二乙醇胺

The title compound (C21H15N5O) was obtained by the reaction of 3-methyl-1-phenyl-1H-pyrazol-5(4H)-one and 4-(2,2-dicyanovinyl)benzonitrile in water in the presence of TEBA and by recrystallization from EtOH(95%) and DMF.

水溶剂中，在三乙基苄基氯化铵存在下，由3-甲基－1-苯基－1H-吡唑－5(4H)-酮和4-（2，2-二氰基）苯基氰合成并经N，N-二甲基甲酰胺与95%乙醇的混合溶剂重结晶得到化合物C21H15N5O的晶体。

BIO-BEAUTE commits to selecting only 100%pure natural extracts: no silicone, no PEG, no petrochemical derivatives, no genetically modified organisms, no artificial coloring agents, no parabens, no EDTA, no formaldehyde, no products with ethoxyl derivatives, no phenoxyethanol.

BIO-BEAUTE 保证选择100%的纯净天然提取物：无硅胶、无聚乙二醇、无石油化学衍生物、无转基因有机体、无人工着色剂、无苯甲酸酯类、无乙二胺四乙酸、无甲醛、无羟乙基衍生产品，无无苯氧乙醇。

Ingredients:Water,Hamamelis Virgin-iana Water,Glycerin,Olive Oil Peg-7 Esters,Gm Euglena Gracilis Polysaccharide,Betaine,Aloe Barb-adensis Leaf Juice,Hydrolyzed Wheat Protein,Sodium Pca,Tocopheryl Acetate,Polysorbate 20,Creatine,Hyaluronic Acid,Tetrasodium Edta,Perfume

成分：去离子水，金缕梅蒸馏液，甘油，橄榄油，PEG-7酯类，细小裸藻多糖，甜菜碱，芦荟叶提取物，水解小麦蛋白，吡咯烷酮羧酸钠，生育酚乙酸酯，聚山梨醇酯-20，肌酸，透明质酸，乙二胺四乙酸四钠，香精，苯氧乙醇，辛二醇，山梨酸。

Some research and analysis on the reaction of 2,4-difluoronitrobenzene and nucleophilic reagent alcohol sodium (methyl alcohol ,ethyl alcohol, propyl alcohol, n-butyl alcohol, t-butyl alcohol, et hl) and the reaction choice of opposite -F in different solvent and conditions have done in this paper.

论文以2，4-二氟硝基苯为主要原料，研究了其与亲核试剂醇钠(甲醇、乙醇、丙醇、正丁醇、叔丁醇等)在不同溶剂中的反应情况，讨论了在几种代表性的溶剂——醇、四氢呋喃、苯、N，N-二甲基甲酰胺中亲核取代反应的情况，研究了温度、反应时间、亲核试剂、溶剂等条件对亲核取代反应的影响。

Project Background and Conditions: The company started research new chemical products in 1998. After two years of efforts, a series of pharmaceutical intermediate sulfathiazole leave instructions, including : 3- methyl sulfathiazole leave instructions, 2- sulfathiazole leave instructions ethanoic acid, 2- acetyl sulfathiazole leave instructions, 2-thiofuran amino ethane ,2-thiofuran acetic, 3,4,5- tighter nitrobenzene have been successfully developed. 2-thiofuran amino ethane are the precursors raw materials of series antibiotic analgesic.

二、项目建设背景及条件：1998年公司开始研究开发高新精细化工产品，经过两年的努力，已成功研制出噻吩系列医药中间体，包括：3-甲基噻吩、2-噻吩乙酸、2-乙酰噻吩、2-噻吩乙胺、2-噻吩乙醇、3，4，5-三氯硝基苯等。2-噻吩乙胺系列噻吩产品使用于血小板及血栓有关的心脏血管病及消炎镇痛等如氯吡格雷、兴孢噻吩钠、兴孢西丁、噻吩洛酸等十几种新药的前体原料，是国家政策鼓励发展和有自主知识产权的项目。

In order to carry out the separation of the azeotropic mixture dipropyl ether + 1-propyl alcohol by extractive distillation, we are studied the influence on the phase equilibria behavior four different solvent: 1-pentanol [2], butyl propionate [3], N,Ndimethylformamide [4] and 2-ethoxyethanol.

为了用萃取性蒸馏法分离二丙醚和1－丙醇组成的共沸混合物，我们正在研究4种不同溶剂对相平衡行为的影响：1-戊醇[2]、丙酸丁酯[3]、N，N－二甲基甲酰胺[4]和2-乙氧基乙醇。

As can be seen in Fig. 5, dipropyl ether will be recovered in the distillate using 1-pentanol, N,N-dimethylformamide and 2-ethoxyethanol as entrainers and butyl propionate is the only entrainer studied that inverts the volatility of the azeotropic mixture.

从图 5可以看出，使用1-戊醇、N，N-二甲基甲酰胺和2-乙氧基乙醇作为共溶剂时二丙醚将在馏分中回收，丙酸丁酯是唯一与共沸混合物挥发性相反的共溶剂。

Examples of suitable polar volatile liquid are amines ethers especially lower alkyl ethers organic acids esters ketones glycols alcohols amides ureas sulphoxides sulphones and water.

合适的极性挥发性液体的例子有胺，醚，尤其是低级烷基醚，有机酸，酯类，酮类，乙二醇，乙醇，酰胺，尿素，sulphoxides，砜和水。

This year the company operating the various organic chemical raw materials, varieties are: methanol, ethanol, ethylene glycol, butanol, isobutanol, isopropanol, glacial acetic acid, vinyl acetate, B lipid, Ding acetic acid lipid, styrene, toluene, phthalic anhydride, xylene, acetone, butanone, cyclohexanone, DMF, sulphuric acid, methyl isobutyl ketone, glycol Dingmi, three toluene, 2 Xin fat, melamine.

本公司常年经营各种有机化工原料，品种有：甲醇、乙醇、乙二醇、正丁醇、异丁醇、异丙醇、冰醋酸、醋酸乙烯、醋酸乙脂、醋酸丁脂、苯乙烯、甲苯、苯酐、二甲苯、丙酮、丁酮、环己酮、DMF、硫酸、甲基异丁基酮、乙二醇丁醚、三甲苯、二辛脂、三聚氰胺。

The company operating a variety of perennial organic chemical raw materials, varieties include: methanol, ethanol, ethylene glycol, n-butyl alcohol, isobutyl alcohol, isopropyl alcohol, acetic acid, vinyl acetate, acetic acid acetate, acetic acid Ding resin, styrene, toluene , phthalic anhydride, xylene, acetone, butanone, cyclohexanone, DMF, sulfuric acid, methyl isobutyl ketone, glycol ether, mesitylene, octyl resin, melamine.

本公司常年经营各种有机化工原料，品种有：甲醇、乙醇、乙二醇、正丁醇、异丁醇、异丙醇、冰醋酸、醋酸乙烯、醋酸乙脂、醋酸丁脂、苯乙烯、甲苯、苯酐、二甲苯、丙酮、丁酮、环己酮、DMF、硫酸、甲基异丁基酮、乙二醇丁醚、三甲苯、二辛脂、三聚氰胺。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。