二甲基苯胺

This invention discloses an intermolecular charge transfer chromogen with triphenylamine group, with a formula indicated by (1), wherein: R1 is hydrogen atom or methyl group or methoxyl group, R2 is hydrogen atom or 2-(5,5-dimethyl-3-vinylcyclohexenyl-2-enylidene)propanedinitrile group.

本发明公开的含三苯胺基团的分子内电荷转移生色团，具有式1所示的结构式，其中R 1 为氢原子或甲基或甲氧基，R 2 为氢原子或2-(5，5-二甲基-3-乙烯环己烯基-2-烯亚基)丙二腈基。

Despite their insolubility in many organic solvents, they are found to be soluble in nitrogen-containing solvents, such as DMF and pyridine.

这些化合物具有较好的稳定性，在胺类或其它含氮的有机溶剂中有较好的溶解度，如苯胺、二甲基甲酰胺或吡啶等。

The main products 40,000 tons / year potassium carbonate, 60000 tons / year of potassium bicarbonate, 1,000 tons / year of 3,4 dichloroaniline, 6000 tons / year dimethyl sulfoxide, 2.5 thousand tons / year Xylitol, 1000 tons / year, such as high-purity hydrogen.

主要产品为4万吨/年碳酸钾，6万吨/年碳酸氢钾，1000吨/年3，4二氯苯胺，6000吨/年二甲基亚砜，2500吨/年木糖醇，1000吨/年高纯硫化氢等。

Anti-aging effects of non-lead and non-nickel antiager of 4,4 -Bis(alpha,alpha-dimethylbenzyl)diphenylamine(445)and 2-phenyl mercaptan parallelism imidazole were dealt with on the mechanical properties and vulcanizing performance of epichlorohydrin rubber.

研究了不含铅、镍重金属盐的防老剂445[4，4′-双(2，2-二甲基苄基)二苯胺]和2-硫醇基苯骈咪唑用于氯醚橡胶的防老化作用，考察了防老剂对ECO的力学性能和硫化特性等性能的影响。

Synthesis process of 2,6-dichloro-3-methylaniline was investigated 3-methylaniline was first N-acetylated with acetic anhydride,then treated with chlorosulphonic acid and ammonia yielding the 2-methyl-4--benzenesulfonic amide,which wasin turn deacetylated,chlorinated and hydrolyzed to the title compound.Hydrochloric acid was used instead of sodium hydroxide in deacetylation and sodium chlorate instead of hydrogen peroxide as oxidant in chlorination.

合成工艺2，6-二氯-3-甲基苯胺调查3-甲基首次N-乙酰与醋酸酐，然后与氯磺酸和氨产量 2-甲基-4--苯磺酰胺基，而擅转乙酰，氯化和水解的标题compound.hydrochloric酸代替氢氧化钠乙酰氯酸钠代替双氧水为氧化剂，加氯。

In this paper,pyromellitic dianhydride,1,2,3,4-cyclobutanetetracarboxylic dianhydride,4[(4-aminophenyl)-bis(4-methoxyphenyl)methyl]benzeneamine,4-hexyloxy-biphenyl-3′,5′-diaminobenzoate,and additive ADD-34 were used to synthesize four PIs.

文章用均苯四甲酸二酐，4[(4-氨基苯基)-二(4-甲氧基苯基)甲基]苯胺，1，2，3，4-环丁烷四羧酸二酐，4-己烷氧基联苯酚-3′，5′-二胺基苯甲酸酯和不同含量的添加剂制备了聚酰亚胺液晶取向剂。

Conductivity measurements of the hydrochloride of aniline, methyl aniline and ethyl aniline in water aud in dioxane-water mixtures have been made at 25℃, by using a Jones Bridge.

作者在25℃时，用Jones电导桥测量氢氯化苯胺、N甲基苯胺及N乙基苯胺在水与水及二氧六圜的混合液里的电导。这些氢氯化物的浓度为0.1，0.02，0.01，及

TpRu(PPh3)(CH3CN)2PF6 (10mol%) catalyst effected the nucleophilic addition of water,alcohols,aniline, acetylacetone, pyrroles, and dimethyl malonate to unfunctionalized enediynes under suitable conditions (100 °C, 12 24 h) and gave functionalized benzene products in good yields.

TpRu 2PF6 （ 10mol ％）催化剂的影响的亲核加成的水，醇，苯胺，丙酮，吡咯和二甲基丙二酸对unfunctionalized enediynes适当的条件下（ 100 ℃， 12日24小时），并官能苯产品良好的收益。

Optimum conditions are as follows: DMF is used as solvent, compound quaternary ammonium salt as catalyst, n(p-nitrochloro benzene):n=1: 1.2, m:m(p-nitrochloro benzene)=4%, m:m(p-nitrochloro benzene)1:1, and reacted under 155~160℃ for 18 h; reduction reaction is carried out in methanol with Raney nickel, which is used as catalyst; the raw product is added an antioxidant, and distilled simply under reduced pressure to obtain 4-fluoroaniline with excellence quality, purity is over 99.5%, total yield is 89.3%.

实验结果表明，氟化反应的最佳条件为：二甲基甲酰胺为溶剂、复合季铵盐为催化剂，n：n=1：1.2，m（催化剂：m=4%，m：m=1：1，于155~160℃下反应18h；还原反应在甲醇中进行，以阮内镍为催化剂；粗产品加入抗氧剂，减压条件下简单蒸馏得高品位的对氟苯胺。

Using N,N′-dimethy-p-toluidineas the catalyst,bisphenol A-glycidyl methacrylate,the resin matrix in most dental composite restorative materials,was synthesized by the reaction of bisphenol A and glycidyl methacrylate,and characterized by FTIR,~1HNMR and M S.

以N，N-二甲基对甲苯胺为催化剂，双酚A和甲基丙烯酸缩水甘油酯为原料合成了一种常用的口腔修复材料树脂基质———双酚A双甲基丙烯酸缩水甘油酯，并用FTIR1、HNMR和质谱对其结构进行表征。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。