二二二

In this paper, a series of low cross-linking polyurethanes are synthesized using polycaprolacton or polybutamethylene adipate or polyethylene-propylene adipate, MDI and glycerin. Their mechanical, thermal and dynamical properties and shape memory function are studied.

采用聚己二酸乙丙二醇酯、聚己二酸丁二醇酯、聚己内酯和 4，4'-二苯基甲烷二异氰酸酯为原料，以丙三醇为交联剂合成了一系列低度交联的聚氨酯，讨论了组成、配比等对性能的影响，比较了它们和线型聚氨酯在性能上的差别。

Three alicyclic dianhydrides, 1,2,3,4-cyclobutanetetracarboxylic dianhydride, 1,2,4,5-cyclopentanetetracarboxylic dianhydride, and 1,2, 4, 5-cydohexane tetracarboxylic dianhydride were polymerized with two aromatic diamines, 1,4-bis (4-amino-2-trifluoromethylphenoxy) benzene (6FAPB, a) and 4, 4'-bis(4-amino-2-trifluoromethyl phenoxy) biphenyl (6FBAB, b) respectively, via a two-step polycondensation procedure to afford two series of fluorinated semi-alicyclic polyimides.

分别将脂环族二酐单体1，2，3，4-环丁烷四酸二酐、1，2，4，5-环戊烷四酸二酐和1，2，4，5-环己烷四酸二酐与芳香族含氟二胺1，4-双（4-胺基-2-三氟甲基苯氧基）苯(6FAPB， a)和4，4'-双（4-胺基-2-三氟甲基苯氧基）联苯(6FBAB， b)反应制备两个系列的含氟半脂环族聚酰亚胺，研究了PI薄膜的热性能和光学性能。

Second, most of the content of the assigned chorus piece were chosen to meet to the elementary students' musical abilities. The form was referred to as AB; two parts songs were usually selected; the meter signature was referred to as quarter note gets one beat and beats can be grouped in twos or fours, it remained stablely in the whole tune; the tempo of assigned chorus piece almostly based on "Moderato" and "Allegretto"; the tonality are combined with the major and minor scales and also present as the pentatonic scales, the minor scale were rarely used.

二 、九十二至九十六学年度国小合唱指定曲的内容，大部分与国小音乐能力指标相符：乐曲曲式明确，以二段式居多；编制以同声二部为主；拍号以单拍子的二拍、四拍为主，少有拍号变化；速度以中板、稍快板为主；调性不完全偏向大小调乐曲，仍兼顾调式乐曲，转调变化的不多，小调乐曲较少出现。

In this paper, three robust estimators: robust best invariant quadratic unbiased estimator, robust minimum norm quadratic unbiased estimator and robust Helmert estimator have been designed. Finally, this paper states that these three classical estimators are particular cases of the RBIQUE.

导出了稳健最优不变二次无偏估计、稳健最小范数二次无偏估计、稳健Helmert估计，并说明了最优不变二次无偏估计、最小范数二次无偏估计以及Helmert估计等均是稳健最优不变二次无偏估计的特例。

To summarize two-dimensional non-normal joint distribution in use, such as Bivariate Weibull Distribution, Bivariate Log-normal Distribution, Bivariate Gumbel Distribution, and Bivariate Gamma Distribution.

归纳总结了已经出现的非正态二维联合概率分布模型，如二维威布尔分布、二维对数正态分布、二维冈贝尔分布及二维伽玛分布等。

This dissertation divides into seven chapters and the main contents and conclusions are listed as following:1. Three series binuclear lanthanide carboxylate coordination polymers 1～7 have been synthesized under hydrothermal conditions by altering the length of carbon chains between carboxyl group and phenyl ring on ligands, which are isophthalic acid, 1,3-phenylenediacetic acid and 1,3-phenoxydiacetic acid, and lanthanide ions such as Pr~(3+), Eu~(3+)and Ho~(3+).

论文共分七章，主要研究内容和结论如下：1、通过改变间苯二甲酸配体的羧基和苯环之间的碳链长度，从间苯二甲酸、间苯二乙酸到间苯二氧乙酸，以及改变稀土离子半径Pr~(3+、Eu~(3+)和Ho~(3+)出发，在水热条件下制备了三个系列双核金属单元的稀土羧酸二维配位聚合物1～7。

The method comprises: adding 4-(3,4-dichlorophenyl)-1-tetralone and solvent at a ratio of 1:(3-4) into a three-necked flask with a stirrer, heating under stirring until 4-(3,4-dichlorophenyl)-1-tetralone is completely dissolved, heating to 60-100 deg.C, refluxing for 0.5-2 h, cooling the filtrate to -5-10 deg.C, filtering, recrystallizing to obtain refined 4-(3,4-dichlorophenyl)-1-tetralone, and drying at 40-80 deg.C to obtain dry 4-(3,4-dichlorophenyl)-1-tetralone.

该方法的步骤是：在带搅拌的三颈瓶中依次加入4-(3，4-二氯苯基)-1-萘满酮和溶剂，溶剂与4-(3，4-二氯苯基)-1-萘满酮的L∶W为3～4∶1，将上述4-(3，4-二氯苯基)-1-萘满酮及混合精制溶剂搅拌下升温，使4-(3，4-二氯苯基)-1-萘满酮全部溶解，升温至60～100℃，回流0.5-2h；滤液用冰水冷却至-5～10℃，过滤，所得物料再用上述方法进行一次重结晶得到精品4-(3，4-二氯苯基)-1-萘满酮，40～80℃干燥后即得到干品4-(3，4-二氯苯基)-1-萘满酮。

Article 3. For the purpose of these Regulations, the term Yangtze River Waterway shall mean the main waterway extending from the line joining Liuheiwu (31 Degree 30 52 N, 121 Degree 18 54 E) at the lower reaches of the Estuary of the Liu River, and the signal post (31 Degree 37 34 N, 121 Degree 22 30 E) at the lower reaches of the Estuary of the Shiqiao River, Congming Island, and upwards to the upper boundary of Zhangjiagang (a line joining point 31 Degree 59 35 N, 120 Degree 20 00 E and point 31 Degree 57 13 N, 120 Degree 20 00 E).

第三条 本规定所说的长江水域，是指自浏河口下游的浏黑屋（北纬三十一度三十分五十二秒、东经一百二十一度十八分五十四秒）与崇明岛施翘河口下游的施信杆（北纬三十一度三十七分三十四秒、东经一百二十一度二十二分三十秒）联线沿长江向上至张家港上界（北纬三十一度五十九分三十五秒、东经一百二十度二十分与北纬三十一度五十七分十三秒、东经一百二十度二十分联线）之间的干线水域。

Through the analysis of oil or gas accumulation conditions of K_1n_2 in Wuerxun depression, this paper points out that there are the differences in organic matter abundance of source rock, the quality space matching relation between caprock and source rock, the lateral seal of faults and oil or gas migration form of K_1n_2 between the south and north of Wuerxun depression.

分析了乌尔逊凹陷南二段油气成藏条件，结果表明：乌尔逊凹陷南二段南北部在源岩有机质丰度、盖源质量空间匹配关系、断层侧向封闭性和油气运移形式上存在着明显的差异性；乌尔逊凹陷北部南一段源岩有机质丰度、南二段和大一段盖源质量空间匹配关系、南二段断层侧向封闭性和油气运移形式均好于南部，导致乌尔逊凹陷北部南二段油气供给、运聚及保存条件均优于南部。这即是造成乌尔逊凹陷北部南二段油气显示好于南部的根本原因

When 〓 is the family of bipartite graphs,the 〓 capacityand the 〓 valency of a graph G are referred to as the biparticitydenoted by β(Gand the bivalencydenoted by 〓(Gof G respectively;when 〓 is the family ofgraphs whose components are complete bipartite graphs,the 〓 capacity and the〓 valency of a graph G are referred to as the complete biparticitydenoted byc(Gand the complete bipartite valencydenoted by 〓(Gof G respectively;andwhen 〓 is the family of star forests,the 〓 capacity and the 〓 valency of a graphG are referred to as the star arboricitydenoted by st(Gand the star valency ofG(denoted by 〓)respectively.

以v记图G的完全二部分解中顶点υ所关联的π中完全二部图的个数，记〓这里π取遍G的所有完全二部分解。我们称υ为G的完全二部次。对一般的图，当图的阶数充分大时，P。〓和L.Pyber给出了υ的一个上界，即，〓。F.R.K.Chung等人及Z.Tuza的结果说明这一上界是不可改进的。对υ的具体值，即使是对某些特殊的图类，结果也知之甚少。P.C.Fishburn和P.L.Hammer给出了一个相关的结果：当n≤16时，〓，（在υ的定义中，以完全二部覆盖替代完全二部分解，即得〓。同时他们提出了下述公开问题。问题1。〓=？

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。