二十烷

The titled compound as an intermediate for preparing muscone is obtained by reacting a tetradecanedioic acid as the starting material with a chlorinating agent——chlorosulfoxide,followed by reacting the resultant reaction product on halogenomethylzinc .

采用直链十四碳二元酸为起始原料，先以氯化亚砜进行酰化，所得酰氯直接与甲基锌试剂反应进行甲基化，从而制得了合成麝香酮的重要中间体2，15-十六烷二酮，产物结构经1HNMRI、R确认。

Sodium fatty alcohlo ether sulfate, S-80, fatty alcohol-polyoxyethylene ether and S-60 resulted in slow photodecomposition of rotenone in aqueous solution revealing a photo-extinction effect, sodium dodecylberzenesulfonate, tween-60, hexadecyl trimethyl ammonium bromide and poyl vinyl pyrrolidone made the photolysis of rotenone in aqueous solution fast showing an obvious photosensitized effect.

室内条件下研究了鱼藤酮水溶液存在不同表面活性剂时，鱼藤酮的紫外光降解，结果表明：脂肪醇聚氧乙烯醚硫酸钠、司本－80、长链脂肪醇聚氧乙烯醚和司本－60对鱼藤酮在水溶液中的光解速率表现出显著的光猝灭降解效应；十二烷基苯磺酸钠、吐温－60、十六烷基三甲基溴化铵和聚乙烯吡咯烷酮对鱼藤酮在水溶液中的降解表现出一定程度的光敏化作用。

Thereinto, the content of eucalyptus oil was the most with 27.20%, the next was Terpinen-4-OL (21.27%), N-methyl-laurotetanine (6.32%), Hepladecanoic acid (4.33%), Phytol (3.53%), Ether linoleic acid (3.45%), 2,6-dimethyl-2,6-octadiene (2.96%) and so on.

其中，含量最高的是桉油(27.20%)，其次是松油烯－4-醇(21.27%)、N甲基山鸡椒痉挛碱(6.32%)、十七烷酸(4.33%)、叶绿醇(3.53%)、乙醚基亚油酸(3.45%)、2，6－二甲基－2，6-辛二烯(2.96%)等。

The optimal carrier gas velocity of prepared SE-30 series capillary chromatographic columns was studied and used to separate isomeric compounds. The efficiency of SE-30 capillary chromatographic columns has been studied with different diameters, film thicknesses and oven temperatures, using n-do-decane, phenol, aminobenzene, and butyl acetate as test samples.

研究自制的SE-30系列毛细管气相色谱柱的载气最佳线速度，并应用于同分异构体的色谱分离分别用十二烷、苯酚、苯胺、醋酸丁酯作试祥在不同载气线速条件下对不同口径、不同膜厚、不同柱温的SE-30毛细管色谱柱的柱效进行考察，并在最佳线速度条件下分离异戊醇、硝基氯苯、硝基甲苯及二乙苯同分异构体体系。

Hydrogels based on n -alkyl methacrylate esters,acrylic acid and acrylamide cross-linked with 4,4′-diazobenzene were preparared,and their deswelling kinetics was studied.

研究了甲基丙烯酸十二烷或丁酯、甲基丙烯酰胺及丙烯酸与4 ，4′-二偶氮苯交联共聚凝胶的消溶胀动力学。

The electrocatalysis of Pd/GCE(GCE: glassy carbon electrode) to reduction of H2O2 was discussed.

在十一烯酸和十二胺为表面活性剂、正辛烷为油相形成的油包水型反胶束体系中，通过调节体系的组成，制得了丝状、棒状和空心球状的BaWO4纳米粒子，其中空心球状BaWO4纳米粒子的制备为首次报道。

In the system droplets in microns are first formed by emulsifying an organic phase consisting of a core material (n- hexadecane) and an oil- soluble reactive monomer,toluene- 2,4- diisocyanate,in an aqueous phase.By adding water- soluble reactive monomer,diamine,monomers TDI and diamine react with each other at the interface of micelles to become a shell.

在含乳化剂的水溶液中，将溶有芯材正十六烷的有机相乳化成微米级油性液滴，随后加入的水溶性单体二胺与甲苯 2， 4-二异氰酸酯在胶束界面相互反应形成囊壁。

Results show that clicyclohexyl ammonium decanoate has the best inhibiting effect in neutral water and dicyclohexyl ammonium hexylate, dicyclohexyl ammonium octoate and dicyclohyxyl ammonium decanoate are good inhibitors of iron and steel in hydrochloric acid.

研究结果表明，十个碳的二环已胺在中性水中具有最好的缓蚀效果。已酸、辛酸及癸酸十二烷胺等是盐酸溶液中钢铁的优良缓蚀剂。

RESULTS: 12 compounds were isolated and identified as aurantiamide acetate (1), aurantiamide benzoate (2), physcion (3), scopoletin (4), vanillin (5), coniferyl aldehyde (6), syringaldehyde (7), syringic acid (8), luteolin (9), apigenin (10), azelaic acid (11), dotriacontanic acid (12), respectively.

结果：从羊耳菊全草的氯仿和乙酸乙酯部分共分离得到12个化合物，分别鉴定为橙黄胡椒酰胺乙酸酯(1)，橙黄胡椒酰胺苯甲酸酯(2)，大黄素甲醚(3)，东莨菪亭(4)，香草醛(5)，松柏醛(6)，丁香醛(7)，丁香酸(8)，木犀草素(9)，芹菜素(10)，壬二酸(11)，三十二烷酸(12)。

An expansion monomer 3, 9-dihydroxymethyl-di (6-methyl-5 -hydroxyl)-2- heptanone-1, 5, 7, 11tetraoxaspiro [5, 5] undecane was synthesized and its volume change during polymerization is about +3.04%. Its prepolymer was also synthesized by toluene 2, 4-diisocyanide with it.

由三经甲基丙烷合成了螺环原碳酸酯单体3'、9'－二羟甲基－3'，9'-二乙基－1，5，7，11－-四氧杂螺环[5、5]十一烷单体（体积膨胀率＋3.04%）以及它的预聚物，并用其来改性环氧树脂B-63。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。