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The development and application of supramolecular chemistry and NMR were reviewed.Based on that,several benzimidazole derivatives were synthesized from o-phenylenediamine.

本文在总结超分子化学及核磁共振的发展及应用的基础上,以邻苯二胺为原料,合成了几种苯并咪唑衍生物,作为分子识别中的客体小分子。

Based on the PTB study situation of the studied area, two terrestrial sections and one marine-terrestrial section were chosen for the sedimentary and sequence stratigraphy study. The former are Chahe section and Zhejue section in Weining, Guizhou, and the latter is Mide section in Xuanwei, Yunnan. The definition and correlation of the TPTB were discussed based on the results of biostratigraphy, isotope stratigraphy, geochemostratigraphy, and molecule stratigraphy. Thus, it supplied a perfect base for the establishment of the TAGSSP in the area.

针对研究区二叠系—三叠系界线剖面研究现状,选择了二条陆相剖面,既贵州威宁岔河剖面和哲觉剖面,一条海、陆交互相剖面即云南宣威密德剖面,开展了有关沉积学和层序地层学方面的研究,并结合生物地层、同位素地层、地球化学地层和分子地层等资料探讨了研究区二叠系—三叠系界线的划分与对比方案,从而为在该区争取建立陆相二叠—三叠系辅助层型剖面和点打下了良好基础。

At first the energy of the microwave will energized the argon to be ionization, and the generated heat make the sulfur volatilizing into bivalency sulfur or dipolymer sulfur high pressure steam. The molecule transition will happen under the microwave energization, and the visible light will be emitted when the sulfur states change into the low energy level. The spectra of the plasma lamp is nearly centering at the visible lights, and there are very little ultraviolet and infrared spectrum, the Fig 3 shows the spectra of the sun and the plasma lamp from which we can see the spectrum character clearly.

微波能量首先激励氩气使其电离,产生的热量使硫挥发成为二价硫分子或二聚物高压蒸汽,在微能量的激励下使它形成分子跃迁,当返回到较低能级的状态时以连续光谱的形式放射出光线,它的光谱基本上集中在可见光,红外线和紫外线的辐射量很少,(图3)硫的放射光谱和太阳光谱的比较图片,可以很清晰地表达这一特性。

Objective To study the mechanisms and treatment of ischemia /reperfusion injury, expression of intracellular adhesion molecule 1 (ICAM-1) and vascular cell adhesion molecule 1 (VCAM-1) were measured, the effect on suppression of ICAM-1 and VCAM-1 by the pyrrolidine dithiocarbamate were investigated.

目的 为研究心肌缺血-再灌注损伤的机制和治疗途径,检测血管内皮细胞缺氧/再给氧后细胞间黏附分子- 1(intracellular adhesion molecule1,ICAM- 1)和血管细胞黏附分子- 1(vascular cell adhesion molecule1,VCAM-1)的表达,探讨抗氧化剂吡咯烷二硫氨基甲酸酯(pyrrolidine dithiocarbamate,PDTC)对血管内皮细胞表面细胞黏附分子表达的抑制作用。

The rest denote sound break down, it be called rest and shown as '0' in the music book. Rest can be disport as note full-rest, half-rest quarter rest, eight rest and sixteen rest.

二分之二拍 2/2 2/2 beat 四分子二拍 2/4 2/4 beat 四分之三拍 3/4 3/4 beat 四分之四拍 4/4 4/4 beat 八分之三拍 3/8 3/8 beat 八分之六拍 6/8 6/8 beat 八分之十二拍 12/8 12/8 beat 三、休止符rest 表示声音停顿的符号,叫休止符,用"0"来表示休止符和音符一样可分为:全休止符,二分休止符,四分休止符,八分休止符和十六分休止符。

In addition, a two-dimernsion host molecular library of amide derivatives of tartaric acid was designed and synthesized.

本论文还设计合成了由20余个酒石酸酰胺衍生物组成的二维主体分子库,并对平行方法筛选主体分子作了一些初步的探索,发现主客体分子识别存在很强的专一性。

A SPE procedure was suggested for extracting and concentrating fisetin by using different volume fractions of ethanol in aqueous solution as the loading conditions.

分别以中药黄栌的主要成分非瑟酮为印迹分子、丙烯酰胺为功能单体及乙二醇二甲基丙烯酸酯为交联剂,通过封管聚合法合成了分子印迹聚合物;将其装于自制的固相萃取柱中,研究了以不同体积比的乙醇-水溶液为溶剂时非瑟酮在柱上的保留行为;通过优化清洗及洗脱条件,使非瑟酮与它的结构相似物槲皮素在柱上得到了很好的分离。

However, the use of Aegliops tauschii in improvement of wheat yield trait has not been reported. In this study, T.durum-Ae.Squarrosa amphidiploids was crossed with common wheat PH85-16, then backcrossed with PH85-16. The variation characteristic of the main yield traits of BC1F1 and BC1F2 were analyzed. Then, QTLs affecting yield traits were detected by 130 SSR primer pairs of D genome in BC_1F_1 and BC_1F_2.The result showed chromosomes in D genome from Aegliops tauschii affected yield trait of wheat significantly.

本研究以二倍体小麦粗山羊草与四倍体硬粒小麦合成的双二倍体Am6为亲本,与普通小麦PH85-16 进行杂交,再用PH85-16 进行回交,对获得的回交后代进行了主要产量性状调查,利用位于小麦D 基组的SSR 分子标记进行了分子标记分析,对来自粗山羊草与产量性状相关的数量性状位点进行定位,探讨粗山羊草对小麦产量性状的影响。

Results of non-reducing sodium dodecyl sulphate polyacrylamide gel electrophoresis of the supernatant and aggregate precipitate formed in refolding process show that except being refolded to native egg white lysozymes, the reduced-denatured lysozymes can also form the aggregates with molecular weights being separately about 30.0 and 35.0 kD, while the reducing SDS-PAGE and the refolding results in the presence of sodium dodecyl sulphate show that these aggregates are formed chiefly through the misconnection of disulfide bonds between the reduced-denatured lysozymes, and the aggregate precipitates are formed through the non-covalent interactions between the aggregates with molecular weight being about 30.0 kD.

复性过程形成的上清和集聚体沉淀的非还原电泳结果表明,除了能复性成天然态的溶菌酶分子外,还原变性蛋白溶菌酶同时还能形成分子量分别约为30.0KD和35.0KD的蛋白溶菌酶分子集聚体;而它们的还原电泳和在SDS存在时的复性结果表明,这些集聚体主要是通过还原变性蛋白溶菌酶分子间的二硫键错配而形成,而集聚体沉淀则是通过分子量约为30.0KD的集聚体分子之间的非共价相互作用而形成。

The complexes areneutral as shown by values of molar conductivity in aqueous solution, namely,〓 The crystal structure determinations show that, in complexes, metal ions werecoordinated by four nitrogen atoms and form slightly distorted square planar configuration,relationship between fluorene ring plane and coordination plane is similar to those betweenpeptide planes of β-folding in proteins. The complex molecules linked by hydrogen bonds formone dimension chain or two dimension network structure.

摩尔电导测定表明他们都是二氧四胺中酰胺氮去质子化后形成的产物。X-射线衍射晶体结构测定表明〓的铜、镍配合物的配位多面体都是稍微畸变的平面正方形,配合物分子中芴基平面与配位平面的关系类似于蛋白质β-折叠结构中肽平面之间的关系,配合物分子之间通过氢键连接成一维链状或二维网状结构。

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