二二二

Phenyl or m -tolyl selenoamides reacted with functionalized α-haloacetic acid in 1∶1 or 1∶2 molar ratio with no catalyst in various alcohols to undergo a selenium transfer reaction. This reaction in dif-ferent molar ratios furnished the same C—Se—Se—C coupling products with a special structure bis diselenide. A new and facile method for synthesis of such bis(alkoxycarbonyl-methyl) diselenides with the advantages of mild reaction conditions, high yields, easy availability of starting materials and good chemical selectivity was provided.

芳基硒代酰胺与氯乙酸在各种醇中无催化剂下以1∶1和1∶2的比例投入，发生硒转移反应，不同原料投入比下的反应生成了同一种C—Se—Se—C偶联产物——具有多功能团的二烷氧羰基甲基二硒醚，提供了一种新的合成二烷氧羰基甲基二硒醚的简便方法，且反应具有条件温和、产率高、原料易得和选择性好等优点。

Four non-ionic europium complexes,〓-phen(11),〓·bipy(12),〓·dia(13) and 〓(14)(TTA=2-thenoyltrifluoroacetone, DBM=dibenzoylmethane, phen=phenanthroline, bipy=2,2'-bipyridine, dia=4,5- diazafluoren-9-one, dmbp=4,4'-dimethyl-2,2,-bipyridine), were synthesised and the triboluminescent phenomena of 12, 13 and 14 were firstly observed. Structure determinations of 11,12 and 14 were carried out. The triboluminescence maxima of 12 and 13 are similar to those of their photoluminescence. X-Ray structure analyses show that Eu atoms all exhibit eight-coordinate tetragonal antiprismatic geometries and complexes 11, 12 and 14 are all centrosymmetric.

二、合成了四个非离子型的铕的配合物：〓、〓、和〓(14)[HTTA=2-噻吩三氟甲酰丙酮，DBM=二苯甲酰基甲烷，phen=邻菲罗啉， bipy=2，2'-联吡啶，dia=4，5-二氮杂芴-9-酮，dmbp=4，4'-二甲基-2，2'-联吡啶]，首次报道了12、13及14的摩擦发光性质，测定了11、12及14的晶体结构，并系统地讨论了晶体结构和摩擦发光活性之间的关系。12及13的摩擦发光光谱的极大值均类似与其相应的光致发光光谱，表明它们有相同的激发态。

Using semi-quantitative RT-PCR, the differential expression profiles of eleven selected genes were confirmed in the ovaries of triploid and diploid. These genes fell in gene categories with a wide range of functions. The results indicated that triploidy affects the dynamic gene regulatory network in triploid ovary. This study established a firm basis for future investigation on characterization of crucial molecular events for normal ovarian development in shrimp.To further dissect exact gene functions for gonad development of shrimp, three differentially expressed genes between diploid and triploid ovary, PCNA (proliferating cell nuclear antigen), CAS/CSE1 (cellular apoptosis susceptibility protein/chromosome segregation 1) and SSRF (spermatogonial stem-cell renewal factor) were characterized on certain aspects.

利用抑制性消减杂交技术，建立了对虾二倍体和三倍体卵巢间的2个消减文库；在正向消减文库(以三倍体卵巢作为实验组，二倍体卵巢作为驱动组)中，鉴定到54个基因；在反向消减文库(以二倍体卵巢为实验组，三倍体卵巢为驱动组)中，鉴定到16个基因；选取11个差异表达的基因，利用半定量RT-PCR的方法对其在二倍体和三倍体卵巢间的表达进行了检测，均能很好地与消减结果相吻合；这些差异基因编码多种功能的蛋白，分析表明染色体的三倍化使三倍体卵巢中的基因调控网络受到了影响；为深入揭示维持卵巢正常发育的关键分子调控事件奠定了基础。

The samples were smeared on slides and stained with Giemsas stain. The stained smears were observed microscopically and photographed. It showed that except typical trophozoites in binary fission. the following trophozoites of abnormal morphs were also observed. for instance abnormal trophozoites with binary fission; enlarged trophozoites with round and irregular shaped eosinophilic bodies in the cell plasma; enlarged cells containing round and irregular shaped eosinophilic bodies and flagella; enlarged cells which contain 6 or 8 nuclear-like bodies and flagella, 3 or 4 embryonic forms of daughter trophozoite in one mother trophozoite; 4 trophozoite embryonic forms with fused plasma 3 trophozoites with fused plasma;4 trophozoites with fused plasma; a pair of trophozoite with binary fission fused with another trophozoite;2 pairs of trophozoite with binary fission fused each other; a trophozoite with 1 nuclear only.

结果 除观察到典型的营二分裂法繁殖的贾第虫滋养体外，还可见到多种形态异常的虫体，包括；虫体呈非典型二分裂；滋养体胀大，胞质中有团块状和不规则形状的嗜酸性物质；在胀大的贾第虫细胞内含有团块状和不规则形状的嗜酸性物质以及鞭毛；在胀大的贾第虫细胞内含有6或8个核状物以及鞭毛；在一个母体细胞中含有3或4个子体细胞的雏形；胞质互相融合的4个滋养体的雏形；胞质互相触合的3个滋养体，胞质互相融合的4个滋养体；1对营二分裂的滋养体与另一个滋养休互相融合；2对营二分裂的滋养体互相融合；仅有1个细胞核的滋养体。

The graph in isometric drawing must be consistent with the topology relations in the threedimensional model, but not be drawn in one uniform scale. Based on the result of analyzing the rules in isometric drawing, the templatebased method is proposed for representing the different and unrelated drawing rules in an uniformed way.

ISO图模型的建立：针对ISO图的自动生成时所需的工厂管道的三维模型和二维图纸模型的统一性要求，提出了一种基于点线关系模型的二三维一体化模型解决方案，把三维空间中工厂管道模型和二维图纸空间中的管道图形统一起来，为二三维模型中的各种功能提供了基础。

Of shares Amount shares Amount HK$'000 HK$'000 Authorised: Ordinary shares of HK$1.00 each 600,000,000 600,000 600,000,000 600,000 Ordinary shares, issued and fully paid: At 1 July 128,356,537 128,357 1,330,309,375 133,031 Consolidation of every ten shares of nominal value of HK$0.10 each into one share of nominal value of HK$1.00 each note (i ––(1,166,678,438)– Repurchase of shares note (ii (1,603,000)(1,603)(35,274,400)(4,674) Share option exercised note (iii 1,975,000 1,975 –– Conversion of convertible notes note (iv 40,909,090 40,909 –– At 30 June 169,637,627 169,638 128,356,537 128,357 Notes: Consolidation of share capital Pursuant to an ordinary resolution passed on 9 May 2007, the issued and unissued ordinary shares of HK$0.10 each of the Company were consolidated on the basis of every ten shares into one share of HK$1.00 each.

GOLDEN HARVEST ENTERTAINMENT LIMITED 180 Annual Report 2008 搜索公告牛即可看到网络上最快的个股公告财务报表附注截至二零零八年六月三十日止年度 28 股本及储备二零零八年二零零七年股份数目金额股份数目金额千港元千港元法定：每股面值1.00港元之普通股 600，000，000 600，000 600，000，000 600，000 已发行及缴足之普通股：于七月一日 128，356，537 128，357 1，330，309，375 133，031 每十股面值为0.10港元之股份合并为一股面值1.00港元之股份––(1，166，678，438)–购回股份(1，603，000)(1，603)(35，274，400)(4，674)已使行购股权 1，975，000 1，975 ––兑换可换股票据 40，909，090 40，909 ––于六月三十日 169，637，627 169，638 128，356，537 128，357 附注：合并股本根据于二零零七年五月九日通过之普通决议案，本公司每股面值0.10港元之已发行及未发行普通股按每十股合并为一股面值1.00港元股份之基准合并。

Starting from this dowble, firstly introduces the basic concept and the double integral method, double Integral calculation music volume and surface area of top cylinder, and the application examples in the double integral application in mechanics.

本文从二重积分入手，首先介绍了二重积分的基本概念和计算方法，二重积分计算曲顶柱体体积和曲面面积的在应用举例，以及二重积分在力学中的应用。

This study concludes the following four parts:(1) acute toxicity of several chloroanilines to zebra fish;(2) effects of chloroanilines on antioxidant defense of crucian carp;(3) effects of chloroanilines on serum sex steroids in crucian carp;(4) effects of chloroanilines on lymphocyte proliferation in crucian carp, and the detailed results and main conclusions are concluded as follows

本论文以2-氯-4-硝基苯胺、4-氯-3-硝基苯胺、2-氯-5-硝基苯胺、2，4-二氯苯胺、3，4-二氯苯胺、2，5-二氯苯胺、2，3-二氯苯胺为研究对象，研究分为四部分：(1)氯代苯胺对鱼类的急性毒性；(2)氯代苯胺对鲫鱼抗氧化系统的影响；(3)氯代苯胺对鲫鱼血清性类固醇激素水平的影响；(4)氯代苯胺对鲫鱼淋巴细胞增殖的影响。

The acute toxicities of 2-chloro-4-nitroaniline, 4-chloro-3-nitroaniline, 2-chloro-5-nitroaniline, 2, 4-dichloroaniline, 3, 4-dichloroaniline, 2, 5-dichloroaniline, 2, 3-dichloroaniline to zebra fish were conducted in lab. 48h LC〓 values were 11. 18, 4. 62, 9. 23, 9. 55, 7. 07, 6. 68, 0.62mg/L respectively, and 96h LC〓 values were 6. 99, 2. 58, 8. 63, 7. 79, 6. 08, 5. 23, 0.49mg/L respectively.

1研究了2-氯-4-硝基苯胺、4-氯-3-硝基苯胺、2-氯-5-硝基苯胺、2，4-二氯苯胺、3，4-二氯苯胺、2，5-二氯苯胺、2，3-二氯苯胺对斑马鱼的急性毒性，经计算48h LC〓分别为11.18、4.62、9.23、9.55、7.07、6.68、0.62mg/L，96h LC〓分别为6.99、2.58、8.63、7.79、6.08、5.23、0.49mg/L，这7种化合物均属于高毒物质。

The thermal decomposition kinetics of the N , N′-bis(5,5-dimethyl-2-phospha-2-thio-1,3-di- oxan-2-yl)ethylenediamine in air were studied by TG-DTG techniques. The kinetic parameters of the decomposition process for the title compound in the two main thermal decomposition steps were calculated through the Friedman and Flynn-Wall-Ozawa methods and the thermal decomposition mechanism of DPTDEDA was also studied with the Coats-Redfern and Achar methods.

以TG-DTG为手段，研究了 N ， N ′-二(5，5-二甲基-2-磷杂-2-硫代-1，3-二噁烷-2-基)乙二胺在空气中的热分解动力学，利用Friedman法、Flynn-Wall-Ozawa法对DPTDEDA进行了动力学分析，求出了该物质两个主要的热分解阶段的热分解动力学参数，同时利用Coats-Redfern法、Achar法研究了该物质的热分解机理。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。