瘤诊断的可能性并与99mTc-甲氧基异丁基异腈(99mTc-MIBI)肿瘤模型显像进行比较。

Triethyl orthoformate, industry 97 37%; diethyl malonate, industry 98%; acetic anhydride, reagent 97%.

原甲酸三乙酯，工业97 37%；丙二酸二乙酯，工业98%；醋酸酐，试剂97%。

For the first time, enantiomers of C2-symmetric 1,1 -spirobiindane-7,7'-diol were resolved with crude menthyl chloroformate by phase-transfer catalysis in the presence of tetrabutylammonium bromide. The reaction was carried out at 0℃-rt. The diastereomers of SPINOL bis-menthyl carbonate can be separated by simple crystallization using alcohol. The hydrolysis of the diastereomers was carried out via aqueous NaOH/EtOH solution.

首次通过相转移催化的方法对螺双二氢茚二酚进行了有效的拆分，用L--氯甲酸薄荷醇酯做拆分剂，以四丁基溴化铵为催化剂在0℃-室温下进行酯化反应生成非对映体衍生物，以乙醇作溶剂，通过重结晶的方法分离衍生物，在水-乙醇混合溶剂条件下，用强碱NaOH或KOH分别水解，制得相应的光学纯度大于99%ee的两个异构体SPINOL，其中总收率：--SPINOL，78.2%；--SPINOL，80.6%。

By the polycondensation of amino acid 5-fluorouracil -1, 3-dipropyl esters with bis (2-chloroethyl) phos- phoramidic dichloride in the presence of 〓 or in vacuo, ten new polymers containing 5- fluorouracil, nitrogen mustard and amino acid were synthesized.

将1，3-双-5-氟尿嘧啶与二氯膦甲酸乙酯或二氯膦乙酸乙酯在DMF中反应制备得到20个三元共聚物，体外抗肿瘤试验表明：含有甘氨酸、缬氨酸、苯丙氨酸和酪氨酸的聚合加显示了一定的选择性，并且分析讨论了生物活性与结构之间的关系。

Trace Hg in aqueous solution was preconcentrated by on-line formation of mercury diethyldithiocarbamate complex and adsorption of the resulting neutral complex on the inner walls of a PTFE knotted reactor.

天然水样中痕量的Hg通过FI在线形成中性的汞-二乙基二氨基甲酸络合物并吸附在聚四氟乙烯管编制的KR的内壁上实现预富集。

The synthesis of poly was based on 4,4′-oxydianiline and pyromellitic dianhydride.

本研究首先经由二胺基二苯基醚(4，4′-ODA)单体和苯均四甲酸二酐单体，反应合成聚醯胺酸前驱物。

Based on 26B4APBN monomer, polyamic acid was obtained by polymerization with pyromellitic dianhydride, and further imidized into polyimide film by heating process.

由二胺单体和均苯四甲酸二酐进行聚合得到26B4APBN/PMDA聚酰胺酸，再经热亚胺化得到聚酰亚胺薄膜；测试了该薄膜的接触角，讨论了单体分子结构对聚合物接触角的影响。

Reduction of N-substituted-4-nitrophthalimides(1)to the corresponding amines(2)was performed in hydrochloric acid at 40 ℃ using stannous chloride as reduction agent, yielding produc...

氮气保护条件下，2与乙醇在固体光气作用下生成(2 取代 1，3 二酮 2，3 二氢 1H 异吲哚 5 )氨基甲酸乙酯(3)，3的产率为67%～92%。各化合物的结构均经1H NMR、IR、元素分析和FAB MS证实。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。