二二二

The major products were methane, ethylene, propylene, butylene, butadiene, cyclopentadiene, benzene, toluene, styrene, vinyl-substituted cyclopentene derivatives and C5/C6 isomers pentadiene, met...

热裂解主要产物为甲烷、乙烯、丙烯、丁烯、丁二烯、环戊二烯、苯、甲苯、苯乙烯、环戊烯的乙烯基取代物及C5，C6异构体(戊二烯、环戊烯的甲基取代物、环己烯、己二烯和环戊二烯甲基取代物)，其中，C1～C4、环戊二烯、苯、甲苯、乙烯基取代环戊烯为初始产物。

The super acid SO〓/ZrO〓, due to its strong acidity, favores the dealkylation and disproportionatin of 4-TBC or/and DTBC, preventing the increase of the selectivity for 4-TBC.

而固体超强酸SO〓/ZrO〓由于酸性较强，易于发生4-叔丁基邻苯二酚和3，5-二叔丁基邻苯二酚的脱烷基反应和4-叔丁基邻苯二酚的歧化反应，因此不利于提高4-叔丁基邻苯二酚的产率。

In present study, a liquid-liquid extraction method was employed to extract the volatile components in mulberry fruit sparkling wine. The analysis with gas chromatography-mass spectrometry detected 69 peaks, among which 63 volatile components were identified. The first 9 volatile components with high relative content were benzyl alcohol, 2-methyl-1-butanol, mono-(2-ethylhexyl)-1, 2-benzene dicarboxylic acid, 3-methyl-1-butanol, toluene, acrylic acid butyl ester, 1H-indole-3-ethanol, isodecyl octyl phthalate and decyl octyl phthalate.

采用液－液萃取法提取桑椹汽酒中的挥发性成分，经气相色谱－质谱联机分析，共检测出69个峰，鉴定出63种挥发性化合物，其相对含量排在前9位的挥发性化合物分别是苯乙醇、2-甲基－1-丁醇、1，2-苯二酸单（2-乙基）己酯、3-甲基－1-丁醇、甲苯、丙烯酸丁酯、1H-吲哚－3-乙醇、邻苯二甲酸异癸基辛基二酯、邻苯二甲酸癸基辛基二酯。

In this paper, the synthesis, performance and kinetics of C_(36) DFAbased di-polyester or tri-polyester and its derivant, their polyesters were synthesizewith DFA and EG or PEG and PPG, were systemically and roundly studied.

本文以天然油脂加工产物——二聚脂肪酸为主要原料，系统地研究了二聚脂肪酸与乙二醇、聚乙二醇、聚丙二醇之间二元或三元缩聚反应的理论问题及合成物应用性能。

Inthis papor,we synthesize and symbolize three sulphide bicarboxylate ligands such as 2.5-bis-1.3,4-thiadiazole;2,2 -(o-phenylenedimethylenethio) diacetic acid(L11); 2,2 -(m-phenylenedimethylenethio) diacetic acid.

本文合成和表征了2，2′-(1，3，4-噻二唑-2，5-二硫基)二乙酸、2，2′-邻苯二甲硫基二乙酸和2，2′-间苯二甲硫基二乙酸三个含硫二元羧酸配体。

And to make the product be easy of purification, the excess of amine was reduced to 50% from 150%. Then the diiodoalkane reacted with dialkylmethylamine into diquaternary ammonium iodide, and obtained three diquaternary compounds whose spacer groups were -(CH2)6-, N,N"-dimethyl- N,N,N",N"-tetraoctyl-1,6-hexane diammonium diiodide, N,N"-dimethyl-N,N,N",N"-tetradecyl-1,6-hexane diammonium diiodide, N,N"-dimethyl-N,N,N",N-tetradodecyl -1,6-hexane diammonium diiodide.

对于更长间隔链的双子型季铵盐，一方面为了加快亲核取代反应速率，先将1，6-二氯己烷、3-氧杂-1，5-二氯戊烷转化成1，6-二碘己烷、3-氧杂-1，5-二碘戊烷，另一方面为了降低产物提纯的难度，将叔胺的过量由150%降到50%，使二碘代烷与双长烷基甲基叔胺在相同的温度下、反应相同的时间，经过相同的后处理，得到3个间隔链为-(CH2)6-的双子型季铵碘化物，(C8H17)2N+(CH3)(CH2)6 (CH3)N+(C8H17)2·2I-、(C10H21)2N+(CH3)(CH2)6(CH3)N+(C10H21)2·2I-和(C12H25)2N+(CH3)(CH2)6(CH3)N+(C12H25)2·2I-。

The method comprises following steps: taking diphenol and 3- trifluoromethyl- 4- chloronitrobenzene as raw material, salt precipitating for diphenol and potash, refluxing with water- containing toluene, reacting with 3- trifluoromethyl- 4- chloronitrobenzene and getting dinitro monomer; taking dinitro monomer, ferro powder and HCl as raw material, ethanol and water as disslovant for refluxing and ethanol recrystallization, getting fluorine- containing aromatic diamido monomer.

合成方法是以二酚与3-三氟甲基-4-氯硝基苯作原料，先将二酚与碳酸钾成盐，甲苯带水回流反应，然后与3-三氟甲基-4-氯硝基苯反应制得二硝基单体；再以二硝基单体，铁粉，HCl为原料，乙醇和水做溶剂，回流反应、乙醇重结晶，得到含氟芳香二胺基单体。

A series of segmented thermally stimulated shape-memory polyurethanes, which consist of polyethylene adipate glycolas the soft segment and 4,4'-diphenylmethane diisocyanate-1,4-butanediol-DPA(which consists of ring components) as the hard segment were synthesized by one-step polymerization.

以聚己二酸乙二醇酯二醇为软段、4，4' -二苯基甲烷二异氰酸酯 1，4 丁二醇含环状结构的扩链剂DPA为硬段，采用一步聚合法制备了一种具有热致形状记忆功能的多嵌段聚氨酯弹性体。

A series of polyether based polyurethaneurea aqueous dispersions with well-defined hard segments were prepared by fractional steps with polyether polyol, 4,4'-diphenylmethane diisocyanate, dimethylolpropionic acid, 1,4-butanediol, isophorone diisocyanate and ethylenediamine.

以二苯基甲烷二异氰酸酯、二羟甲基丙酸、1，4-丁二醇、异佛尔酮二异氰酸酯和乙二胺为硬段，聚醚多元醇为软段，通过分子设计采用分步合成法，制备了具有规整硬段和良好分散性能的聚醚型聚氨酯脲水分散液。

A series of polyether based polyurethaneurea aqueous dispersions with well-defined hard segment s were prepared by fractional steps with polyether polyol, 4,4′-diphenylmethane diisocyanate,dimethylolpropionic acid,1,4-butanediol,isophorone diisocyanate and ethylenediamine.

以二苯基甲烷二异氰酸酯、二羟甲基丙酸、1，4-丁二醇、异佛尔酮二异氰酸酯和乙二胺为硬段，聚醚多元醇为软段，通过分子设计采用分步合成法，制备了具有规整硬段和良好分散性能的聚醚型聚氨酯脲水分散液。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。