二甲酸

Pentanediol dithiophene ester was synthesized by means of alcoholysis reaction using 2,4-Pentanediol and Aroly chloride as raw materials, and 1H NMR spectrum was characterized and it can not be explained.

以2，4-戊二醇和芳酰氯为原料，通过醇解反应合成了一种新的内给电子体化合物二(2-噻吩甲酸)-2，4-戊二醇酯，表征其1H-NMR谱，发现化学位移在2附近出现了三组亚甲基峰，无法解释。

N,N-Dimethyl dodecylamine was synthesized with dodecyl amine, formic acid and formaldehyde as raw material in this article.

以十二胺、甲酸和甲醛为原料，合成了N，N-二甲基十二烷基叔胺。

Dimethylhexane-1,6-dimethyleurethane is the key material for preparation of 1,6-hexamethylene diisocyanate by non-phosgene route. Our work mainly focuses on the study of the catalytic performances of metal oxysalts and metal oxides for the ammonolysis of DMC to HDU-M. Experiment effect showed the ammonolysis was omposed by two steps, in which the first step was easier to occur than the second.

中文摘要六亚甲基-1，6-二氨基甲酸甲酯是非光气合成六亚甲基二异氰酸酯的关键原料，本文主要对金属含氧酸盐和金属氧化物这两类用于碳酸二甲酯胺解合成HDU-M 的催化剂进行了初步研究并优化了工艺条件。

During the manufacturing of the critical intermediate cephalosporin nucleus --7-amino-3-chloro-cephalosporanic acid diphenylmethyl ester hydrochloride salt, first the feasibility of the one-pot synthetic route of open loop, closed loop and ozonization when chlorine is passed over is qualified by experiments. Then the critical factors that will influence this reaction are studied as follows: the mol ratio of triphenyl phosphite and Diphenylmethyl 3-hydroxy-7-phenylacetaminoceph-3-em-4-carboxylate-l-oxide is four to one; the quantity of the stablizer should be at least more than two to one. The temperature of the system must be 25℃ when chlorine is passed over so that the hydrochloride can be precipitated to obtain cephalosporin nucleus of cefaclor--7-amino-3-chloro-cephalosporanic acid diphenylmethyl ester hydrochloride salt.

在制备关键中间体头孢母核7-氨基-3-氯头孢烷酸二苯甲酯盐酸盐时，先通过实验验证把开环、闭环、臭氧化三步在通入氯气时并为一锅煮的合成路线的可行性之外，又研究了影响该反应的几个重要因素：亚磷酸三苯酯与3-羟基-7-头孢烷-5-亚砜-2-甲酸二苯甲酯的摩尔比为4：1；稳定剂2-甲基-2-丁烯的用量至少大于2：1，通入氯化氢气体时体系温度在25℃时盐酸盐则能够顺利析出，获得头孢克洛的头孢母核—7-氨基-3-氯头孢烷酸二苯甲酯盐酸盐。

Carbon disulfide, dialkylamine, antimony trioxide have been used to synthesize the other organic antimony compounds-dialkyldithiocarbamate. The optimal technological conditions and purificating method have been studied in detail.

以二硫化碳、二元仲胺、三氧化二锑为原料合成了结构为Sb-〓的另一类含Sb-S键的有机锑化合物，通过大量的实验探索，详细研究了各种二烷基二硫代氨基甲酸锑的最佳合成工艺条件及产品的提纯方法，为该类化合物的制备提供了一种工艺简便，收率较高的合成工艺途径。

In this article, we have been investigated that synthesizing and properties of shape memory polyurethane. The shape memory polyurethane was synthesized from PCL diol, MDI(4, 4'-diphenylmethane diisocyanate) and BDO (1,4-butanediol) in this experiment. We analyzed that the effect of differential mole ratio of monomers to synthesized SMPU. Besides, the various concentrations of Nano-silver were mixed with SMPU. Mechanical properties and shape memory behavior of SMPU nanocomposite films were investigated.

本研究目的为藉由改变4，4'-二苯甲基二异氰酸盐(4，4'-diphenylmethane diisocyanate， MDI)/聚己内酯二元醇(polycaprolactone diol， PCL diol)/1，4-丁二醇(1，4-butanediol， BDO)等不同莫耳比制备形状记忆型聚氨基甲酸酯(Shape Memory Polyurethane， SMPU)；并探讨改变不同单体莫耳比及添加不同浓度奈米银溶液对其物性及形状记忆性的影响。

The fluorescence properties of polymethylene bis-b-naphthoates I (n = 2, 3, 4, 5, 10) in poor solvents such as DMSO-water and ethylene glycol-water were measured under stationary and nonstationary conditions at various temps.

本文研究了双-β-萘甲酸多亚甲基二醇酯在二甲基亚砜-水(DMSO-H2O)和乙二醇-水(EG-H2O)两种混合溶剂中的稳态和时间辨荧光光谱以及温度、溶剂组成对荧光光谱的影响。

The effects of imidization method,coagulation bath and temperature were studied on the structure and separation performance of polyimide membrane,prepared by using pyromellitic dianhidride and 4,4′-oxydianiline as raw materials.

针对以均苯四甲酸二酐和4， 4′-二氨基二苯醚为原料合成聚酰亚胺的过程，研究了亚胺化方法、凝胶浴组成与温度等条件对膜的结构和分离性能的影响。

The results showed that the ultimately productive rate of formic acid reached 95.75% when the mol ratio of sodium formate and phosphoric acid was 1:1.30, the quantity of phosphorus pentoxide was 35.73 g, vapouring temperature was 115℃.

实验结果表明：在一定实验体系中，甲酸钠与磷酸摩尔比为1：1.03、五氧化二磷加入量为35.73 g、蒸馏温度为115℃时，甲酸最终浓度可达到95.75%。

The main reason for the deactivation is that the catalysts react directly with methyl formate produced to form alkali formates (sodium formate and potassium formate) and diemthyl ether.

导致催化剂活性降低的主要原因是甲醇钠可以直接与产物甲酸甲酯反应形成甲酸钠和二甲醚。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。