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二氯甲基苯

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Suitable water-immiscible organic solvents include aromatic hydrocarbons, eg toluene, xylene, naphthalene, tetrahydronaphthalene and methyl naphthalene; chlorinated aromatic hydrocarbons, eg chlorobenzene, fluorobenzene, chloronaphthalene and bromonaphthalene; esters, eg butyl acetate, ethyl acetate, methyl benzoate, ethyl benzoate, benzyl benzoate, butyl benzoate, phenylethyl acetate, butyl lactate, benzyl lactate, diethyleneglycol dipropionate, dimethyl phthalate, diethyl phthalate, dibutyl phthalate, di(2-ethylhexyl) phthalate; alcohols having six or more carbon atoms, eg hexanol, octanol, benzyl alcohol, phenyl ethanol, phenoxy ethanol, phenoxy propanol and phenoxy butanol; ethers having at least 5 carbon atoms, preferably C 5-14 ethers, eg anisole and phenetol; nitrocellulose, cellulose ether, cellulose acetate; low odour petroleum distillates; turpentine; white spirits; naphtha; isopropylbiphenyl; terpene; vegetable oil; mineral oil; essential oil; and natural oil; and mixtures of any two or more thereof.

适用于水互溶的有机溶剂包括芳香族碳氢化合物,如甲苯,二甲苯,萘,四氢萘和甲基萘;氯代芳香族碳氢化合物,如氯苯,氟,氯萘和萘;酯类,如醋酸丁酯,醋酸乙酯,苯甲酸甲酯,苯甲酸乙酯,苄酯,苯甲酸正丁酯,苯,醋酸丁酯乳酸,乳酸苄,二甘醇二丙酸酯,邻苯二甲酸二甲酯,邻苯二甲酸二乙酯,邻苯二甲酸二丁酯,二(2乙基己基)酯;醇有6个或更多碳原子,如己醇,辛醇,苯甲醇,苯乙醇,苯氧基乙醇,丙醇和苯氧基苯氧丁醇;醚至少有5个碳原子,最好荤5-14醚,如苯甲醚和phenetol;硝化棉,纤维素醚,醋酸纤维素,低气味石油蒸馏;松节油;白酒,石脑油isopropylbiphenyl;萜类,植物油,矿物油,挥发油;和天然油,以及任何两个或两个以上其混合物。

Water,Hydrogenated Polyisobutene,Cyclohexasiloxane,Glycerin,Alcohol Denat,Cetearyl Alcohol,PEG-20,Petrolatum,C13-14 Isoparaffin,Zea Mays Oil,Tocopheryl Acetate,Hydroxypropyl Tetrahydropyrantriol,Hydrolyzed Soy Protein,CI 14700/Red 4,Phenoxyethanol,Adenosine,PEG-100 Stearate,Ethylparaben,Triethanolamine,Polyacrylamide,Malus Domestica Stem Cell Culture,CI 19140/Yellow 5,Dimethyl Isosorbide,Dimethicone,Dimethiconol,Limonene,Xanthan Gum,Pentaerythrityl Tetra-Di-T-Butyl Hydroxyhydrocinnamate,Linalool,2-Oleamido-1,3-Octadecanediol,Capryloyl Salicylic Acid,Acrylates/C10-30 Alkyl Acrylate Crosspolymer,Passiflora Edulis Seed Oil,Disodium EDTA,Castanea Sativa Seed Extract,Butyrospermum Parkii· Cetyl Alcohol,Butylene Glycol,Octyldodecanol,Cetearyl Glucoside,Methylparaben,Citronellol,Prunus Armeniaca Kernel Oil,Laureth-7,Coumarin,Oryza Sativa Bran Oil,Glyceryl Stearate,Fragrance

水,甘油,氢化聚异丁烯,液体石蜡/矿油,丁二醇,环己硅氧烷,鲸蜡醇,甘油硬脂酸酯,棕榈油,玉米胚芽油,PEG-100硬脂酸酯,白蜂蜡/蜂蜡,肉豆蔻醇肉豆蔻酸酯,石蜡,香精,腺苷,苧烯,山梨醇,CI 14700,CI 19140,稻糠油,杏仁油,EDTA二钠,羟丙基四氢吡喃三醇,苯氧乙醇,聚乙二醇-14M,异十六烷,氢氧化钠,辛基十二醇,季戊四醇四(双-t-丁基羟基氢化肉桂酸)酯,山梨坦三硬脂酸酯,水解大豆蛋白,卡波姆,鸡蛋果籽油,苹果果实提取物,欧洲栗籽提取物,异山梨醇酐二甲醚,聚山梨醇酯-80,辛酰水杨酸,2-油酰胺基-1,3-十八烷二醇,氯苯甘醚,麦芽糖醇,香豆素,黄原胶,微晶蜡,丙烯酰胺/丙烯酰基二甲基牛磺酸钠共聚物,丙二醇,芳樟醇,香茅醇,玉米油,羟苯丙酯,羟苯甲酯

Water, Cyclomethicone, Glycerin, Sd Alcohol 40-B (Alcohol Denat.), Propylene Glycol, Melia Azadirachta Leaf Extract, Lecithin, Arctium Lappa Root Extract, Xylitol, Lactitol, Alpha-Glucan Oligosaccharide, Lactoferrin, Potassium Thiocyanate, Glucose Pentaacetate, Glucose Oxidase, Lactoperoxidase, Glycoproteins, Panax Ginseng Root Extract, Equisetum Arvense Extract, Hydrolyzed Milk Protein, Peg-8, Caprylyl Glycol, Sebacic Acid, Sodium Polyacrylate, Betula Alba Bark Extract, Cupressus Sempervirens Leaf Extract, Hamamelis Virginiana Extract, Avena Sativa Meal Extract, Humulus Lupulus Extract, Silk, Nylon-12, Polyacrylamide, Polymethyl Methacrylate, Butylene Glycol, Salicylic Acid, Lauryl Methacrylate/Glycol Dimethacrylate Copolymer, Tocopheryl Acetate, C13-14 Isoparaffin, Laureth-7, Triethanolamine, Xanthan Gum, Acrylates/C10-30 Alkyl Acrylate Crosspolymer, Phenoxyethanol, Chlorphenesin, Benzoic Acid, Methylparaben, Fragrance, Titanium Dioxide

水,环甲硅脂,甘油,Sd Alcohol 40-B,丙二醇,印度楝树叶萃取,卵燐脂,牛蒡根萃取,木糖醇,乳糖醇,α-葡低聚糖,乳铁蛋白,硫氰酸钾,葡萄糖五乙酸酯,葡萄糖氧化酶,乳过氧化物酶,糖蛋白,人参根萃取,问荆萃取,水解牛奶蛋白,聚乙二醇-8,辛乙二醇,癸二酸,聚丙烯酸酯钠,白桦萃取,丝柏叶萃取,金缕梅萃取,燕麦萃取,啤酒花萃取,丝,尼龙-12,聚丙烯醯胺,聚甲基丙烯酸甲酯,丁二醇,水杨酸,甲基丙烯酸十二酯,醋酸盐维他命E,C13-14 异烷烃,月桂醇聚醚-7,三乙醇胺,山羊胶,丙烯酸/C10-30烷基丙烯酸聚合物,苯氧乙醇,氯苯甘醚,苯甲酸,羟苯甲酯,香料,二氧化钛

During the manufacturing of the critical intermediate cephalosporin nucleus --7-amino-3-chloro-cephalosporanic acid diphenylmethyl ester hydrochloride salt, first the feasibility of the one-pot synthetic route of open loop, closed loop and ozonization when chlorine is passed over is qualified by experiments. Then the critical factors that will influence this reaction are studied as follows: the mol ratio of triphenyl phosphite and Diphenylmethyl 3-hydroxy-7-phenylacetaminoceph-3-em-4-carboxylate-l-oxide is four to one; the quantity of the stablizer should be at least more than two to one. The temperature of the system must be 25℃ when chlorine is passed over so that the hydrochloride can be precipitated to obtain cephalosporin nucleus of cefaclor--7-amino-3-chloro-cephalosporanic acid diphenylmethyl ester hydrochloride salt.

在制备关键中间体头孢母核7-氨基-3-氯头孢烷酸二苯甲酯盐酸盐时,先通过实验验证把开环、闭环、臭氧化三步在通入氯气时并为一锅煮的合成路线的可行性之外,又研究了影响该反应的几个重要因素:亚磷酸三苯酯与3-羟基-7-头孢烷-5-亚砜-2-甲酸二苯甲酯的摩尔比为4:1;稳定剂2-甲基-2-丁烯的用量至少大于2:1,通入氯化氢气体时体系温度在25℃时盐酸盐则能够顺利析出,获得头孢克洛的头孢母核—7-氨基-3-氯头孢烷酸二苯甲酯盐酸盐。

Methods Benzhydrylpiperazine was synthesized by condensation of chlorodiphenylmethane and anhydrous piperazine in absolute ethanol.

以二苯甲基氯和无水哌嗪为原料,无水乙醇做溶剂,两者经缩合制得二苯甲基哌嗪。

Water,butylene glycol,biosaccharide gum-1,ppg-26-buteth-26,panthenol,peg-40 hydrogenated caster oil,hydroxyethylcellulose,imidazolidinyl urea,saccharide isomerate,benzophenone-4,phenoxyethanol,triethanolamine,citrus aurantium dulcisoil,pentadecalactone,methylparaben,sodium hyaluronate,citric acid,butylparaben,ethylparaben,citrus aurantium amaraoil,propylparaben,methylchloroisothiazolinone,methylisothiazolinone,red 4,yellow 5,red 33,limonene,linalool

水,丁二醇,多醣物质,PPG-26-丁醇聚醚-26,维生素B5,PEG-40氢化蓖麻油,羟乙基纤维素,尿素醛,天然异构寡糖,二苯甲酮- 4,苯氧乙醇,三乙醇胺,甜橙油,环十五内酯,羟苯甲酯,透明质酸钠,柠檬酸,羟苯丁酯,羟苯乙酯,苦橙油,羟苯丙酯,甲基氯异塞唑晽酮,甲基异噻唑啉酮,红4,黄5,红33,柠檬精油,芳樟醇

Water,butylene glycol,glycerin,glyceryl polymethacrylate,triethanolamine,carbomer,ppg-26-bueth-26,chondrus crispus,peg-40 hydrogenated castor oil,phenoxyethanol,imidazolidinyl urea,propylene glycol,benzophenone-4,retinyl palmitate,citrus aurantiudulcisoil,phospholipids,methylparaben,tocopheryl acetate,c12-23 alkyl lactate,disodium EDTA,centella asiatica extract,iris germanica root extract,pentadecalactone,aloe barbadensis leaf juice,mimosa tenuiflora bark extract,sodium hyaluronate,menthol,biosaccharide gum-1,citrus aurantium amara oil,propylparaben,methylchloroisothiazolinone,sodium benzoate,potassium sorbate,citric acid,calcium sorbate,methylisothiazolinone,butylparaben,ethylparaben,yellow 5(CI 19140),limonene,linalool

水,丁二醇,甘油,甘油聚甲基丙烯酸酯,三乙醇胺,卡波姆,PPG-26-丁醇聚醚-26,鹿角菜胶,PEG-40 氢化蓖麻油,苯氧乙醇,尿素醛,丙二醇,二苯酮-4,维他命A酯,甜橙油,磷脂质,羟苯甲酯,醋酸盐维他命E,C12-13 烷醇乳酸酯,乙二胺四乙基二钠,雷公根萃取,鸢尾花根萃取,环十五内酯,吉拉索芦荟叶汁,含羞草萃取,透明质酸钠,薄荷脑,多醣物质,苦橙油,羟苯丙酯,甲基氯异塞唑晽酮,苯甲酸钠,山梨酸钾,柠檬酸,山梨酸钙,甲基异噻唑啉酮,羟苯丁酯,羟苯乙酯,柠檬黄,柠檬精油,沈香醇水:几乎所有护肤品成分第一位都是水。丁二醇:保湿剂及溶剂,质地温和

Five Butenafine's analogues were designed and synthesized according to the structure-activity relationship and operating mechanism of benzylamine antimycotics.

根据苄胺类抗真菌化合物的构效关系、作用机理,设计合成了 5个布替萘芬类似物,N (2 氯 5 吡啶甲基) N 甲基 1 萘甲胺,N ,N 二(4 叔丁基苄基) 1 萘甲胺,N (4 叔丁基苄基) N (2 氯 5 吡啶甲基) 1 萘甲胺,N ,N 二苄基 4 叔丁基苯甲胺,N (2 氯 5 吡啶甲基) N 苄基 4 叔丁基苯甲胺。

The method comprises following steps: taking diphenol and 3- trifluoromethyl- 4- chloronitrobenzene as raw material, salt precipitating for diphenol and potash, refluxing with water- containing toluene, reacting with 3- trifluoromethyl- 4- chloronitrobenzene and getting dinitro monomer; taking dinitro monomer, ferro powder and HCl as raw material, ethanol and water as disslovant for refluxing and ethanol recrystallization, getting fluorine- containing aromatic diamido monomer.

合成方法是以二酚与3-三氟甲基-4-氯硝基苯作原料,先将二酚与碳酸钾成盐,甲苯带水回流反应,然后与3-三氟甲基-4-氯硝基苯反应制得二硝基单体;再以二硝基单体,铁粉,HCl为原料,乙醇和水做溶剂,回流反应、乙醇重结晶,得到含氟芳香二胺基单体。

The compound of BNTMBP wassynthesized by the condensation reaction between 4-chloronitrobenzene (4CNB) and 4, 4'-dihydroxy-3, 3', 5, 5'-tetramethyl biphenyl in the presence of potassium carbonate in the mixture solvents of N, N-dimethylformamide and tolune.

4, 4'-二羟基-3, 3', 5, 5'-四甲基联苯、4-氯硝基苯(4CNB)和碳酸钾在N, N-二甲基甲酰胺和甲苯的混合溶剂体系中回流反应,合成得到了4, 4'-双(4-硝基苯氧基)-3, 3', 5, 5'-四甲基联苯;随后,在Pd/C-水合肼的还原体系中,被进一步还原,得到了4, 4'-双(4-氨基苯氧基)-3, 3', 5, 5'-四甲基联苯。

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Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在,所有的孩子都要在综合学校继续学习,所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地,使人们普遍认识到发展不能以牺牲农业为代价。

Detailed Intrinsic Reaction Coordination calculations were carried out to guarantee the optimized transition-state structures being connected to the related tautomers.

同时,做了详尽的内禀反应坐标计算,以保证所得到的过渡态连接相应的始末异构体。