二二二

Effect of ratio of dimethylol propionic acid to polybutylene adipate glycol on Tg and basic properties of films was studied.

考察了二羟甲基丙酸/聚己二酸丁二醇酯二醇比例对Tg以及膜基本性能的影响。

The studies segmented polyester polyurethaneurea elastomers based on 4,4'-diphenylmethane diisocyanate, ethylene diamine and polybutylene adipate (M. W. 1975 and M. W. 1228) were studied by means of IR spectrascopy.

用红外光谱法对基於4，4'-二苯基甲烷二异氰酸酯、乙二胺和聚己二酸丁二醇酯（分子量分别为1975和1228）的嵌段聚脲氨酯弹性体进行了研究。

B., aluminum oxide (Al2O3), cupric 2, 4-dihydroxy-benzoate ,cupric adipate and lead phthaiate were used as inert materials.

三氧化二铝(A12O3)、2， 4-二羟基苯甲酸铜、己二酸铜和邻苯二甲酸铅等惰性材料的相容性。

Hydrogen bonding in hard segment domains of segmented polyester polyurethaneurea based on 4,4'-diphenylmethane diisocyanate, ethylene diamine and polybutylene adipate(M. W. 1975 and M. W. 1228) was studied by means of IR spectroscopy.

用红外光谱法对基於4，4'-二苯基甲烷二异氰酸酯、乙二胺和聚己二酸丁二醇酯（分子量分别为1975和1228）的两系列嵌段聚酯型聚脲氨酯硬段微区中的氢键化进行了研究。

A series of polyurethane anionomers were synthesized from isophorone diisocyanate, polyneopentanediol adipate and dimethanol propionic acid.

用异佛尔酮二异氰酸酯、聚己二酸新戊二醇酯和二羟甲基丙酸合成了负离子型聚氨酯离聚体。

The blast power of TBE was higher due to the enhancement of afterburning to shock wave. The percentage of total energy released in explosive reaction of TBE was about 42% as analysis, which indicated that it had potential to be improved. A modified thermobaric explosive containing chemically active material was studied by experiment.

对含化学活性材料温压药剂M-TBE的实验表明：其冲击波曲线有两个规律的正压作用区；二次冲击波在火球区外形成，火球区内是后续燃烧反应对爆炸波增强而引起的压缩波积累压力平台；二次冲击波峰值压力不小于第一个冲击波的40%，二次冲量占总冲量的12.5%~43.7%，其对爆炸/冲击波威力的贡献不可忽略；化学活性材料对温压药剂的后续燃烧反应有增强作用，有利于二次冲击波的形成和传播。

A C++ program is developed for composing the stiffness matrix of the temperature field, saving it in changing bandwidth method and calculating the linear algebraic function group through using the Gauss eliminating method. A module for drawing the color fringe of tire temperature field is created, which makes the result more visual. Taking the 9.00-20 cross-ply tire on CA1092 as an example, the finite element numerical simulation analysis of automobile tire 2-D steady temperature field is completed. Through comparing the result with the analysis data by ANSYS, this software is proved to be capable of the modeling, calculating and post-processing of FEA of automobile tire 2-D steady temperature field.

采用C++语言完成了温度刚度矩阵的总体合成及其一维变带宽存贮，以及线性代数方程组高斯消去法求解等工作，采用C++语言实现了汽车轮胎二维稳态温度场云纹图的绘制，使得计算结果更加直观，也更能形象地显示汽车轮胎二维稳态温度场的分布状况，以CA1092（原CA142）五吨载货汽车用9.00-20尼龙斜交胎为例，进行了汽车轮胎二维稳态温度场有限元数值仿真分析，通过与ANSYS分析结果进行比较，说明所开发的有限元建模、求解以及后处理软件能够用于汽车轮胎二维稳态温度场有限元分析。

Molybdenum-glycol complexes synthesized with different alkylene glycols and Mo/alcohol ratios have different acidity and catalytic activity. For the topic reaction, the catalytic activity of Mo-1, 2-ethandiol or Mo-1, 2-propanediol is higher than that of Mo-butanediol.

结果表明，用不同的二醇和不同醇／钼比制备的钼醇催化剂具有不同的催化性能和酸性，用乙二醇和丙二醇制备的催化剂，催化性能优于丁二醇制备的催化剂。

In this paper, through a series of experiments, two series of quaternary-ammounium Gemini surfactants were synthesized, namely the pair alkylene double quaternary ammonium salt surfactant m-s-m·2Br and the pair the alkylene double quaternary ammonium salt surfactant -s-·2Br. We has carried on the attribute with the infrared spectrum to its structure, and to affected the factor which the synthesis pair the alkylene double quaternary ammonium salt surfactant responded to carry on the discussion. We has discovered the synthesis pair the ethylene double quaternary ammonium salt surfactant m-2-m·2Br optimum condition: The bromo alkane and a tetramethyl ethylene diamine mole of ratio is 3.0: 1.0, makes the solvent by the ethyl alcohol, 80℃ under responds for 48 hours in the backflow temperature; Synthesis pair alkylene double quaternary ammonium salt surfactant 12-S-12 ·2Br optimum condition: 12 tertiary amine and 1, 3- propylene dibromide (1, 4- two bromines butane) a mole of ratio is 2.2: 1.0, makes the solvent by the ethyl alcohol, responds for 48 hours in the constant temperature 80 ℃ under backflow.

本文通过一系列的实验，合成了两个系列的Gemini型表面活性剂，即双烷撑双季铵盐表面活性剂m-s-m·2Br和双烷撑双季铵盐表面活性剂-s-·2Br，用红外光谱对其结构进行了表征，并且对影响合成双烷撑双季铵盐表面活性剂反应的因素进行了讨论，找出了合成双乙撑双季铵盐表面活性剂m-2-m·2Br的最佳条件：溴代烷与四甲基乙二胺的摩尔比为3.0：1.0，以乙醇作溶剂，在回流温度80℃下反应48小时；合成双烷撑双季铵盐表面活性剂12-s-12·2Br的最佳条件：十二叔胺与1，3-二溴丙烷(1，4-二溴丁烷)摩尔比为2.2：1.0，以乙醇作溶剂，在恒温80℃下回流反应48小时。

Anesthesis was performed by interscalene brachial plexus block.the onset and duration of analgesia,the level of block as well as adverse effects were recorded.hr and map were measured before anesthesia,5,10,30 and 60 minates after anesthesia.results:the onset time of block was significantly shorter and shivering was significantly lower in groups two and three as compared with group one.there was significant difference in the duration of anesthesia between group two and group three.

肌间沟法行臂丛神经阻滞，观察阻滞起效时间及持续时间、神经阻滞节断数、术中镇痛质量、不良反应以及注药前、注药后5、10、30、60分时心率和平均动脉压。结果：二、三组麻醉起效时间短于一组（p＜0.05）；麻醉持续时间二、三组长于一组但差异无显著性；二、三组组间比较差异有显著性；各组阻滞节断数、术中牵涉痛发生率、hr及map差异无显著性；一组寒战发生率高于二、三组（p＜0.05）。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。